#------------------------------------------------------------------------------ #$Date: 2022-09-13 03:48:08 +0200 (Tue, 13 Sep 2022) $ #$Revision: 277787 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/26/2022665.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022665 loop_ _publ_author_name 'Kayukova, Lyudmila A.' 'Vologzhanina, Anna V.' 'Yergaliyeva, Elmira M.' 'Baitursynova, Gulnur P.' 'Shulgau, Zarina T.' 'Sergazy, Shynggys' _publ_section_title ; Crystal structure and antidiabetic activity of 2-aminospiropyrazolinium tosylates and the product of O-tosylation of \b-(benzimidazol-1-yl)propioamidoxime ; _journal_coeditor_code ZO3026 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first ; ; _journal_paper_doi 10.1107/S2053229622008464 _journal_volume 78 _journal_year 2022 _chemical_formula_iupac 'C13 H19 N4 +, C7 H7 O3 S -' _chemical_formula_moiety 'C13 H19 N4 +, C7 H7 O3 S -' _chemical_formula_sum 'C20 H26 N4 O3 S' _chemical_formula_weight 402.51 _chemical_name_common ; 2-Amino-8-phenyl-1,5,8-triazaspiro[4.5]dec-1-en-5-ium tosylate ; _chemical_name_systematic ; 2-Amino-8-phenyl-1,5,8-triazaspiro[4.5]dec-1-en-5-ium 4-methylbenzenesulfonate ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 100.3150(10) _cell_angle_beta 96.5330(10) _cell_angle_gamma 95.678(2) _cell_formula_units_Z 4 _cell_length_a 8.4423(3) _cell_length_b 12.0126(4) _cell_length_c 20.3063(6) _cell_measurement_reflns_used 5975 _cell_measurement_temperature 100.0(2) _cell_measurement_theta_max 30.46 _cell_measurement_theta_min 2.42 _cell_volume 1997.85(11) _computing_cell_refinement ; SAINT (Bruker, 2013) ; _computing_data_collection ; APEX2 (Bruker, 2013) ; _computing_data_reduction ; SAINT (Bruker, 2013) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; OLEX2 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100.0(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measurement_device_type 'Bruker D8 Quest PHOTON detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0665 _diffrn_reflns_av_unetI/netI 0.0831 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 32048 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.544 _diffrn_reflns_theta_min 1.840 _exptl_absorpt_coefficient_mu 0.191 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_correction_T_min 0.6929 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2016) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.338 _exptl_crystal_description plate _exptl_crystal_F_000 856 _exptl_crystal_size_max 0.28 _exptl_crystal_size_mid 0.16 _exptl_crystal_size_min 0.03 _refine_diff_density_max 0.440 _refine_diff_density_min -0.506 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.005 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 507 _refine_ls_number_reflns 12050 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.005 _refine_ls_R_factor_all 0.0921 _refine_ls_R_factor_gt 0.0525 _refine_ls_shift/su_max 0.005 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0470P)^2^+0.5831P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1095 _refine_ls_wR_factor_ref 0.1281 _reflns_number_gt 8283 _reflns_number_total 12050 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file zo3026sup1.cif _cod_data_source_block 9 _cod_database_code 2022665 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.948 _shelx_estimated_absorpt_t_max 0.994 _shelx_hkl_file ; -1 0 0 5.70 1.80 -1 0 0 4.80 1.40 1 0 0 4.10 1.20 1 0 0 5.10 1.90 -3 0 0 96.39 11.10 -3 0 0 90.89 7.00 3 0 0 65.39 8.70 3 0 0 81.39 6.70 -4 0 0 4.90 4.80 -4 0 0 1.50 3.40 4 0 0 4.10 5.20 4 0 0 5.80 3.80 -5 0 0 473.95 20.20 -5 0 0 447.76 24.60 5 0 0 520.25 20.60 5 0 0 466.35 25.60 -6 0 0 83.39 10.10 -6 0 0 80.99 13.00 6 0 0 75.39 9.40 6 0 0 80.59 13.30 -7 0 0 574.14 26.40 -7 0 0 598.94 33.10 7 0 0 579.24 34.50 7 0 0 559.84 25.50 8 0 0 16.80 10.70 8 0 0 30.50 7.80 9 0 0 153.58 17.40 9 0 0 195.48 26.50 10 0 0 19.30 13.40 10 0 0 18.50 7.50 11 0 0 33.70 10.10 11 -1 0 -0.40 7.50 10 -1 0 -13.30 10.00 10 -1 0 6.90 4.60 9 -1 0 26.10 13.00 8 -1 0 118.09 20.00 8 -1 0 118.49 14.60 -8 1 0 115.79 18.20 7 -1 0 3.60 5.70 7 -1 0 -0.20 4.10 -7 1 0 -3.80 5.30 6 -1 0 19.10 9.10 6 -1 0 7.50 4.40 -6 1 0 6.20 6.90 5 -1 0 41.20 7.20 5 -1 0 37.60 8.80 -5 1 0 47.90 7.60 -5 1 0 40.60 9.30 4 -1 0 1.90 5.70 4 -1 0 0.50 3.40 -4 1 0 -1.20 2.90 3 -1 0 -3.90 4.10 3 -1 0 4.60 2.90 -3 1 0 -1.70 2.40 -3 1 0 -1.00 4.10 2 -1 0 39.10 6.50 2 -1 0 55.99 5.10 -2 1 0 47.50 6.60 1 -1 0 57.19 4.90 -1 1 0 66.49 5.00 0 1 0 3.20 0.80 -1 -1 0 3.80 1.80 -1 -1 0 13.60 2.10 1 1 0 8.00 2.30 1 1 0 10.80 1.80 -2 -1 0 333.77 13.90 -2 -1 0 345.67 11.80 2 1 0 355.16 14.20 2 1 0 334.87 11.50 -3 -1 0 142.19 11.10 -3 -1 0 173.98 9.30 3 1 0 186.38 12.60 3 1 0 166.98 9.00 -4 -1 0 11.40 3.80 -4 -1 0 4.70 4.80 4 1 0 14.90 6.20 -5 -1 0 4.60 3.60 -5 -1 0 -0.40 3.90 5 1 0 -5.90 4.70 5 1 0 0.20 3.00 -6 -1 0 166.68 16.00 -6 -1 0 177.18 13.20 6 1 0 184.88 18.40 6 1 0 181.88 13.00 -7 -1 0 -1.20 5.50 -7 -1 0 4.40 5.30 7 1 0 13.40 4.90 7 1 0 -0.50 7.20 -8 -1 0 45.10 10.00 8 1 0 60.99 14.60 8 1 0 37.30 8.40 9 1 0 22.80 12.10 9 1 0 9.80 6.00 10 1 0 17.30 8.30 10 1 0 14.20 14.90 11 1 0 16.50 7.10 11 -2 0 179.88 21.70 10 -2 0 6.50 6.20 10 -2 0 12.90 13.00 9 -2 0 3.80 8.70 9 -2 0 -4.70 3.70 8 -2 0 105.59 13.80 8 -2 0 94.59 18.50 -8 2 0 78.99 14.70 7 -2 0 11.00 8.90 7 -2 0 19.40 6.20 -7 2 0 8.20 7.20 6 -2 0 728.03 37.00 6 -2 0 789.22 29.50 -6 2 0 756.92 36.60 5 -2 0 0.50 3.00 5 -2 0 2.50 5.70 -5 2 0 1.90 4.90 4 -2 0 48.20 6.80 4 -2 0 41.70 9.20 -4 2 0 34.50 8.10 3 -2 0 1148.49 37.80 3 -2 0 1186.98 32.10 -3 2 0 1161.78 37.60 2 -2 0 3044.50 73.09 -2 2 0 3174.88 73.19 1 -2 0 158.68 8.60 1 -2 0 149.88 6.80 -1 2 0 168.68 8.60 0 -2 0 306.47 8.30 0 -2 0 305.57 9.20 0 2 0 301.07 8.10 0 2 0 298.17 9.10 -1 -2 0 2657.53 55.39 -1 -2 0 2770.12 57.39 1 2 0 2733.03 57.29 1 2 0 2686.33 55.49 -2 -2 0 1006.00 25.80 -2 -2 0 976.90 26.70 2 2 0 1062.29 27.40 2 2 0 1025.00 26.00 -3 -2 0 365.86 14.30 -3 -2 0 373.56 16.30 3 2 0 377.96 17.00 3 2 0 384.56 14.50 -4 -2 0 942.31 32.80 -4 -2 0 953.10 29.20 4 2 0 993.00 34.10 4 2 0 965.00 29.40 -5 -2 0 93.69 12.20 -5 -2 0 86.99 9.80 5 2 0 119.09 9.70 5 2 0 103.49 13.50 -6 -2 0 1266.27 40.10 -6 -2 0 1286.87 46.30 6 2 0 1226.98 39.30 6 2 0 1265.27 47.50 -7 -2 0 4.40 4.90 7 2 0 9.20 4.90 7 2 0 -11.10 5.20 -8 -2 0 561.94 27.90 8 2 0 597.04 27.70 8 2 0 588.64 35.40 -9 -2 0 3.70 5.00 9 2 0 1.10 8.50 9 2 0 1.40 5.20 10 2 0 158.38 18.20 10 2 0 142.89 24.60 11 2 0 2.50 6.70 11 -3 0 8.30 7.70 10 -3 0 17.40 7.70 10 -3 0 24.90 14.20 9 -3 0 1.40 9.00 9 -3 0 4.20 5.30 8 -3 0 39.20 14.00 8 -3 0 31.40 9.00 -8 3 0 37.30 11.30 7 -3 0 33.30 7.70 7 -3 0 16.40 10.60 -7 3 0 12.50 8.50 6 -3 0 38.40 11.90 6 -3 0 72.59 10.20 -6 3 0 63.89 12.40 5 -3 0 365.26 18.30 5 -3 0 385.96 24.60 -5 3 0 366.16 23.50 4 -3 0 2.30 3.70 4 -3 0 -5.20 3.70 -4 3 0 -2.80 4.10 3 -3 0 536.35 24.10 -3 3 0 479.45 22.60 2 -3 0 518.75 21.20 -2 3 0 532.05 20.90 1 -3 0 12.30 3.00 1 -3 0 12.50 3.90 -1 3 0 15.70 3.10 -1 3 0 7.20 3.10 0 -3 0 35.90 3.60 0 3 0 40.80 3.80 -1 -3 0 433.46 13.30 1 3 0 410.16 13.10 -2 -3 0 151.48 8.00 -2 -3 0 148.99 7.20 2 3 0 153.88 7.90 2 3 0 165.28 7.90 -3 -3 0 26.80 5.20 3 3 0 23.10 5.40 3 3 0 29.30 4.80 -4 -3 0 453.55 18.30 -4 -3 0 465.45 20.20 4 3 0 449.26 20.70 4 3 0 479.65 18.50 -5 -3 0 90.49 10.30 -5 -3 0 77.19 11.10 5 3 0 81.59 11.70 5 3 0 91.49 8.80 -6 -3 0 266.97 16.30 -6 -3 0 244.38 18.20 6 3 0 283.77 20.80 6 3 0 259.17 15.50 -7 -3 0 45.70 9.40 7 3 0 42.70 10.90 7 3 0 37.90 7.50 -8 -3 0 48.00 9.40 8 3 0 39.50 8.90 8 3 0 31.70 11.30 -9 -3 0 3.60 5.00 9 3 0 0.40 4.60 9 3 0 1.00 8.60 -10 -3 0 14.30 6.90 10 3 0 11.90 6.60 10 3 0 6.80 9.80 11 3 0 16.30 7.30 11 -4 0 24.90 9.80 10 -4 0 64.49 12.70 9 -4 0 33.50 8.80 9 -4 0 25.70 15.40 8 -4 0 6.00 9.20 8 -4 0 8.10 5.80 -8 4 0 30.00 10.50 7 -4 0 438.96 23.50 7 -4 0 395.86 30.90 -7 4 0 463.65 30.90 6 -4 0 -0.70 3.50 -6 4 0 0.80 5.30 5 -4 0 1309.27 49.90 5 -4 0 1328.87 41.00 -5 4 0 1282.37 48.10 4 -4 0 4.80 6.00 4 -4 0 -0.10 3.20 -4 4 0 1.00 5.10 3 -4 0 1880.01 54.99 -3 4 0 1879.61 54.09 2 -4 0 167.58 12.30 2 -4 0 157.48 9.30 -2 4 0 145.79 11.30 1 -4 0 954.00 25.90 -1 4 0 902.81 25.50 -1 4 0 937.51 26.60 0 -4 0 0.70 1.80 0 -4 0 0.60 1.80 0 4 0 -1.50 1.40 -1 -4 0 328.57 12.20 1 4 0 341.37 12.50 -2 -4 0 493.35 16.70 2 4 0 485.95 16.50 2 4 0 470.35 12.90 -3 -4 0 98.09 7.90 3 4 0 99.59 7.70 3 4 0 114.79 9.70 -4 -4 0 1031.70 31.90 4 4 0 1099.59 33.70 4 4 0 1054.49 31.80 -5 -4 0 125.99 10.20 5 4 0 145.19 10.60 5 4 0 123.19 12.40 -6 -4 0 429.96 21.00 6 4 0 396.36 23.30 6 4 0 413.16 20.20 -7 -4 0 23.40 6.40 7 4 0 14.50 7.70 7 4 0 15.80 5.20 -8 -4 0 18.50 5.70 8 4 0 23.90 7.80 8 4 0 5.40 7.00 -9 -4 0 15.00 7.70 9 4 0 19.60 7.80 9 4 0 28.30 10.80 10 4 0 10.50 6.20 10 4 0 -15.50 10.40 11 4 0 -26.20 13.60 11 -5 0 -6.40 8.80 10 -5 0 14.60 6.80 9 -5 0 -11.30 8.40 9 -5 0 -4.80 4.50 8 -5 0 12.60 8.80 -8 5 0 1.50 11.90 7 -5 0 28.10 7.40 7 -5 0 30.90 11.40 -7 5 0 33.20 11.30 6 -5 0 9.10 8.80 6 -5 0 22.50 6.50 -6 5 0 22.20 10.10 5 -5 0 139.09 17.90 5 -5 0 162.28 12.50 -5 5 0 162.18 16.30 4 -5 0 194.28 17.20 4 -5 0 203.78 12.60 -4 5 0 165.08 15.60 3 -5 0 27.30 5.70 3 -5 0 15.80 6.90 2 -5 0 253.17 12.50 2 -5 0 256.97 15.70 -2 5 0 269.87 15.10 1 -5 0 575.84 20.60 1 -5 0 597.04 19.50 -1 5 0 559.34 19.20 -1 5 0 551.44 19.40 0 -5 0 0.00 1.80 0 -5 0 2.40 2.40 0 5 0 2.20 1.70 -1 -5 0 24.30 4.20 1 5 0 29.40 4.80 -2 -5 0 6.80 3.10 2 5 0 9.40 3.00 -3 -5 0 26.60 5.10 3 5 0 20.40 4.20 3 5 0 30.00 4.00 -4 -5 0 24.10 5.00 4 5 0 31.30 5.70 4 5 0 29.20 5.40 -5 -5 0 23.90 6.20 5 5 0 19.20 5.20 5 5 0 25.80 6.10 -6 -5 0 27.40 7.80 6 5 0 30.60 6.30 6 5 0 33.10 8.30 -7 -5 0 1.40 4.20 7 5 0 1.00 6.00 7 5 0 -0.30 2.70 -8 -5 0 193.28 16.70 8 5 0 199.58 17.60 -9 -5 0 10.40 9.50 9 5 0 3.80 7.60 9 5 0 1.70 3.90 10 5 0 -10.90 9.60 10 5 0 12.80 6.30 11 -6 0 44.70 12.40 10 -6 0 -3.80 5.20 9 -6 0 79.79 20.20 9 -6 0 79.39 13.70 8 -6 0 62.19 12.40 8 -6 0 59.99 15.60 7 -6 0 115.79 19.40 7 -6 0 86.79 12.90 -7 6 0 92.59 17.70 6 -6 0 267.37 18.10 6 -6 0 294.67 25.00 -6 6 0 308.07 24.70 5 -6 0 -6.20 5.50 5 -6 0 1.00 2.60 -5 6 0 -1.70 4.60 4 -6 0 7.60 3.70 4 -6 0 0.90 5.50 -4 6 0 -2.60 5.10 3 -6 0 146.69 14.40 3 -6 0 162.68 11.30 -3 6 0 140.09 12.90 2 -6 0 -1.10 3.90 2 -6 0 -0.60 2.40 -2 6 0 2.60 3.50 1 -6 0 886.91 26.80 1 -6 0 801.42 26.80 0 -6 0 7.40 3.00 0 -6 0 7.10 2.70 0 6 0 7.70 3.00 -1 -6 0 200.68 10.60 1 6 0 184.78 10.70 -2 -6 0 16.20 3.80 2 6 0 14.40 4.00 -3 -6 0 805.92 26.30 3 6 0 782.02 26.00 3 6 0 776.32 18.10 3 6 0 754.52 17.60 -4 -6 0 204.38 12.50 4 6 0 186.38 13.70 4 6 0 203.08 12.40 -5 -6 0 1041.30 34.60 5 6 0 1020.80 34.00 5 6 0 983.30 31.60 -6 -6 0 79.19 10.90 6 6 0 66.59 9.80 6 6 0 78.39 10.60 -7 -6 0 112.99 13.20 7 6 0 95.19 13.00 7 6 0 119.09 13.60 -8 -6 0 88.29 13.30 8 6 0 76.69 13.00 8 6 0 77.49 12.00 -9 -6 0 24.50 8.20 9 6 0 16.70 6.80 9 6 0 1.50 7.90 10 6 0 -9.10 10.00 10 6 0 12.90 7.40 11 -7 0 2.10 8.20 10 -7 0 74.09 14.70 9 -7 0 8.10 5.30 9 -7 0 9.00 11.20 9 -7 0 -3.60 6.10 8 -7 0 6.30 5.80 8 -7 0 25.10 11.90 8 -7 0 1.80 5.60 7 -7 0 17.00 5.60 7 -7 0 23.00 7.00 7 -7 0 2.80 7.80 6 -7 0 122.99 19.00 6 -7 0 104.79 13.50 6 -7 0 150.48 14.10 -6 7 0 99.89 16.40 5 -7 0 145.59 19.70 5 -7 0 132.59 12.00 -5 7 0 143.29 18.80 4 -7 0 188.18 17.70 4 -7 0 215.28 14.10 -4 7 0 196.58 16.90 3 -7 0 50.69 10.20 3 -7 0 51.49 8.00 -3 7 0 49.20 9.30 2 -7 0 132.19 9.70 2 -7 0 122.99 12.10 -2 7 0 137.39 10.20 1 -7 0 53.79 7.30 1 -7 0 49.50 7.30 -1 7 0 67.59 8.40 0 -7 0 77.39 5.80 0 -7 0 74.29 7.10 0 7 0 78.19 7.30 -1 -7 0 274.47 13.50 1 7 0 249.38 13.20 -2 -7 0 4.20 2.70 2 7 0 2.40 2.40 -3 -7 0 484.95 20.30 3 7 0 503.85 20.40 -4 -7 0 41.10 7.20 4 7 0 44.30 3.10 4 7 0 55.49 8.00 4 7 0 45.50 3.30 5 7 0 -1.10 3.00 5 7 0 1.00 2.90 -6 -7 0 19.70 5.90 6 7 0 12.30 4.60 6 7 0 7.60 4.50 -7 -7 0 -2.70 4.50 7 7 0 -2.70 3.60 7 7 0 5.70 4.10 -8 -7 0 66.49 12.30 8 7 0 95.89 13.20 8 7 0 88.39 12.60 -9 -7 0 4.20 7.20 9 7 0 8.70 7.60 9 7 0 26.20 7.70 10 7 0 47.10 12.30 10 7 0 109.69 16.60 11 -8 0 2.50 10.60 10 -8 0 95.99 16.40 9 -8 0 13.60 7.90 8 -8 0 48.20 10.00 8 -8 0 62.39 13.00 7 -8 0 19.50 8.00 7 -8 0 29.90 11.30 7 -8 0 17.50 6.40 6 -8 0 58.49 10.00 6 -8 0 67.59 15.20 6 -8 0 82.19 13.00 5 -8 0 205.28 21.20 5 -8 0 194.58 14.80 4 -8 0 5.50 5.40 3 -8 0 486.75 26.00 3 -8 0 412.66 20.40 2 -8 0 171.98 11.90 2 -8 0 156.08 13.40 -2 8 0 176.58 12.30 1 -8 0 291.87 15.30 1 -8 0 330.87 16.00 -1 8 0 300.37 15.70 0 -8 0 40.20 4.50 0 -8 0 30.50 3.70 0 -8 0 36.30 6.30 0 8 0 30.10 5.70 -1 -8 0 317.67 15.80 1 8 0 356.36 16.90 -2 -8 0 35.90 6.30 2 8 0 32.10 6.20 -3 -8 0 6.20 3.70 3 8 0 3.90 2.70 -4 -8 0 78.79 9.80 4 8 0 66.99 9.40 -5 -8 0 2.90 4.00 5 8 0 3.60 3.60 -6 -8 0 61.99 10.00 6 8 0 41.10 8.10 6 8 0 44.80 5.40 6 8 0 47.80 5.70 -7 -8 0 250.87 18.60 7 8 0 241.58 13.70 7 8 0 254.87 14.20 -8 -8 0 12.10 11.70 8 8 0 6.70 4.00 8 8 0 -4.60 3.90 8 8 0 6.50 4.70 9 8 0 123.59 13.10 9 8 0 124.39 14.40 9 8 0 109.09 15.70 10 -9 0 39.90 11.60 9 -9 0 3.00 6.90 8 -9 0 21.20 14.50 8 -9 0 1.90 6.10 8 -9 0 11.70 7.10 7 -9 0 5.40 5.10 7 -9 0 -6.10 3.80 7 -9 0 -7.20 7.70 6 -9 0 159.58 17.60 6 -9 0 148.39 21.20 5 -9 0 2.50 4.10 5 -9 0 13.90 7.90 4 -9 0 188.28 14.20 4 -9 0 171.18 20.60 3 -9 0 53.29 11.10 2 -9 0 85.99 11.80 2 -9 0 90.49 10.90 -2 9 0 74.29 9.80 1 -9 0 194.48 12.90 1 -9 0 191.38 12.50 -1 9 0 184.08 13.00 0 -9 0 3.60 1.90 0 -9 0 2.00 3.30 0 -9 0 5.20 1.60 0 9 0 3.50 3.20 -1 -9 0 662.13 25.30 1 9 0 640.04 25.30 -2 -9 0 188.48 12.70 2 9 0 166.68 12.30 -3 -9 0 143.09 11.70 3 9 0 131.99 11.50 -4 -9 0 88.69 11.00 4 9 0 102.99 11.80 -5 -9 0 7.10 5.10 5 9 0 2.40 3.40 -6 -9 0 11.20 5.20 6 9 0 4.80 4.20 -7 -9 0 25.80 8.10 7 9 0 21.30 2.50 7 9 0 25.30 7.60 7 9 0 17.60 2.30 -8 -9 0 1.30 6.80 8 9 0 6.20 5.10 8 9 0 -4.20 2.50 8 9 0 -3.70 3.10 9 9 0 -2.50 4.90 9 9 0 10.30 6.60 10 -10 0 2.30 7.30 9 -10 0 23.80 10.20 8 -10 0 3.60 6.50 8 -10 0 1.20 10.90 7 -10 0 7.80 5.90 7 -10 0 11.00 6.60 7 -10 0 -1.90 9.60 6 -10 0 65.29 17.30 6 -10 0 79.59 12.30 5 -10 0 6.90 4.70 5 -10 0 1.20 5.90 4 -10 0 97.79 16.70 4 -10 0 110.89 13.50 3 -10 0 71.29 10.70 3 -10 0 74.09 13.20 2 -10 0 -3.20 1.80 2 -10 0 -2.20 4.70 -2 10 0 3.50 3.60 1 -10 0 23.90 5.90 -1 10 0 50.49 8.30 0 -10 0 24.00 2.30 0 -10 0 23.20 2.00 0 -10 0 30.50 6.00 0 10 0 26.10 6.10 -1 -10 0 253.17 15.60 1 10 0 223.78 14.90 -2 -10 0 424.66 21.00 2 10 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5.40 7 -13 3 -3.90 14.50 7 -13 3 19.00 7.90 8 -13 3 -1.40 7.20 7 12 -3 39.40 9.10 -7 -12 3 53.89 11.80 6 12 -3 -2.10 4.40 -6 -12 3 1.20 5.50 5 12 -3 49.60 9.20 -5 -12 3 37.50 8.40 4 12 -3 6.80 4.30 -4 -12 3 2.30 4.10 3 12 -3 25.20 6.50 -3 -12 3 24.70 6.00 2 12 -3 11.80 4.50 -2 -12 3 5.10 4.30 1 12 -3 15.00 4.90 -1 -12 3 14.60 4.70 0 12 -3 23.30 6.30 0 -12 3 23.80 5.70 0 -12 3 28.30 3.60 0 -12 3 38.20 3.20 1 -12 3 8.70 3.20 1 -12 3 12.50 4.70 1 -12 3 13.20 5.20 2 -12 3 124.39 11.50 2 -12 3 121.09 15.20 2 -12 3 116.89 11.50 3 -12 3 60.79 10.10 3 -12 3 56.69 12.30 4 -12 3 23.60 7.30 4 -12 3 34.30 10.50 5 -12 3 92.69 18.40 5 -12 3 105.49 14.20 6 -12 3 -1.50 9.50 6 -12 3 -1.50 6.00 6 -12 3 15.20 6.30 7 -12 3 96.09 16.80 7 -12 3 86.99 21.50 8 -12 3 29.30 10.50 9 -12 3 24.20 9.50 8 11 -3 33.40 8.40 -8 -11 3 63.09 12.30 7 11 -3 12.40 6.10 -7 -11 3 26.50 7.90 6 11 -3 28.40 7.20 -6 -11 3 21.00 6.70 5 11 -3 2.70 4.30 -5 -11 3 2.60 4.20 4 11 -3 10.70 4.20 -4 -11 3 3.60 4.50 3 11 -3 261.07 15.80 -3 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2 -10 3 11.70 4.40 3 -10 3 40.10 9.90 3 -10 3 64.39 9.70 4 -10 3 7.60 4.60 4 -10 3 -10.60 5.90 5 -10 3 20.70 8.90 5 -10 3 11.90 5.90 6 -10 3 115.29 15.80 6 -10 3 142.99 17.00 6 -10 3 110.09 19.40 7 -10 3 -1.80 7.90 7 -10 3 7.60 5.70 7 -10 3 7.20 6.30 8 -10 3 34.30 10.10 8 -10 3 65.49 16.60 9 -10 3 1.30 7.10 10 -10 3 14.80 9.20 9 9 -3 117.89 11.50 9 9 -3 92.49 12.80 -9 -9 3 138.99 18.00 8 9 -3 7.50 4.50 8 9 -3 9.70 6.30 -8 -9 3 10.90 7.20 7 9 -3 78.09 11.30 7 9 -3 75.79 6.90 -7 -9 3 101.79 14.00 6 9 -3 15.50 6.40 -6 -9 3 13.10 5.70 5 9 -3 1.60 3.10 -5 -9 3 6.70 4.80 4 9 -3 109.99 9.50 -4 -9 3 124.19 10.20 3 9 -3 148.89 10.80 -3 -9 3 147.99 10.50 2 9 -3 248.68 13.70 -2 -9 3 238.68 13.10 1 9 -3 96.59 8.70 -1 -9 3 100.09 4.60 -1 -9 3 96.99 8.30 -1 -9 3 95.49 5.20 0 9 -3 21.20 5.20 0 -9 3 14.60 3.10 0 -9 3 17.80 4.40 0 -9 3 23.00 5.00 1 -9 3 18.90 5.20 1 -9 3 20.90 4.70 1 -9 3 14.70 5.60 2 -9 3 11.60 4.30 2 -9 3 12.50 6.00 3 -9 3 22.50 8.30 3 -9 3 24.40 5.90 4 -9 3 47.00 11.10 4 -9 3 53.39 8.90 5 -9 3 30.70 11.50 5 -9 3 24.30 7.50 5 -9 3 36.00 8.20 6 -9 3 28.40 8.00 6 -9 3 52.79 14.00 6 -9 3 33.60 8.40 7 -9 3 71.69 13.00 7 -9 3 69.09 11.90 7 -9 3 117.39 20.50 8 -9 3 110.79 21.60 8 -9 3 102.49 14.30 8 -9 3 81.49 12.80 9 -9 3 26.00 9.60 10 -9 3 23.20 10.20 9 8 -3 -5.40 5.00 -9 -8 3 7.80 8.60 8 8 -3 43.60 8.20 -8 -8 3 56.89 10.90 7 8 -3 42.90 7.10 7 8 -3 47.10 8.90 -7 -8 3 44.80 9.90 6 8 -3 18.10 5.60 6 8 -3 35.50 5.90 -6 -8 3 36.40 7.40 5 8 -3 70.19 5.40 5 8 -3 91.19 10.70 -5 -8 3 86.39 10.20 4 8 -3 40.60 6.40 4 8 -3 34.00 3.00 -4 -8 3 35.60 6.00 3 8 -3 273.37 13.90 -3 -8 3 261.97 13.40 2 8 -3 0.50 1.80 -2 -8 3 -0.20 2.30 1 8 -3 535.25 20.00 -1 -8 3 555.94 15.00 -1 -8 3 521.55 15.90 -1 -8 3 540.05 19.70 0 8 -3 239.08 12.40 0 -8 3 209.38 11.80 0 -8 3 213.78 11.70 0 -8 3 233.48 10.50 1 -8 3 220.88 13.00 1 -8 3 223.18 12.50 1 -8 3 210.38 13.80 2 -8 3 0.10 3.50 2 -8 3 2.20 3.00 3 -8 3 129.09 10.70 3 -8 3 164.38 15.60 4 -8 3 224.58 20.70 4 -8 3 211.88 14.50 5 -8 3 429.76 23.00 5 -8 3 385.46 20.90 5 -8 3 440.66 29.30 6 -8 3 520.05 26.00 6 -8 3 462.75 32.30 6 -8 3 520.95 26.80 7 -8 3 236.88 24.60 7 -8 3 227.98 18.60 7 -8 3 214.68 17.60 8 -8 3 147.39 23.00 8 -8 3 152.38 19.00 8 -8 3 116.59 15.30 9 -8 3 10.80 7.10 10 7 -3 -0.60 9.30 10 7 -3 40.30 8.70 9 7 -3 31.60 8.00 9 7 -3 19.60 8.90 -9 -7 3 24.90 9.10 8 7 -3 -11.80 4.20 8 7 -3 6.60 4.60 -8 -7 3 -0.10 4.60 7 7 -3 31.40 7.20 7 7 -3 34.70 7.50 -7 -7 3 21.60 6.60 6 7 -3 21.10 5.10 6 7 -3 31.30 6.10 -6 -7 3 30.30 6.60 5 7 -3 82.79 9.80 5 7 -3 78.09 7.10 -5 -7 3 80.39 8.10 -5 -7 3 71.49 8.80 4 7 -3 221.28 12.60 4 7 -3 225.08 9.80 -4 -7 3 229.18 11.60 -4 -7 3 220.58 12.40 3 7 -3 101.99 5.10 3 7 -3 85.19 7.40 -3 -7 3 109.69 8.00 -3 -7 3 96.29 6.10 2 7 -3 137.89 8.80 -2 -7 3 131.99 8.50 -2 -7 3 140.39 6.30 1 7 -3 106.29 7.50 -1 -7 3 111.49 5.70 -1 -7 3 124.39 8.00 0 7 -3 56.69 6.70 0 -7 3 46.80 4.90 0 -7 3 57.09 6.70 0 -7 3 43.30 6.20 1 -7 3 122.19 9.70 1 -7 3 132.39 10.80 1 -7 3 136.89 9.20 2 -7 3 52.89 7.30 2 -7 3 53.49 8.80 3 -7 3 235.38 17.70 3 -7 3 206.78 13.00 4 -7 3 150.78 16.10 4 -7 3 145.39 11.30 5 -7 3 -0.60 4.20 6 -7 3 14.20 8.60 6 -7 3 12.80 5.90 7 -7 3 -1.30 7.60 7 -7 3 2.40 4.50 8 -7 3 24.30 12.40 9 -7 3 -2.40 10.20 9 -7 3 12.30 5.50 10 -7 3 29.90 9.50 11 -7 3 5.40 9.20 10 6 -3 6.20 6.10 10 6 -3 -11.90 8.70 -10 -6 3 -1.40 8.00 9 6 -3 2.80 4.30 9 6 -3 2.40 6.90 -9 -6 3 -0.10 5.20 8 6 -3 6.30 6.80 8 6 -3 1.60 3.60 -8 -6 3 2.50 4.40 7 6 -3 228.58 17.00 7 6 -3 244.58 15.60 -7 -6 3 218.78 15.50 -7 -6 3 240.28 18.40 6 6 -3 8.80 4.70 6 6 -3 6.20 3.80 -6 -6 3 2.40 3.50 -6 -6 3 -1.30 3.30 5 6 -3 500.55 20.30 5 6 -3 507.85 20.70 -5 -6 3 470.95 20.00 -5 -6 3 505.15 22.30 4 6 -3 0.20 2.10 4 6 -3 3.80 2.20 -4 -6 3 1.10 2.40 -4 -6 3 2.00 3.60 3 6 -3 40.50 4.10 3 6 -3 37.50 5.10 -3 -6 3 38.00 5.10 -3 -6 3 32.10 4.80 2 6 -3 59.79 4.20 2 6 -3 53.99 5.90 -2 -6 3 72.09 5.80 -2 -6 3 57.29 5.30 1 6 -3 483.65 16.50 -1 -6 3 495.15 16.40 -1 -6 3 509.25 14.60 0 6 -3 431.56 15.20 0 -6 3 400.76 14.70 0 -6 3 390.46 14.30 1 -6 3 221.68 13.00 1 -6 3 239.88 11.50 2 -6 3 85.59 7.40 2 -6 3 85.79 11.00 3 -6 3 166.78 15.10 3 -6 3 172.48 11.30 4 -6 3 35.70 6.70 4 -6 3 47.10 11.40 5 -6 3 101.29 12.00 5 -6 3 98.49 15.90 6 -6 3 100.09 13.40 6 -6 3 96.89 17.40 7 -6 3 120.39 15.70 7 -6 3 118.39 20.00 8 -6 3 172.48 25.60 8 -6 3 202.28 17.10 9 -6 3 19.40 7.70 9 -6 3 7.30 13.60 10 -6 3 156.98 20.20 11 -6 3 -1.90 8.50 11 5 -3 27.10 10.00 11 5 -3 23.20 14.30 10 5 -3 23.30 10.90 10 5 -3 17.90 6.10 -10 -5 3 30.30 9.60 9 5 -3 2.70 4.50 9 5 -3 1.10 7.30 -9 -5 3 7.10 6.70 8 5 -3 7.80 6.50 8 5 -3 -2.00 3.00 -8 -5 3 -1.80 5.40 -8 -5 3 3.10 5.30 7 5 -3 181.28 13.50 7 5 -3 177.58 16.10 -7 -5 3 201.28 17.50 -7 -5 3 165.48 13.60 6 5 -3 28.50 5.90 6 5 -3 36.30 8.00 -6 -5 3 35.80 8.70 -6 -5 3 40.40 7.70 5 5 -3 466.25 19.10 5 5 -3 479.15 21.40 -5 -5 3 460.65 19.40 -5 -5 3 480.95 23.00 4 5 -3 2.90 2.60 -4 -5 3 -0.20 3.30 -4 -5 3 2.20 2.70 3 5 -3 584.14 19.10 3 5 -3 599.44 18.70 -3 -5 3 605.24 21.20 -3 -5 3 621.74 19.50 2 5 -3 58.19 4.30 2 5 -3 66.89 5.00 -2 -5 3 69.59 6.10 -2 -5 3 56.29 4.90 1 5 -3 281.17 10.40 1 5 -3 269.27 10.50 -1 -5 3 268.27 10.30 -1 -5 3 281.87 9.80 0 5 -3 -0.50 1.50 0 -5 3 0.70 1.50 0 -5 3 -1.10 1.30 1 -5 3 375.46 16.30 1 -5 3 339.67 13.30 2 -5 3 323.87 13.80 2 -5 3 316.37 17.20 3 -5 3 427.66 22.60 3 -5 3 433.36 18.30 4 -5 3 60.49 11.50 4 -5 3 63.89 9.10 5 -5 3 129.99 18.10 5 -5 3 111.19 10.80 6 -5 3 102.29 17.80 6 -5 3 132.99 12.80 7 -5 3 -0.30 6.50 7 -5 3 -7.50 2.80 8 -5 3 4.80 7.50 8 -5 3 10.40 6.30 9 -5 3 9.20 10.90 9 -5 3 4.60 4.80 10 -5 3 1.00 5.70 11 -5 3 13.20 8.40 11 4 -3 0.80 6.40 11 4 -3 -40.80 13.40 10 4 -3 13.50 6.90 10 4 -3 19.10 12.50 9 4 -3 7.50 5.00 9 4 -3 -5.90 6.50 -9 -4 3 3.00 5.30 8 4 -3 22.60 8.00 8 4 -3 26.70 7.70 -8 -4 3 20.90 8.90 -8 -4 3 28.30 7.50 7 4 -3 106.29 12.00 7 4 -3 118.49 15.70 -7 -4 3 94.79 15.30 6 4 -3 693.93 25.80 6 4 -3 674.53 30.40 -6 -4 3 679.33 31.40 -6 -4 3 648.84 25.50 5 4 -3 21.00 4.60 5 4 -3 23.40 6.60 -5 -4 3 19.20 7.20 -5 -4 3 17.40 4.80 4 4 -3 627.44 20.90 4 4 -3 621.34 23.60 -4 -4 3 639.54 25.60 -4 -4 3 689.43 21.90 3 4 -3 497.65 17.60 3 4 -3 462.85 15.70 -3 -4 3 458.05 15.90 -3 -4 3 493.45 19.50 2 4 -3 93.49 5.50 2 4 -3 85.79 5.50 -2 -4 3 84.09 6.80 -2 -4 3 85.89 5.40 1 4 -3 46.60 3.80 1 4 -3 42.10 3.50 -1 -4 3 51.89 3.80 -1 -4 3 35.80 3.70 0 4 -3 99.19 5.40 0 -4 3 100.89 5.50 0 -4 3 99.99 6.20 1 -4 3 331.07 12.00 2 -4 3 12.10 4.80 3 -4 3 319.07 18.80 4 -4 3 13.10 4.30 4 -4 3 4.80 5.70 5 -4 3 124.99 11.20 5 -4 3 126.59 16.50 6 -4 3 -0.60 6.50 6 -4 3 10.80 5.30 7 -4 3 10.10 9.10 7 -4 3 5.50 5.00 8 -4 3 0.10 7.70 9 -4 3 9.20 5.80 9 -4 3 -1.20 8.60 10 -4 3 8.10 7.40 11 -4 3 -11.10 5.70 11 3 -3 -6.40 5.30 10 3 -3 1.20 5.60 10 3 -3 -8.40 9.30 9 3 -3 2.60 9.60 -9 -3 3 15.50 7.20 8 3 -3 27.90 7.30 8 3 -3 21.70 9.20 -8 -3 3 29.50 7.70 -8 -3 3 24.90 8.70 7 3 -3 68.69 10.20 7 3 -3 64.79 13.40 -7 -3 3 52.69 9.90 -7 -3 3 43.50 10.40 6 3 -3 28.40 9.20 6 3 -3 25.70 6.00 -6 -3 3 37.30 6.90 -6 -3 3 19.70 8.10 5 3 -3 62.49 7.40 5 3 -3 63.19 10.10 -5 -3 3 71.79 11.30 -5 -3 3 63.09 7.90 4 3 -3 5.10 2.70 4 3 -3 9.10 4.80 -4 -3 3 -0.90 4.30 -4 -3 3 2.50 2.50 3 3 -3 156.78 7.80 3 3 -3 152.28 10.10 -3 -3 3 151.78 7.90 -3 -3 3 130.19 10.70 2 3 -3 140.49 7.90 2 3 -3 148.19 6.30 -2 -3 3 132.09 6.20 -2 -3 3 144.09 8.90 1 3 -3 133.99 5.20 1 3 -3 142.69 6.50 -1 -3 3 138.09 5.20 -1 -3 3 150.78 6.90 0 3 -3 84.79 6.10 0 -3 3 84.29 4.20 0 -3 3 91.19 5.70 -1 3 -3 693.43 18.20 -1 3 -3 694.83 17.20 2 -3 3 16.60 5.10 2 -3 3 13.30 3.70 3 -3 3 112.79 8.50 3 -3 3 116.89 11.70 4 -3 3 20.20 7.70 4 -3 3 17.80 4.90 5 -3 3 13.70 4.80 5 -3 3 34.90 9.90 6 -3 3 35.30 11.80 6 -3 3 26.40 6.70 7 -3 3 5.60 4.70 7 -3 3 4.30 8.30 8 -3 3 74.29 16.50 8 -3 3 62.79 11.40 9 -3 3 -7.20 7.30 9 -3 3 2.40 4.90 10 -3 3 28.60 9.00 11 -3 3 10.20 8.30 11 2 -3 14.60 8.10 10 2 -3 54.49 11.60 9 2 -3 11.50 6.20 9 2 -3 7.10 9.30 -9 -2 3 8.80 6.20 8 2 -3 177.58 21.50 8 2 -3 169.08 14.20 -8 -2 3 215.48 21.00 7 2 -3 119.29 11.20 7 2 -3 115.29 16.20 -7 -2 3 115.99 17.30 -7 -2 3 143.19 12.20 6 2 -3 214.38 18.30 6 2 -3 233.28 13.70 -6 -2 3 221.48 13.80 -6 -2 3 212.28 18.70 5 2 -3 10.20 4.00 5 2 -3 13.50 6.40 -5 -2 3 9.40 6.10 -5 -2 3 18.20 5.00 4 2 -3 2.70 2.50 4 2 -3 3.70 4.20 -4 -2 3 10.90 5.60 -4 -2 3 5.40 2.90 3 2 -3 445.76 18.90 3 2 -3 471.25 14.90 -3 -2 3 459.65 15.10 -3 -2 3 473.05 20.30 2 2 -3 914.01 28.70 2 2 -3 1004.60 22.90 -2 -2 3 958.60 27.70 -2 -2 3 961.30 22.90 1 2 -3 1372.26 28.50 1 2 -3 1380.76 32.30 -1 -2 3 1376.96 32.70 -1 -2 3 1385.16 28.50 0 2 -3 72.19 5.20 0 -2 3 74.49 4.90 1 -2 3 2272.47 49.30 -2 2 -3 97.69 6.90 2 -2 3 95.29 6.70 -3 2 -3 118.99 8.60 3 -2 3 129.89 8.70 3 -2 3 115.69 11.00 -4 2 -3 618.34 22.60 4 -2 3 572.84 27.40 4 -2 3 572.84 21.90 -5 2 -3 2.10 3.80 5 -2 3 8.10 6.40 5 -2 3 -0.10 3.10 -6 2 -3 359.56 19.70 6 -2 3 361.36 26.00 6 -2 3 368.76 19.60 7 -2 3 28.70 7.40 7 -2 3 56.09 14.30 8 -2 3 456.05 25.20 8 -2 3 471.05 33.90 9 -2 3 100.99 14.60 9 -2 3 103.89 19.80 10 -2 3 87.49 20.30 10 -2 3 109.29 15.90 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0.40 4.30 -2 12 3 0.10 4.10 1 -12 -3 72.79 6.00 1 -12 -3 58.69 5.20 1 -12 -3 77.69 12.60 0 -12 -3 29.80 7.80 0 12 3 51.29 15.50 -1 -12 -3 157.78 14.00 1 12 3 160.68 21.10 -2 -12 -3 6.90 5.80 2 12 3 5.20 4.90 -3 -12 -3 34.20 8.80 3 12 3 29.00 8.60 -4 -12 -3 2.00 5.40 4 12 3 1.80 5.30 -5 -12 -3 -3.50 5.90 5 12 3 -2.10 4.90 6 12 3 45.70 10.70 8 -13 -3 20.50 9.20 7 -13 -3 67.89 18.10 6 -13 -3 -15.40 8.40 5 -13 -3 -3.20 8.60 4 -13 -3 -0.40 6.00 4 -13 -3 0.40 6.00 3 -13 -3 14.50 6.60 3 -13 -3 -5.80 3.90 2 -13 -3 1.00 3.20 2 -13 -3 1.20 6.10 -2 13 3 3.10 4.80 1 -13 -3 60.59 10.60 -1 13 3 52.79 10.80 0 -13 -3 7.40 5.90 0 13 3 -3.00 4.70 -1 -13 -3 7.40 6.60 1 13 3 12.30 6.40 -2 -13 -3 12.70 6.50 2 13 3 16.00 5.70 -3 -13 -3 27.30 7.90 3 13 3 38.00 9.50 -4 -13 -3 14.10 10.90 4 13 3 9.20 6.50 5 13 3 23.40 8.50 6 -14 -3 15.40 12.80 5 -14 -3 93.99 17.70 4 -14 -3 72.39 13.60 3 -14 -3 32.10 8.30 2 -14 -3 40.30 5.80 2 -14 -3 27.90 6.10 2 -14 -3 56.39 10.70 -2 14 3 27.50 10.00 1 -14 -3 5.90 5.60 -1 14 3 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-15 4 2.50 4.80 3 -15 4 15.80 7.20 4 -15 4 91.19 16.80 4 -15 4 82.39 14.10 4 -15 4 119.29 18.80 5 -15 4 28.20 12.80 5 -15 4 48.70 11.20 6 -15 4 72.89 16.40 6 -15 4 55.39 17.10 5 14 -4 16.20 6.80 -5 -14 4 -2.30 5.60 4 14 -4 40.50 10.40 -4 -14 4 43.90 9.20 3 14 -4 17.70 6.50 -3 -14 4 23.00 7.80 2 14 -4 13.30 5.00 -2 -14 4 17.40 5.80 1 14 -4 6.60 3.90 -1 -14 4 -1.90 4.10 0 -14 4 23.00 6.10 1 -14 4 28.10 4.80 1 -14 4 36.50 6.80 1 -14 4 39.30 8.50 2 -14 4 29.20 8.30 2 -14 4 40.90 9.40 2 -14 4 24.30 6.20 3 -14 4 5.00 4.80 3 -14 4 3.60 5.10 4 -14 4 55.69 11.70 4 -14 4 61.69 11.30 4 -14 4 64.79 13.60 5 -14 4 -11.40 6.30 5 -14 4 17.70 11.10 5 -14 4 -0.60 6.80 6 -14 4 9.90 11.10 6 -14 4 2.80 6.50 6 13 -4 110.39 13.80 -6 -13 4 106.59 13.60 5 13 -4 2.60 5.20 -5 -13 4 -0.60 4.90 4 13 -4 85.79 11.40 -4 -13 4 74.29 11.30 3 13 -4 10.90 4.90 -3 -13 4 4.50 4.60 2 13 -4 33.20 7.30 -2 -13 4 43.10 7.50 1 13 -4 -1.60 3.30 -1 -13 4 -3.70 3.40 0 13 -4 10.10 5.40 0 -13 4 8.40 4.80 0 -13 4 14.60 2.30 0 -13 4 10.50 2.50 1 -13 4 17.00 5.90 1 -13 4 30.20 6.30 1 -13 4 26.10 4.80 2 -13 4 63.49 9.60 2 -13 4 82.59 12.80 2 -13 4 67.69 10.50 3 -13 4 3.90 4.60 3 -13 4 3.00 4.50 3 -13 4 9.60 5.70 4 -13 4 105.49 16.00 4 -13 4 102.69 13.80 4 -13 4 120.39 18.60 5 -13 4 11.70 9.90 5 -13 4 -4.70 4.90 6 -13 4 75.69 13.60 6 -13 4 53.09 11.40 7 -13 4 -3.80 5.30 8 -13 4 -4.90 7.20 7 12 -4 30.30 8.00 -7 -12 4 11.70 8.20 6 12 -4 -0.60 4.80 -6 -12 4 9.20 5.10 5 12 -4 5.70 4.30 -5 -12 4 13.00 5.80 4 12 -4 -0.20 3.70 -4 -12 4 4.40 4.60 3 12 -4 -0.60 3.40 -3 -12 4 7.60 4.60 2 12 -4 30.90 6.80 -2 -12 4 24.10 5.40 1 12 -4 -2.40 2.50 -1 -12 4 -0.50 2.60 0 12 -4 119.19 11.20 0 -12 4 116.19 6.80 0 -12 4 97.69 8.10 0 -12 4 88.99 10.70 1 -12 4 25.60 6.30 1 -12 4 14.50 6.30 1 -12 4 17.60 5.00 2 -12 4 85.49 11.10 2 -12 4 110.49 13.10 2 -12 4 93.79 13.00 3 -12 4 30.70 6.70 3 -12 4 31.00 9.30 3 -12 4 37.50 9.50 4 -12 4 6.70 9.00 4 -12 4 19.80 6.20 5 -12 4 25.60 11.50 5 -12 4 30.40 7.90 6 -12 4 12.20 11.20 6 -12 4 18.80 7.10 6 -12 4 19.20 7.60 7 -12 4 4.50 12.30 7 -12 4 -2.50 5.30 8 -12 4 46.00 10.60 9 -12 4 0.30 8.50 8 11 -4 13.10 6.30 -8 -11 4 16.60 9.40 7 11 -4 73.09 11.00 -7 -11 4 83.99 13.50 6 11 -4 5.50 4.50 -6 -11 4 3.50 4.60 5 11 -4 59.79 9.60 -5 -11 4 69.19 10.00 4 11 -4 27.70 6.00 -4 -11 4 21.20 5.40 3 11 -4 355.46 18.10 -3 -11 4 370.56 18.60 2 11 -4 448.86 21.00 -2 -11 4 465.15 20.30 1 11 -4 31.20 6.40 -1 -11 4 38.10 6.60 0 11 -4 413.16 20.00 0 -11 4 417.96 17.80 0 -11 4 415.26 15.20 0 -11 4 388.96 19.10 1 -11 4 -5.00 4.00 1 -11 4 2.20 3.20 1 -11 4 3.60 2.70 2 -11 4 52.09 8.80 2 -11 4 66.19 11.10 2 -11 4 48.70 8.90 3 -11 4 16.10 7.10 3 -11 4 3.20 3.50 4 -11 4 107.89 17.00 4 -11 4 135.09 12.60 5 -11 4 43.10 9.40 5 -11 4 26.30 7.10 5 -11 4 35.20 11.30 6 -11 4 92.49 14.20 6 -11 4 84.59 17.20 6 -11 4 82.59 13.30 7 -11 4 7.30 7.10 7 -11 4 1.20 5.10 7 -11 4 19.70 10.30 8 -11 4 14.80 7.00 9 -11 4 33.40 10.50 9 10 -4 -0.50 4.10 9 10 -4 15.90 7.70 -9 -10 4 12.90 10.40 8 10 -4 19.60 4.00 8 10 -4 38.30 8.90 -8 -10 4 36.30 9.30 7 10 -4 0.60 3.90 -7 -10 4 2.50 5.20 6 10 -4 20.80 6.10 -6 -10 4 26.20 6.40 5 10 -4 24.50 6.30 -5 -10 4 12.90 4.70 4 10 -4 6.30 3.40 -4 -10 4 3.10 3.30 3 10 -4 -0.30 2.30 -3 -10 4 -3.10 2.60 2 10 -4 16.70 4.70 -2 -10 4 20.50 4.60 1 10 -4 3.60 2.90 -1 -10 4 0.10 2.30 -1 -10 4 -0.50 2.00 -1 -10 4 -1.10 1.40 0 10 -4 66.79 8.70 0 -10 4 58.09 5.50 0 -10 4 63.39 8.20 0 -10 4 59.69 7.80 1 -10 4 96.59 11.90 1 -10 4 111.19 9.40 1 -10 4 94.49 8.80 2 -10 4 205.28 15.70 2 -10 4 204.58 13.80 2 -10 4 223.18 17.30 3 -10 4 -3.20 2.70 3 -10 4 3.50 5.80 4 -10 4 249.18 25.80 4 -10 4 236.28 16.50 5 -10 4 126.79 20.00 5 -10 4 101.79 14.20 5 -10 4 121.49 14.90 6 -10 4 424.46 32.20 6 -10 4 410.56 25.10 6 -10 4 397.06 23.70 7 -10 4 -14.00 7.50 7 -10 4 -2.10 4.40 7 -10 4 -3.20 7.20 8 -10 4 78.79 14.10 8 -10 4 62.89 16.20 9 -10 4 -1.80 6.90 10 -10 4 -1.70 6.30 9 9 -4 70.99 12.00 9 9 -4 75.79 9.70 -9 -9 4 58.49 12.10 8 9 -4 17.30 6.20 8 9 -4 31.40 6.50 -8 -9 4 29.20 9.40 7 9 -4 21.20 6.00 7 9 -4 19.20 4.50 -7 -9 4 15.60 6.60 6 9 -4 3.10 3.60 6 9 -4 1.60 2.10 -6 -9 4 10.80 4.70 5 9 -4 13.50 4.00 5 9 -4 13.80 2.50 -5 -9 4 6.90 4.20 4 9 -4 7.60 3.50 -4 -9 4 5.80 3.40 3 9 -4 84.19 7.90 -3 -9 4 83.99 7.70 2 9 -4 19.20 4.70 -2 -9 4 13.40 3.50 1 9 -4 171.68 11.10 -1 -9 4 184.68 10.90 -1 -9 4 179.18 8.30 -1 -9 4 197.28 9.70 0 9 -4 26.60 5.30 0 -9 4 28.90 5.50 0 -9 4 32.40 5.90 0 -9 4 24.80 4.50 1 -9 4 46.00 7.20 1 -9 4 48.80 8.80 1 -9 4 53.19 7.80 2 -9 4 5.80 4.70 2 -9 4 15.30 5.10 2 -9 4 4.10 3.40 3 -9 4 233.78 19.10 3 -9 4 214.78 14.30 4 -9 4 143.29 18.20 4 -9 4 134.29 11.90 5 -9 4 221.78 22.50 5 -9 4 233.38 16.50 5 -9 4 263.67 18.40 6 -9 4 194.98 25.60 6 -9 4 136.89 15.90 6 -9 4 170.28 14.90 7 -9 4 44.90 9.70 7 -9 4 27.30 8.10 7 -9 4 54.59 15.90 8 -9 4 38.60 11.10 8 -9 4 38.80 12.70 8 -9 4 34.60 10.20 9 -9 4 -1.20 6.20 10 -9 4 75.49 15.70 10 8 -4 -5.50 8.50 10 8 -4 3.30 5.60 9 8 -4 -1.20 6.00 9 8 -4 -3.60 4.60 -9 -8 4 6.00 8.20 8 8 -4 4.00 4.50 8 8 -4 3.80 4.00 -8 -8 4 -1.90 5.70 7 8 -4 -2.00 3.20 7 8 -4 0.00 3.70 -7 -8 4 3.90 4.40 6 8 -4 8.20 3.70 6 8 -4 2.20 2.80 -6 -8 4 8.50 5.10 5 8 -4 273.67 15.10 5 8 -4 272.77 12.00 -5 -8 4 326.97 14.70 -5 -8 4 274.17 15.00 4 8 -4 37.20 6.20 -4 -8 4 33.20 4.80 -4 -8 4 33.30 5.60 3 8 -4 315.17 10.60 3 8 -4 306.97 14.20 -3 -8 4 277.87 13.80 -3 -8 4 302.77 11.40 2 8 -4 30.60 5.20 -2 -8 4 39.10 4.40 -2 -8 4 34.50 5.30 -1 -8 4 1.70 2.30 -1 -8 4 1.00 1.70 0 8 -4 1.20 2.20 0 -8 4 4.10 2.20 0 -8 4 8.30 3.40 0 -8 4 2.00 1.50 1 -8 4 142.29 9.80 1 -8 4 153.38 11.10 1 -8 4 158.78 12.00 2 -8 4 58.39 9.70 2 -8 4 71.09 8.70 3 -8 4 221.38 13.80 3 -8 4 195.58 17.20 4 -8 4 83.99 11.30 4 -8 4 87.19 11.10 4 -8 4 58.69 12.70 5 -8 4 47.00 11.70 5 -8 4 49.50 8.80 5 -8 4 58.69 10.50 6 -8 4 440.76 23.70 6 -8 4 425.26 23.90 6 -8 4 379.06 30.20 7 -8 4 48.00 14.00 7 -8 4 60.19 11.50 8 -8 4 91.79 18.10 8 -8 4 91.49 14.60 9 -8 4 40.50 11.80 10 -8 4 234.18 38.40 10 7 -4 26.50 11.70 10 7 -4 36.10 8.90 -10 -7 4 36.10 10.70 9 7 -4 17.40 8.20 9 7 -4 34.70 8.70 -9 -7 4 56.79 11.10 8 7 -4 108.09 12.80 8 7 -4 84.99 12.40 -8 -7 4 108.19 13.20 7 7 -4 13.80 4.90 7 7 -4 12.70 5.20 -7 -7 4 19.10 6.10 -7 -7 4 24.40 7.60 6 7 -4 106.69 10.00 6 7 -4 121.69 10.40 -6 -7 4 97.89 10.90 -6 -7 4 125.69 12.10 5 7 -4 22.00 4.90 5 7 -4 12.90 3.80 -5 -7 4 24.50 5.00 -5 -7 4 23.70 5.70 4 7 -4 34.20 4.70 4 7 -4 39.90 6.10 -4 -7 4 34.20 5.80 -4 -7 4 31.90 6.10 3 7 -4 213.28 11.20 -3 -7 4 204.38 10.70 -3 -7 4 215.38 11.00 2 7 -4 2.40 1.80 2 7 -4 1.40 1.50 -2 -7 4 0.80 2.20 -2 -7 4 0.60 1.20 1 7 -4 591.34 19.30 -1 -7 4 581.54 17.60 -1 -7 4 569.74 18.80 0 7 -4 20.90 4.10 0 -7 4 24.50 4.30 0 -7 4 32.50 4.70 1 -7 4 -0.70 2.40 1 -7 4 2.10 3.20 1 -7 4 3.80 2.00 2 -7 4 14.70 3.80 2 -7 4 17.80 5.90 3 -7 4 76.89 9.20 3 -7 4 98.49 14.00 4 -7 4 121.09 11.30 4 -7 4 167.48 16.40 4 -7 4 167.18 12.10 5 -7 4 87.29 16.40 5 -7 4 69.89 11.00 6 -7 4 60.79 10.60 6 -7 4 127.99 20.60 7 -7 4 1.20 4.10 7 -7 4 11.70 8.60 8 -7 4 32.10 12.30 8 -7 4 28.30 8.30 9 -7 4 144.49 34.70 9 -7 4 83.19 13.90 10 -7 4 5.30 5.90 11 -7 4 9.70 9.10 10 6 -4 12.30 9.30 10 6 -4 21.50 7.30 -10 -6 4 13.90 8.60 9 6 -4 -3.60 6.60 9 6 -4 8.50 5.30 -9 -6 4 5.70 6.40 8 6 -4 43.80 7.80 -8 -6 4 55.69 10.40 -8 -6 4 25.60 7.70 7 6 -4 -4.60 4.40 7 6 -4 3.40 3.20 -7 -6 4 3.70 4.80 -7 -6 4 -2.50 3.10 6 6 -4 6.10 4.60 6 6 -4 10.40 4.50 -6 -6 4 13.60 4.50 -6 -6 4 5.30 5.00 5 6 -4 4.00 3.10 5 6 -4 2.40 2.90 -5 -6 4 5.30 3.00 -5 -6 4 2.60 4.30 4 6 -4 2.90 2.50 4 6 -4 1.30 2.50 -4 -6 4 0.00 1.70 -4 -6 4 -3.20 3.10 3 6 -4 93.19 6.20 3 6 -4 84.19 6.40 -3 -6 4 91.29 6.80 -3 -6 4 90.19 8.30 2 6 -4 149.29 7.90 2 6 -4 155.58 8.20 -2 -6 4 158.18 8.80 -2 -6 4 161.08 8.10 1 6 -4 331.37 12.50 -1 -6 4 339.37 12.30 -1 -6 4 334.57 12.20 0 6 -4 26.50 4.00 0 -6 4 33.00 4.30 0 -6 4 37.10 5.10 1 -6 4 30.80 5.70 1 -6 4 49.20 5.90 2 -6 4 -3.50 3.00 2 -6 4 -2.80 1.40 3 -6 4 252.77 17.90 3 -6 4 249.78 14.10 4 -6 4 18.70 5.50 4 -6 4 22.10 7.90 5 -6 4 393.06 26.80 5 -6 4 360.26 19.80 6 -6 4 103.49 18.70 6 -6 4 112.19 13.80 7 -6 4 442.06 24.80 7 -6 4 466.35 33.70 8 -6 4 35.80 9.30 8 -6 4 42.90 14.30 9 -6 4 137.79 18.30 9 -6 4 136.39 23.10 10 -6 4 17.50 7.60 11 -6 4 17.70 9.30 11 5 -4 -32.50 11.70 11 5 -4 5.30 6.60 10 5 -4 -1.00 9.30 10 5 -4 6.30 6.30 9 5 -4 -2.90 8.30 -9 -5 4 1.50 5.60 -9 -5 4 17.20 9.50 8 5 -4 1.60 5.80 8 5 -4 0.60 3.20 -8 -5 4 1.70 4.50 -8 -5 4 -0.40 4.60 7 5 -4 30.90 6.60 7 5 -4 35.30 9.00 -7 -5 4 53.39 11.30 6 5 -4 42.70 7.30 6 5 -4 32.70 7.40 -6 -5 4 31.90 8.70 -6 -5 4 30.90 6.60 5 5 -4 4.80 4.40 5 5 -4 1.50 2.50 -5 -5 4 0.60 2.00 4 5 -4 59.69 5.60 4 5 -4 54.59 7.10 -4 -5 4 51.79 6.10 -4 -5 4 43.40 7.80 3 5 -4 4.90 2.10 3 5 -4 3.50 2.30 -3 -5 4 3.60 3.90 -3 -5 4 1.50 2.20 2 5 -4 4.70 1.90 2 5 -4 6.80 2.70 -2 -5 4 4.60 3.00 -2 -5 4 5.40 2.20 1 5 -4 13.00 2.50 1 5 -4 8.20 3.80 -1 -5 4 13.10 2.60 -1 -5 4 10.00 2.50 0 5 -4 544.25 16.30 0 -5 4 556.84 18.20 0 -5 4 541.45 16.20 1 -5 4 120.49 9.40 1 -5 4 144.89 7.90 2 -5 4 827.32 30.10 3 -5 4 173.58 14.40 3 -5 4 153.98 10.50 4 -5 4 7.70 5.90 4 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56.49 8.90 3 -9 7 39.00 9.30 3 -9 7 48.40 10.90 3 -9 7 43.50 8.20 4 -9 7 69.89 14.30 4 -9 7 68.09 10.50 4 -9 7 57.59 9.30 5 -9 7 2.90 3.90 5 -9 7 -6.70 3.20 5 -9 7 4.20 7.50 6 -9 7 9.10 9.20 6 -9 7 3.10 5.50 6 -9 7 4.80 5.10 7 -9 7 4.00 5.60 7 -9 7 -6.40 8.20 8 -9 7 18.60 12.10 8 -9 7 15.70 7.70 9 -9 7 14.50 9.60 10 -9 7 8.80 8.20 10 8 -7 5.50 5.50 10 8 -7 -3.60 9.80 9 8 -7 3.40 4.70 9 8 -7 5.10 7.50 -9 -8 7 11.50 6.70 -9 -8 7 1.10 5.70 8 8 -7 -1.40 5.50 8 8 -7 12.30 4.20 -8 -8 7 9.60 6.00 -8 -8 7 7.80 5.50 7 8 -7 22.50 5.70 7 8 -7 18.00 5.60 -7 -8 7 22.40 5.60 -7 -8 7 29.20 7.90 6 8 -7 75.99 9.00 6 8 -7 77.19 7.50 -6 -8 7 78.39 11.80 -6 -8 7 64.09 8.30 5 8 -7 2.70 2.80 5 8 -7 2.60 2.30 -5 -8 7 3.50 3.00 -5 -8 7 18.40 8.20 4 8 -7 60.19 6.40 4 8 -7 59.09 6.60 -4 -8 7 56.99 9.00 -4 -8 7 56.79 6.60 3 8 -7 24.90 4.50 3 8 -7 17.20 3.50 -3 -8 7 22.20 4.00 -3 -8 7 26.30 5.80 2 8 -7 53.69 7.20 2 8 -7 54.19 5.00 -2 -8 7 57.69 7.40 -2 -8 7 56.39 4.80 -1 -8 7 47.30 6.40 -1 -8 7 40.30 4.90 0 -8 7 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5.30 -7 -5 8 -14.50 4.80 6 5 -8 78.59 11.70 6 5 -8 61.39 7.50 -6 -5 8 79.59 14.00 5 5 -8 41.90 8.30 5 5 -8 42.30 5.20 -5 -5 8 42.10 5.60 -5 -5 8 45.30 9.90 4 5 -8 4.90 1.80 4 5 -8 1.70 3.20 -4 -5 8 5.90 2.30 -4 -5 8 13.20 6.30 3 5 -8 291.97 14.80 3 5 -8 285.97 8.50 -3 -5 8 264.97 8.60 2 5 -8 68.39 7.00 -2 -5 8 80.69 8.50 1 5 -8 121.19 9.50 -1 -5 8 113.69 3.50 -1 -5 8 115.29 3.70 -1 -5 8 107.79 9.00 0 5 -8 115.59 10.20 0 -5 8 114.29 5.50 0 -5 8 111.39 9.40 0 -5 8 110.79 5.70 1 -5 8 1.20 2.10 1 -5 8 2.10 2.50 2 -5 8 75.29 6.80 2 -5 8 71.89 10.80 3 -5 8 35.80 8.20 3 -5 8 27.60 5.80 4 -5 8 75.89 9.50 4 -5 8 93.69 13.40 5 -5 8 16.60 7.90 5 -5 8 13.40 5.90 6 -5 8 42.70 12.50 6 -5 8 25.40 7.30 7 -5 8 7.30 5.60 7 -5 8 15.20 10.20 8 -5 8 56.69 11.00 9 -5 8 4.90 6.00 10 -5 8 -6.40 5.70 11 4 -8 15.90 7.00 -11 -4 8 4.10 10.10 10 4 -8 -13.30 7.80 10 4 -8 6.20 4.50 -10 -4 8 3.40 7.60 9 4 -8 135.09 12.30 9 4 -8 91.09 16.00 -9 -4 8 100.49 30.20 8 4 -8 4.00 7.10 8 4 -8 1.90 3.40 -8 -4 8 18.10 9.20 7 4 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12.90 2 -14 9 68.99 11.30 3 -14 9 27.40 7.60 3 -14 9 11.00 5.50 3 -14 9 19.60 6.60 3 -14 9 28.70 10.70 4 -14 9 11.80 7.60 4 -14 9 21.40 10.10 4 -14 9 18.70 8.10 4 -14 9 7.30 6.60 5 -14 9 55.59 12.00 5 -14 9 39.50 12.30 5 -14 9 36.70 9.90 5 -14 9 62.29 16.10 6 -14 9 25.70 12.90 6 -14 9 15.00 8.10 6 13 -9 24.30 5.70 -6 -13 9 8.10 5.50 5 13 -9 40.90 6.50 -5 -13 9 50.29 7.30 4 13 -9 14.10 4.40 -4 -13 9 7.60 3.50 -3 -13 9 209.88 12.50 -2 -13 9 5.80 3.20 -2 -13 9 4.90 3.20 -2 -13 9 -0.70 3.10 -1 -13 9 137.49 11.60 -1 -13 9 126.59 10.00 -1 -13 9 139.79 17.30 0 -13 9 44.40 8.50 0 -13 9 42.00 7.10 0 -13 9 52.59 8.20 1 -13 9 75.89 10.50 1 -13 9 67.89 12.00 2 -13 9 6.20 4.00 2 -13 9 1.00 3.80 2 -13 9 9.60 6.20 3 -13 9 159.08 14.10 3 -13 9 184.68 16.90 3 -13 9 186.18 14.90 3 -13 9 175.78 22.30 4 -13 9 88.19 16.60 4 -13 9 95.59 13.40 4 -13 9 88.99 16.20 5 -13 9 50.29 10.60 5 -13 9 40.30 12.20 5 -13 9 47.50 15.30 5 -13 9 78.59 15.00 6 -13 9 42.50 11.40 6 -13 9 32.90 11.30 6 -13 9 48.00 13.90 6 -13 9 27.60 8.30 7 -13 9 8.10 9.70 7 -13 9 11.90 7.00 8 -13 9 16.30 12.70 8 -13 9 3.30 8.50 7 12 -9 5.00 4.70 6 12 -9 -2.70 3.70 -6 -12 9 9.20 4.40 5 12 -9 62.39 7.80 -5 -12 9 65.99 8.20 4 12 -9 16.90 4.10 -4 -12 9 15.40 3.40 -4 -12 9 14.00 4.50 3 12 -9 32.70 5.60 -3 -12 9 36.60 6.10 -3 -12 9 39.10 6.00 -2 -12 9 47.40 7.30 -2 -12 9 29.60 5.20 -1 -12 9 8.00 2.80 -1 -12 9 0.30 2.90 -1 -12 9 4.20 3.80 0 -12 9 59.19 9.70 0 -12 9 51.99 8.30 0 -12 9 63.69 8.30 1 -12 9 139.99 10.90 1 -12 9 157.38 13.20 1 -12 9 137.19 14.70 2 -12 9 2.90 3.40 2 -12 9 4.50 3.00 3 -12 9 48.30 8.10 3 -12 9 47.60 9.90 3 -12 9 40.10 8.60 3 -12 9 31.60 10.90 4 -12 9 8.90 7.20 4 -12 9 -1.00 5.20 4 -12 9 -2.00 4.00 4 -12 9 7.70 4.80 5 -12 9 28.10 10.30 5 -12 9 22.20 7.30 5 -12 9 19.00 9.30 5 -12 9 27.80 7.40 6 -12 9 -2.50 6.40 6 -12 9 -3.80 5.70 6 -12 9 -4.40 8.40 6 -12 9 -1.00 6.40 7 -12 9 14.20 10.80 7 -12 9 3.40 6.20 8 -12 9 1.20 10.80 8 -12 9 5.70 8.60 8 11 -9 90.19 10.60 8 11 -9 66.19 8.70 -8 -11 9 67.29 10.50 7 11 -9 29.70 6.10 7 11 -9 36.60 6.60 -7 -11 9 41.40 7.10 6 11 -9 21.80 5.20 6 11 -9 20.60 5.00 -6 -11 9 16.30 5.20 -6 -11 9 21.20 5.20 5 11 -9 52.59 6.60 5 11 -9 58.69 7.40 -5 -11 9 57.49 7.30 -5 -11 9 65.19 8.40 4 11 -9 23.30 4.50 -4 -11 9 14.60 3.90 -4 -11 9 26.10 6.10 -3 -11 9 72.99 6.50 -3 -11 9 68.69 9.20 -2 -11 9 15.90 5.10 -1 -11 9 190.68 10.50 -1 -11 9 203.08 13.40 0 -11 9 38.60 7.20 0 -11 9 36.70 5.70 1 -11 9 129.79 13.70 1 -11 9 120.29 9.50 1 -11 9 109.69 11.10 2 -11 9 7.90 5.00 2 -11 9 14.50 7.30 2 -11 9 18.90 6.40 2 -11 9 20.60 5.30 3 -11 9 19.80 5.50 3 -11 9 24.50 8.00 3 -11 9 22.60 6.10 3 -11 9 36.90 9.70 4 -11 9 82.49 11.70 4 -11 9 102.39 13.00 4 -11 9 64.89 14.00 4 -11 9 82.49 15.00 5 -11 9 56.69 9.80 5 -11 9 38.10 11.80 5 -11 9 48.80 9.70 5 -11 9 38.70 11.90 6 -11 9 120.49 15.20 6 -11 9 96.69 21.60 6 -11 9 110.79 19.20 6 -11 9 108.49 14.80 7 -11 9 61.89 11.20 7 -11 9 72.19 17.00 7 -11 9 52.59 11.10 8 -11 9 28.10 9.20 8 -11 9 35.80 12.00 9 -11 9 -5.10 11.10 9 -11 9 -2.20 6.90 8 10 -9 36.00 7.10 8 10 -9 42.10 8.10 -8 -10 9 47.10 8.40 -8 -10 9 50.99 8.60 7 10 -9 0.00 3.70 7 10 -9 -1.10 2.70 -7 -10 9 -4.20 4.00 -7 -10 9 4.20 5.40 6 10 -9 23.20 5.40 6 10 -9 18.50 4.40 -6 -10 9 18.00 4.60 -6 -10 9 17.80 6.70 5 10 -9 25.80 4.90 5 10 -9 26.10 5.50 -5 -10 9 30.20 5.10 -5 -10 9 34.60 7.70 4 10 -9 102.09 9.10 4 10 -9 92.99 7.10 -4 -10 9 84.19 6.60 -4 -10 9 112.49 13.30 3 10 -9 62.79 5.60 3 10 -9 76.09 9.30 -3 -10 9 68.99 9.60 -3 -10 9 59.49 6.30 -2 -10 9 112.69 7.20 -1 -10 9 392.26 14.90 -1 -10 9 392.76 18.70 0 -10 9 19.90 5.50 0 -10 9 28.30 4.90 1 -10 9 456.35 23.00 1 -10 9 504.35 19.60 2 -10 9 171.78 15.10 2 -10 9 170.08 16.10 2 -10 9 154.98 11.70 2 -10 9 174.38 12.60 3 -10 9 32.10 8.80 3 -10 9 52.49 8.30 3 -10 9 51.39 8.90 3 -10 9 38.20 10.10 4 -10 9 1.10 6.40 4 -10 9 -2.00 3.90 4 -10 9 -0.30 4.40 4 -10 9 1.90 3.40 5 -10 9 26.30 7.10 5 -10 9 21.90 7.10 5 -10 9 10.70 6.50 5 -10 9 24.00 8.90 6 -10 9 132.89 16.20 6 -10 9 131.39 21.00 6 -10 9 146.69 17.00 6 -10 9 133.09 20.20 7 -10 9 7.80 9.30 7 -10 9 0.50 7.30 7 -10 9 21.80 7.80 7 -10 9 9.40 5.80 8 -10 9 8.30 6.60 9 -10 9 9.10 7.70 9 9 -9 7.60 5.30 9 9 -9 6.40 7.40 -9 -9 9 0.70 6.50 8 9 -9 68.49 10.10 8 9 -9 58.69 8.30 -8 -9 9 88.39 13.20 7 9 -9 -2.30 3.50 7 9 -9 2.90 3.00 -7 -9 9 -3.10 5.40 -7 -9 9 -2.60 3.10 6 9 -9 138.59 11.40 6 9 -9 125.49 8.80 -6 -9 9 127.99 9.50 -6 -9 9 137.09 14.60 5 9 -9 59.29 6.60 5 9 -9 63.69 8.40 -5 -9 9 59.99 6.80 -5 -9 9 65.29 11.00 4 9 -9 80.69 6.00 4 9 -9 73.89 9.10 -4 -9 9 79.69 6.20 -4 -9 9 74.69 11.00 3 9 -9 251.27 14.90 3 9 -9 247.28 10.20 -3 -9 9 243.48 10.00 2 9 -9 1.40 2.70 -2 -9 9 8.10 4.50 -2 -9 9 4.50 2.00 -1 -9 9 293.47 15.70 -1 -9 9 262.77 10.90 0 -9 9 99.79 7.10 0 -9 9 116.99 10.20 1 -9 9 61.89 7.50 1 -9 9 61.09 9.90 1 -9 9 69.49 7.90 2 -9 9 297.67 15.30 2 -9 9 310.97 16.20 2 -9 9 316.97 20.10 3 -9 9 83.79 10.50 3 -9 9 73.79 9.90 3 -9 9 101.19 24.30 3 -9 9 87.69 14.30 4 -9 9 2.60 3.50 4 -9 9 -4.40 4.50 4 -9 9 4.80 3.60 4 -9 9 5.80 5.70 5 -9 9 -0.80 6.40 5 -9 9 4.10 3.80 5 -9 9 19.30 9.30 6 -9 9 30.60 9.90 6 -9 9 8.90 9.70 6 -9 9 28.80 7.90 7 -9 9 27.90 12.50 7 -9 9 2.30 5.00 8 -9 9 9.60 6.20 9 -9 9 61.09 12.90 10 -9 9 21.10 11.00 9 8 -9 6.40 4.60 9 8 -9 27.10 9.90 -9 -8 9 22.70 7.60 8 8 -9 7.80 3.60 8 8 -9 -8.30 4.40 -8 -8 9 9.20 7.10 7 8 -9 34.70 6.20 7 8 -9 27.00 7.00 -7 -8 9 43.60 9.90 -7 -8 9 36.00 6.70 6 8 -9 339.27 14.70 6 8 -9 323.67 18.30 -6 -8 9 322.77 14.90 -6 -8 9 339.47 22.30 5 8 -9 346.97 17.80 5 8 -9 363.26 14.00 -5 -8 9 356.06 14.20 -5 -8 9 373.36 23.00 4 8 -9 282.67 15.50 4 8 -9 298.37 11.30 -4 -8 9 301.57 11.50 -4 -8 9 295.67 19.10 3 8 -9 1.30 2.40 3 8 -9 0.40 1.30 -3 -8 9 3.50 4.30 -3 -8 9 1.70 1.60 2 8 -9 121.39 10.40 -2 -8 9 137.79 11.10 1 8 -9 70.29 9.70 -1 -8 9 66.59 4.70 -1 -8 9 79.79 8.20 0 -8 9 6.70 3.00 0 -8 9 4.00 1.80 1 -8 9 416.26 16.40 1 -8 9 408.06 21.00 1 -8 9 416.26 16.50 2 -8 9 140.69 9.90 2 -8 9 162.98 14.20 2 -8 9 129.09 9.90 3 -8 9 401.76 18.80 3 -8 9 457.25 26.50 3 -8 9 419.56 26.60 3 -8 9 470.35 20.70 4 -8 9 14.80 7.10 4 -8 9 20.40 8.60 4 -8 9 5.50 4.80 5 -8 9 768.52 31.70 5 -8 9 791.82 41.90 5 -8 9 728.03 39.80 6 -8 9 13.10 8.90 6 -8 9 8.60 5.50 7 -8 9 363.76 23.60 8 -8 9 77.79 13.70 9 -8 9 89.29 15.00 10 -8 9 -15.00 6.50 10 7 -9 22.90 13.70 10 7 -9 41.10 8.10 -10 -7 9 32.00 11.60 9 7 -9 -6.20 6.60 9 7 -9 0.30 3.60 -9 -7 9 0.90 7.40 8 7 -9 13.80 4.00 8 7 -9 7.70 5.90 -8 -7 9 31.60 9.10 7 7 -9 11.50 3.50 -7 -7 9 -3.00 5.30 6 7 -9 54.29 9.10 6 7 -9 59.59 6.80 -6 -7 9 46.10 6.70 -6 -7 9 61.09 11.80 5 7 -9 174.58 8.80 5 7 -9 164.38 12.40 -5 -7 9 169.68 9.20 -5 -7 9 153.28 17.50 4 7 -9 23.80 5.30 4 7 -9 18.10 2.80 -4 -7 9 16.10 6.60 -4 -7 9 18.10 3.20 3 7 -9 24.30 5.20 3 7 -9 26.20 2.50 -3 -7 9 31.90 3.00 -3 -7 9 19.50 6.30 2 7 -9 25.70 5.80 -2 -7 9 31.00 2.50 -2 -7 9 32.50 6.40 1 7 -9 291.37 16.50 -1 -7 9 236.88 8.20 -1 -7 9 253.97 14.80 0 -7 9 198.48 8.60 0 -7 9 197.68 8.90 0 -7 9 197.18 13.00 1 -7 9 2.00 1.90 1 -7 9 3.80 2.00 1 -7 9 2.70 2.30 2 -7 9 273.37 13.60 2 -7 9 241.78 17.10 3 -7 9 34.20 9.10 3 -7 9 20.50 5.60 4 -7 9 54.69 9.00 4 -7 9 68.49 13.70 4 -7 9 49.20 11.50 5 -7 9 105.89 12.70 5 -7 9 96.69 15.80 5 -7 9 114.09 17.90 6 -7 9 4.80 5.40 6 -7 9 25.70 10.90 7 -7 9 12.30 8.30 7 -7 9 8.70 4.90 8 -7 9 41.20 14.10 8 -7 9 25.80 8.80 9 -7 9 -7.40 5.20 10 -7 9 -0.60 7.00 10 6 -9 18.90 11.90 10 6 -9 12.10 5.10 -10 -6 9 8.70 8.40 9 6 -9 4.40 6.50 9 6 -9 12.80 5.30 8 6 -9 -5.10 5.10 8 6 -9 6.00 3.70 -8 -6 9 -1.30 6.30 7 6 -9 8.10 3.70 7 6 -9 30.20 7.70 -7 -6 9 22.20 8.20 6 6 -9 126.29 12.70 6 6 -9 121.59 8.30 -6 -6 9 129.29 17.00 5 6 -9 0.20 3.00 5 6 -9 1.70 2.10 -5 -6 9 3.30 5.80 4 6 -9 93.69 5.00 4 6 -9 82.79 9.80 -4 -6 9 91.89 12.40 -4 -6 9 89.29 7.20 3 6 -9 51.89 2.60 3 6 -9 58.49 8.10 -3 -6 9 47.50 8.60 2 6 -9 112.99 9.40 -2 -6 9 109.29 10.20 1 6 -9 44.30 7.30 -1 -6 9 50.09 2.80 -1 -6 9 56.89 8.20 -1 -6 9 47.00 2.50 0 6 -9 180.28 13.60 0 -6 9 213.28 8.30 0 -6 9 165.08 8.60 0 -6 9 196.18 12.90 1 -6 9 6.30 2.80 1 -6 9 15.10 4.90 2 -6 9 123.59 10.40 2 -6 9 120.69 12.10 3 -6 9 43.10 9.50 3 -6 9 78.59 9.40 4 -6 9 102.79 24.80 4 -6 9 100.79 9.80 4 -6 9 111.09 16.20 5 -6 9 -2.70 3.70 5 -6 9 9.20 8.20 5 -6 9 2.00 4.40 6 -6 9 304.57 26.60 6 -6 9 311.27 19.70 7 -6 9 1.80 5.10 7 -6 9 -6.20 7.30 8 -6 9 32.80 11.70 8 -6 9 34.40 9.20 9 -6 9 131.79 18.40 10 -6 9 -5.80 6.50 11 5 -9 26.30 7.10 -11 -5 9 41.10 13.40 10 5 -9 11.30 6.20 10 5 -9 15.90 10.60 -10 -5 9 -0.90 8.50 9 5 -9 41.80 11.50 9 5 -9 35.80 7.00 -9 -5 9 42.50 13.00 8 5 -9 112.79 15.90 8 5 -9 114.29 10.40 -8 -5 9 152.18 20.90 7 5 -9 -0.20 4.30 7 5 -9 6.90 3.60 -7 -5 9 23.50 9.30 6 5 -9 275.97 19.00 6 5 -9 252.17 12.70 -6 -5 9 255.27 22.00 5 5 -9 1.80 3.90 5 5 -9 0.30 1.70 -5 -5 9 1.70 5.10 4 5 -9 30.10 3.30 4 5 -9 29.40 6.20 -4 -5 9 30.40 8.40 3 5 -9 1.70 2.70 -3 -5 9 -0.50 3.40 2 5 -9 36.00 6.20 -2 -5 9 37.10 6.70 1 5 -9 9.10 3.80 -1 -5 9 8.10 4.30 0 5 -9 59.89 8.80 0 -5 9 73.89 4.60 0 -5 9 66.89 4.30 0 -5 9 69.29 8.70 1 -5 9 -0.90 2.30 1 -5 9 -0.30 1.80 2 -5 9 5.00 2.80 2 -5 9 8.10 4.30 3 -5 9 47.70 10.10 3 -5 9 55.19 7.60 4 -5 9 49.50 7.90 4 -5 9 44.70 10.20 5 -5 9 331.37 25.10 5 -5 9 325.07 18.70 5 -5 9 338.57 24.60 6 -5 9 19.50 10.10 6 -5 9 29.40 8.10 7 -5 9 83.49 17.20 8 -5 9 166.28 16.30 8 -5 9 192.58 26.50 9 -5 9 -1.60 5.40 10 -5 9 21.60 9.80 -11 -4 9 71.39 17.00 10 4 -9 6.90 5.90 10 4 -9 -5.10 8.30 -10 -4 9 4.50 8.90 9 4 -9 181.38 21.90 9 4 -9 178.38 13.90 -9 -4 9 167.18 23.00 8 4 -9 118.39 10.70 8 4 -9 160.58 19.70 -8 -4 9 113.19 18.60 7 4 -9 64.79 8.30 7 4 -9 82.69 13.30 -7 -4 9 64.79 12.80 6 4 -9 370.56 15.70 6 4 -9 381.66 23.00 -6 -4 9 411.26 27.50 5 4 -9 5.40 4.40 5 4 -9 1.60 1.70 -5 -4 9 3.10 5.90 4 4 -9 123.29 11.10 4 4 -9 122.69 6.10 -4 -4 9 142.39 14.10 3 4 -9 8.50 3.80 3 4 -9 19.00 1.50 3 4 -9 16.50 1.40 -3 -4 9 9.80 5.60 2 4 -9 1148.99 35.30 -2 -4 9 1137.29 37.40 1 4 -9 10.30 3.90 0 4 -9 2627.04 68.19 0 -4 9 2659.53 66.79 0 -4 9 2666.03 56.09 -1 4 -9 238.98 15.70 -1 4 -9 198.28 9.50 1 -4 9 191.18 13.30 1 -4 9 199.98 9.30 -2 4 -9 650.43 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10 23.10 8.30 4 -8 10 11.30 5.20 5 -8 10 140.99 19.80 5 -8 10 124.29 20.20 5 -8 10 151.98 13.80 6 -8 10 16.40 7.10 6 -8 10 24.00 9.80 6 -8 10 20.70 9.40 7 -8 10 108.39 15.40 7 -8 10 145.79 23.60 7 -8 10 153.18 24.60 8 -8 10 -1.20 5.10 8 -8 10 -1.20 7.60 9 -8 10 30.90 13.20 9 -8 10 9.80 8.50 10 -8 10 41.70 10.70 10 -8 10 31.70 24.80 10 7 -10 14.40 10.00 10 7 -10 8.40 6.10 -10 -7 10 19.30 10.00 9 7 -10 93.89 14.70 9 7 -10 72.19 9.60 -9 -7 10 100.59 24.10 8 7 -10 16.10 3.80 8 7 -10 7.30 6.30 -8 -7 10 12.10 6.80 7 7 -10 76.19 11.50 7 7 -10 67.59 7.70 -7 -7 10 91.09 14.90 6 7 -10 59.29 5.50 6 7 -10 60.19 10.10 -6 -7 10 67.99 13.20 5 7 -10 45.20 4.10 5 7 -10 56.49 8.90 -5 -7 10 48.00 11.10 4 7 -10 88.69 9.10 4 7 -10 65.99 3.70 -4 -7 10 65.99 10.90 3 7 -10 0.60 2.80 -3 -7 10 5.80 4.90 2 7 -10 147.59 11.60 -2 -7 10 150.08 12.20 1 7 -10 22.20 5.80 -1 -7 10 17.50 4.70 -1 -7 10 23.20 2.30 -1 -7 10 20.70 2.30 0 -7 10 138.99 6.90 0 -7 10 129.89 6.90 0 -7 10 140.29 11.60 1 -7 10 82.39 6.60 1 -7 10 76.79 10.70 1 -7 10 67.59 5.90 2 -7 10 109.79 11.60 2 -7 10 95.49 8.10 3 -7 10 2.70 4.00 3 -7 10 0.80 3.30 4 -7 10 108.79 16.50 4 -7 10 102.09 16.30 4 -7 10 110.29 10.70 5 -7 10 0.20 4.40 5 -7 10 -4.00 5.30 5 -7 10 0.20 4.20 6 -7 10 4.40 7.30 6 -7 10 2.90 4.40 7 -7 10 -1.00 9.30 7 -7 10 3.00 6.00 7 -7 10 1.90 3.80 8 -7 10 58.39 11.60 8 -7 10 62.69 14.30 8 -7 10 71.19 15.60 9 -7 10 28.40 13.20 9 -7 10 10.90 7.90 10 -7 10 33.30 15.60 10 -7 10 14.20 9.70 10 6 -10 5.70 10.40 10 6 -10 19.50 6.10 -10 -6 10 25.10 11.10 9 6 -10 -9.90 6.60 9 6 -10 7.20 3.80 -9 -6 10 7.20 7.60 8 6 -10 2.10 3.20 8 6 -10 7.00 6.00 -8 -6 10 -2.20 6.00 7 6 -10 114.99 9.00 7 6 -10 113.09 15.40 -7 -6 10 153.98 20.60 6 6 -10 500.65 17.60 6 6 -10 475.45 25.10 -6 -6 10 528.15 31.10 5 6 -10 438.36 22.20 5 6 -10 441.86 14.10 -5 -6 10 415.86 26.30 4 6 -10 156.78 5.70 4 6 -10 170.68 12.80 -4 -6 10 146.99 14.70 3 6 -10 759.42 28.40 -3 -6 10 769.62 31.10 2 6 -10 38.10 6.90 -2 -6 10 43.60 7.90 1 6 -10 273.97 16.30 -1 -6 10 293.67 16.30 0 6 -10 79.99 11.20 0 -6 10 87.19 5.00 0 -6 10 77.19 10.00 1 -6 10 83.89 6.40 1 -6 10 88.79 11.40 2 -6 10 246.78 17.50 3 -6 10 0.50 4.10 3 -6 10 6.40 3.00 4 -6 10 1257.17 39.90 4 -6 10 1259.47 50.09 5 -6 10 281.67 18.00 5 -6 10 325.87 24.90 5 -6 10 345.27 25.40 6 -6 10 1114.69 51.69 6 -6 10 1119.59 52.49 6 -6 10 1114.19 40.90 7 -6 10 -0.20 5.20 7 -6 10 -2.90 4.60 7 -6 10 6.80 9.70 8 -6 10 96.49 21.00 8 -6 10 134.69 21.80 8 -6 10 112.89 16.50 9 -6 10 27.40 11.30 9 -6 10 8.70 6.20 10 -6 10 52.49 12.80 10 -6 10 32.20 14.10 10 5 -10 -5.10 9.60 10 5 -10 7.50 4.70 -10 -5 10 13.30 9.20 9 5 -10 4.10 7.50 9 5 -10 15.20 4.20 -9 -5 10 13.20 10.80 8 5 -10 -13.90 5.20 8 5 -10 3.30 3.30 -8 -5 10 -2.30 6.20 7 5 -10 141.39 15.10 7 5 -10 117.69 9.10 -7 -5 10 136.79 18.90 6 5 -10 60.99 10.80 6 5 -10 45.80 5.90 -6 -5 10 64.19 13.30 5 5 -10 175.98 14.20 5 5 -10 177.98 8.20 -5 -5 10 172.48 19.90 4 5 -10 18.50 5.50 4 5 -10 10.40 1.70 -4 -5 10 12.90 7.50 3 5 -10 3.20 2.20 -3 -5 10 2.00 4.30 2 5 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-10 75.59 4.40 4 4 -10 79.79 4.50 4 4 -10 84.59 11.10 -4 -4 10 69.19 11.30 3 4 -10 278.47 16.00 -3 -4 10 295.17 18.70 2 4 -10 329.27 16.70 -2 -4 10 275.97 16.50 1 4 -10 1333.37 40.90 -1 -4 10 1340.57 40.90 0 4 -10 434.26 21.20 0 -4 10 466.45 20.80 0 -4 10 432.96 12.80 -1 4 -10 103.09 10.80 -1 4 -10 124.99 7.50 1 -4 10 117.89 7.20 1 -4 10 124.39 11.00 -2 4 -10 301.07 13.90 2 -4 10 277.37 13.10 2 -4 10 297.37 18.10 -3 4 -10 4.00 3.40 3 -4 10 1.90 2.70 3 -4 10 1.90 4.20 -4 4 -10 406.66 19.70 4 -4 10 423.86 19.70 4 -4 10 357.76 24.00 -5 4 -10 239.88 16.80 5 -4 10 362.66 25.10 5 -4 10 309.77 17.80 5 -4 10 252.47 22.00 -6 4 -10 68.09 10.90 6 -4 10 81.19 15.90 6 -4 10 71.99 11.70 6 -4 10 67.19 14.60 -7 4 -10 78.49 12.40 7 -4 10 52.89 10.70 7 -4 10 84.19 17.90 7 -4 10 39.90 12.60 8 -4 10 108.49 19.20 8 -4 10 125.39 19.60 8 -4 10 69.79 12.40 9 -4 10 3.90 8.40 9 -4 10 2.20 5.40 10 -4 10 89.49 16.50 11 3 -10 4.20 6.20 -11 -3 10 9.70 10.40 10 3 -10 8.80 10.80 -10 -3 10 18.50 10.20 9 3 -10 8.90 4.60 9 3 -10 -3.30 7.90 -9 -3 10 22.40 10.20 8 3 -10 37.50 7.20 8 3 -10 36.20 10.40 -8 -3 10 38.80 12.70 7 3 -10 51.69 7.60 7 3 -10 32.70 10.20 -7 -3 10 23.80 15.30 6 3 -10 1.40 2.50 -6 -3 10 12.20 8.70 5 3 -10 3.10 2.10 5 3 -10 2.60 2.10 5 3 -10 -3.20 2.70 -5 -3 10 -0.80 5.70 4 3 -10 190.68 8.00 4 3 -10 171.88 7.70 4 3 -10 161.08 13.50 -4 -3 10 180.58 16.60 3 3 -10 3.60 1.10 3 3 -10 2.80 1.10 3 3 -10 2.20 3.10 -3 -3 10 9.70 4.90 2 3 -10 -0.30 2.10 -2 -3 10 5.00 4.30 1 3 -10 50.99 3.00 1 3 -10 49.80 8.10 -1 -3 10 31.10 6.30 -1 -3 10 50.39 2.80 0 3 -10 248.68 15.40 0 3 -10 272.07 11.00 0 -3 10 248.88 14.80 0 -3 10 258.27 9.30 -1 3 -10 3.50 2.50 -1 3 -10 -1.00 3.00 1 -3 10 -3.30 1.50 1 -3 10 1.40 3.10 -2 3 -10 2.50 2.70 2 -3 10 0.80 2.20 2 -3 10 -1.40 2.70 -3 3 -10 50.49 7.70 3 -3 10 42.60 6.90 3 -3 10 57.79 10.30 -4 3 -10 169.78 12.20 4 -3 10 155.68 12.00 4 -3 10 153.98 15.50 -5 3 -10 66.29 10.10 5 -3 10 65.59 9.90 5 -3 10 62.69 13.10 5 -3 10 63.89 13.20 -6 3 -10 324.47 20.40 6 -3 10 325.47 25.20 6 -3 10 315.47 25.70 6 -3 10 328.37 19.90 -7 3 -10 33.60 8.80 7 -3 10 40.00 8.60 7 -3 10 31.50 10.90 -8 3 -10 -2.80 6.60 8 -3 10 12.20 7.20 8 -3 10 5.30 5.90 9 -3 10 17.30 10.00 9 -3 10 28.40 10.10 10 -3 10 134.19 24.10 10 -3 10 112.09 16.80 11 2 -10 20.90 7.50 -11 -2 10 25.80 12.10 10 2 -10 86.59 12.90 10 2 -10 42.20 15.60 -10 -2 10 95.89 19.50 9 2 -10 -1.80 8.80 9 2 -10 3.20 4.30 -9 -2 10 15.60 9.70 8 2 -10 98.19 16.70 8 2 -10 74.99 10.30 -8 -2 10 97.39 19.20 7 2 -10 33.50 9.50 7 2 -10 30.00 6.50 -7 -2 10 46.00 13.60 6 2 -10 37.00 9.70 6 2 -10 45.60 6.40 6 2 -10 30.40 5.40 -6 -2 10 22.50 9.80 5 2 -10 43.70 8.70 5 2 -10 50.69 6.20 5 2 -10 62.49 6.00 -5 -2 10 73.69 14.20 4 2 -10 14.10 5.40 4 2 -10 12.10 2.80 4 2 -10 20.60 3.70 -4 -2 10 13.40 7.10 3 2 -10 313.07 11.70 3 2 -10 324.17 17.80 -3 -2 10 285.77 18.90 2 2 -10 783.32 28.60 2 2 -10 794.22 19.10 -2 -2 10 776.52 30.10 1 2 -10 2139.79 46.00 1 2 -10 2150.28 56.79 -1 -2 10 2102.89 57.09 -1 -2 10 2093.59 46.10 0 2 -10 1621.64 46.90 0 2 -10 1635.24 37.80 0 -2 10 1581.84 45.90 0 -2 10 1559.94 37.30 -1 2 -10 426.66 15.70 -1 2 -10 441.56 21.90 1 -2 10 427.06 15.40 1 -2 10 462.35 20.90 -2 2 -10 115.89 8.90 2 -2 10 119.49 9.50 2 -2 10 143.19 12.00 -3 2 -10 405.26 18.20 3 -2 10 416.46 18.30 3 -2 10 410.26 22.40 -4 2 -10 117.49 10.90 4 -2 10 134.79 14.30 4 -2 10 120.59 10.60 -5 2 -10 185.08 14.30 5 -2 10 157.08 19.70 5 -2 10 205.78 18.80 5 -2 10 172.08 13.70 -6 2 -10 268.57 18.40 6 -2 10 277.47 23.90 6 -2 10 244.48 17.50 6 -2 10 270.37 22.70 -7 2 -10 4.50 5.70 7 -2 10 -0.40 6.20 7 -2 10 4.80 4.70 7 -2 10 0.60 5.70 -8 2 -10 93.09 14.90 8 -2 10 98.19 15.00 8 -2 10 109.29 20.50 8 -2 10 138.19 20.90 9 -2 10 37.40 14.10 9 -2 10 18.30 10.30 9 -2 10 31.80 9.10 10 -2 10 131.99 18.70 10 -2 10 118.89 20.50 11 1 -10 43.20 10.60 11 1 -10 39.60 9.80 -11 -1 10 78.69 19.20 10 1 -10 38.50 9.00 10 1 -10 18.50 14.80 10 1 -10 32.40 8.20 -10 -1 10 45.50 13.90 9 1 -10 16.70 5.90 9 1 -10 4.20 9.30 -9 -1 10 30.90 11.00 8 1 -10 118.49 11.50 8 1 -10 128.29 18.40 -8 -1 10 120.59 21.30 7 1 -10 209.28 13.40 7 1 -10 165.38 11.90 7 1 -10 153.88 20.10 -7 -1 10 221.08 26.00 6 1 -10 12.50 4.50 6 1 -10 12.20 5.80 6 1 -10 16.10 4.70 -6 -1 10 8.40 8.50 5 1 -10 24.40 5.60 5 1 -10 29.10 5.00 5 1 -10 33.20 8.70 -5 -1 10 24.60 9.50 4 1 -10 14.00 5.70 4 1 -10 10.80 3.10 -4 -1 10 7.90 6.80 3 1 -10 104.29 10.70 3 1 -10 105.69 6.30 -3 -1 10 113.89 14.10 2 1 -10 421.56 13.30 2 1 -10 413.46 19.80 -2 -1 10 417.56 21.40 -2 -1 10 420.96 13.60 1 1 -10 145.09 11.20 1 1 -10 161.38 7.50 -1 -1 10 146.89 7.30 -1 -1 10 163.28 12.20 0 1 -10 16.20 4.40 0 1 -10 12.60 3.50 0 -1 10 13.10 2.90 0 -1 10 15.50 4.80 -1 1 -10 0.80 2.10 -1 1 -10 -0.60 3.00 1 -1 10 1.60 2.40 1 -1 10 1.10 2.30 -2 1 -10 93.79 8.00 2 -1 10 92.99 7.80 2 -1 10 75.09 9.40 -3 1 -10 41.60 6.60 3 -1 10 47.90 7.60 3 -1 10 41.00 8.40 -4 1 -10 142.69 11.70 4 -1 10 128.09 13.10 4 -1 10 139.79 11.40 -5 1 -10 1.10 4.20 5 -1 10 -2.30 2.80 5 -1 10 6.40 6.80 5 -1 10 0.60 4.30 -6 1 -10 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10 82.09 17.30 6 -12 -10 39.40 13.20 -6 12 10 44.90 12.60 5 -12 -10 198.58 22.90 -5 12 10 266.07 25.00 4 -12 -10 37.80 9.50 -4 12 10 36.80 10.60 3 -12 -10 119.49 12.70 -3 12 10 105.79 15.20 -3 12 10 109.59 16.50 2 -12 -10 1.40 3.90 -2 12 10 -1.90 4.90 -2 12 10 0.40 4.30 1 -12 -10 67.49 8.20 -1 12 10 79.39 13.80 0 12 10 38.50 10.50 1 12 10 4.10 6.00 2 12 10 89.19 15.10 3 12 10 1.00 5.80 4 12 10 -0.40 8.30 6 -13 -10 -15.50 8.40 -6 13 10 3.70 8.40 5 -13 -10 65.89 13.20 -5 13 10 78.99 14.70 4 -13 -10 8.50 6.70 -4 13 10 14.90 8.90 3 -13 -10 71.59 10.50 -3 13 10 64.79 14.30 -3 13 10 80.19 12.60 2 -13 -10 8.60 3.70 -2 13 10 0.90 4.40 -2 13 10 25.40 9.80 1 -13 -10 7.00 3.10 -1 13 10 13.70 7.90 0 13 10 29.90 8.70 1 13 10 32.70 10.00 2 13 10 -7.40 5.40 3 13 10 107.69 19.10 5 -14 -10 -3.80 9.90 4 -14 -10 2.80 6.90 -3 14 10 19.00 8.50 2 -14 -10 9.40 4.60 -2 14 10 23.60 8.90 -1 14 10 -1.60 7.40 0 14 10 6.80 9.10 1 14 10 44.30 11.70 -2 -16 11 0.30 4.40 -1 -16 11 12.00 4.90 0 -16 11 9.70 6.00 0 -16 11 19.40 5.40 0 -16 11 1.20 6.60 0 -16 11 -1.30 4.30 1 -16 11 24.50 7.30 1 -16 11 35.30 10.00 1 -16 11 32.30 8.00 1 -16 11 25.90 6.90 2 -16 11 10.90 5.90 2 -16 11 47.70 12.90 2 -16 11 20.70 7.20 2 -16 11 6.00 5.50 3 -16 11 -4.50 6.40 3 -16 11 0.80 6.10 3 -16 11 -2.20 7.80 3 -16 11 19.30 11.10 4 -16 11 13.70 8.10 4 -16 11 0.60 12.80 4 -16 11 -0.10 7.10 -4 -15 11 10.30 4.40 -3 -15 11 8.60 4.30 -2 -15 11 48.90 6.70 -1 -15 11 21.40 4.80 -1 -15 11 14.70 8.70 -1 -15 11 30.00 6.90 0 -15 11 32.40 6.30 0 -15 11 31.90 8.00 0 -15 11 18.20 6.70 1 -15 11 -3.50 4.90 1 -15 11 3.60 6.60 1 -15 11 0.20 4.60 1 -15 11 0.50 4.60 2 -15 11 30.30 8.70 2 -15 11 66.09 10.10 2 -15 11 52.39 10.20 2 -15 11 54.09 13.10 3 -15 11 27.60 7.10 3 -15 11 25.80 8.40 3 -15 11 25.40 8.50 3 -15 11 52.89 12.00 4 -15 11 51.89 10.10 4 -15 11 40.90 10.70 4 -15 11 67.89 16.40 4 -15 11 45.80 10.60 5 -15 11 148.89 18.20 5 -15 11 113.49 18.00 -5 -14 11 2.20 3.90 -4 -14 11 12.00 3.80 -3 -14 11 -2.60 2.30 -3 -14 11 -2.20 2.80 -2 -14 11 4.20 4.90 -2 -14 11 5.30 4.10 -2 -14 11 12.30 3.50 -1 -14 11 14.60 5.30 -1 -14 11 1.00 4.40 -1 -14 11 6.60 3.40 0 -14 11 66.79 10.10 0 -14 11 71.79 11.60 0 -14 11 73.99 8.90 1 -14 11 13.30 4.50 1 -14 11 2.30 4.00 1 -14 11 -1.30 3.40 1 -14 11 -2.30 6.30 2 -14 11 194.78 14.20 2 -14 11 185.98 16.50 2 -14 11 186.18 22.20 2 -14 11 170.18 14.50 3 -14 11 33.10 11.90 3 -14 11 21.90 7.80 3 -14 11 15.30 6.20 3 -14 11 26.70 7.20 4 -14 11 64.79 13.50 4 -14 11 90.69 19.10 4 -14 11 94.39 13.20 4 -14 11 71.19 12.10 5 -14 11 -2.40 6.70 5 -14 11 -16.40 6.10 5 -14 11 6.70 9.40 5 -14 11 -1.80 5.50 6 -14 11 60.29 15.10 6 -14 11 21.60 9.00 6 13 -11 144.19 12.10 -5 -13 11 0.40 2.70 -4 -13 11 73.19 7.70 -4 -13 11 65.49 6.50 -3 -13 11 24.10 4.10 -2 -13 11 143.89 8.60 -2 -13 11 127.49 12.20 -1 -13 11 55.89 9.60 -1 -13 11 54.09 8.90 -1 -13 11 57.79 7.10 0 -13 11 79.69 12.40 0 -13 11 78.69 9.30 0 -13 11 85.99 8.20 0 -13 11 84.89 10.90 1 -13 11 46.30 8.90 1 -13 11 47.40 7.70 1 -13 11 42.00 7.60 1 -13 11 43.20 9.60 2 -13 11 12.90 5.10 2 -13 11 16.60 6.40 2 -13 11 16.30 5.40 2 -13 11 22.80 8.00 3 -13 11 37.10 8.70 3 -13 11 36.20 10.50 3 -13 11 30.10 8.00 3 -13 11 31.40 7.20 4 -13 11 3.80 8.90 4 -13 11 3.00 6.60 4 -13 11 -8.40 4.40 4 -13 11 -0.20 6.60 5 -13 11 22.70 8.40 5 -13 11 26.90 9.40 5 -13 11 27.90 13.00 5 -13 11 26.40 8.70 6 -13 11 2.70 7.80 6 -13 11 -9.60 7.20 6 -13 11 -14.10 4.70 7 -13 11 36.00 11.00 7 -13 11 20.20 18.90 7 12 -11 -10.50 4.70 7 12 -11 -9.20 4.90 6 12 -11 108.29 7.60 -6 -12 11 94.79 7.20 -5 -12 11 3.10 2.70 -4 -12 11 138.69 7.50 -3 -12 11 12.60 5.90 -3 -12 11 15.60 3.20 -2 -12 11 128.19 7.50 -2 -12 11 110.49 11.90 -1 -12 11 87.89 11.40 -1 -12 11 88.79 6.80 0 -12 11 0.80 2.50 0 -12 11 10.40 4.40 0 -12 11 4.50 3.30 1 -12 11 -0.20 2.70 1 -12 11 -0.30 3.30 1 -12 11 4.90 2.50 2 -12 11 1.90 3.60 2 -12 11 2.60 5.00 2 -12 11 6.90 3.80 2 -12 11 -3.80 3.30 3 -12 11 34.20 7.80 3 -12 11 26.70 7.50 3 -12 11 44.70 10.90 3 -12 11 30.90 9.00 4 -12 11 273.67 18.50 4 -12 11 299.37 26.70 4 -12 11 256.27 23.50 4 -12 11 240.78 17.70 5 -12 11 45.10 9.80 5 -12 11 76.39 15.20 5 -12 11 47.00 10.50 6 -12 11 111.79 15.10 6 -12 11 109.29 25.20 6 -12 11 121.09 22.00 6 -12 11 111.19 14.90 7 -12 11 57.39 14.90 7 -12 11 61.59 12.60 8 -12 11 158.18 26.30 8 -12 11 119.79 17.90 8 11 -11 36.70 6.20 8 11 -11 45.40 9.20 -8 -11 11 67.29 10.90 7 11 -11 58.29 9.40 7 11 -11 51.89 6.60 -7 -11 11 45.60 8.40 6 11 -11 12.00 3.30 6 11 -11 16.50 5.40 -6 -11 11 16.30 6.20 5 11 -11 171.18 8.10 5 11 -11 209.18 14.00 -5 -11 11 173.88 15.90 -5 -11 11 175.88 8.40 4 11 -11 8.90 4.80 -4 -11 11 3.90 2.30 -4 -11 11 5.10 5.80 -3 -11 11 24.30 3.40 -3 -11 11 32.50 7.60 -2 -11 11 13.90 5.80 -2 -11 11 16.20 3.00 -1 -11 11 33.50 7.30 -1 -11 11 38.20 4.70 0 -11 11 12.70 3.40 0 -11 11 20.60 6.50 0 -11 11 13.90 4.30 1 -11 11 -3.30 2.80 1 -11 11 0.80 2.50 1 -11 11 -1.50 2.40 2 -11 11 276.87 20.00 2 -11 11 241.78 20.70 2 -11 11 256.87 14.90 2 -11 11 259.37 15.40 3 -11 11 6.50 5.80 3 -11 11 -2.50 2.90 3 -11 11 8.40 4.00 3 -11 11 12.40 5.20 4 -11 11 133.29 13.00 4 -11 11 138.19 13.00 4 -11 11 153.48 20.00 4 -11 11 127.69 19.60 5 -11 11 62.59 11.50 5 -11 11 50.99 9.60 5 -11 11 65.59 14.70 5 -11 11 86.59 16.80 6 -11 11 6.50 9.60 6 -11 11 19.40 7.30 6 -11 11 12.70 7.40 6 -11 11 6.10 7.60 7 -11 11 4.40 7.50 7 -11 11 7.30 7.90 7 -11 11 -2.80 6.90 8 -11 11 12.20 11.40 8 -11 11 20.30 8.10 8 10 -11 13.20 4.20 8 10 -11 16.20 6.00 -8 -10 11 6.30 6.90 7 10 -11 112.69 8.20 7 10 -11 118.69 13.80 -7 -10 11 119.19 15.80 6 10 -11 69.89 5.50 6 10 -11 78.19 10.60 -6 -10 11 84.49 13.00 5 10 -11 40.50 4.20 5 10 -11 39.40 6.70 -5 -10 11 38.10 4.30 -5 -10 11 56.09 10.90 4 10 -11 118.39 11.60 -4 -10 11 141.59 15.00 -4 -10 11 126.99 7.10 3 10 -11 0.50 3.80 -3 -10 11 12.60 6.10 -3 -10 11 3.50 1.30 -2 -10 11 105.29 11.20 -1 -10 11 32.10 4.00 -1 -10 11 35.00 7.40 -1 -10 11 47.80 5.30 0 -10 11 250.87 12.10 0 -10 11 261.17 16.90 0 -10 11 259.77 11.70 1 -10 11 9.30 3.60 1 -10 11 4.20 3.70 1 -10 11 4.10 2.80 2 -10 11 67.79 11.60 2 -10 11 99.29 9.00 2 -10 11 98.19 10.70 3 -10 11 9.60 6.60 3 -10 11 4.80 5.10 3 -10 11 0.60 4.10 3 -10 11 0.70 3.30 4 -10 11 7.90 4.30 4 -10 11 1.50 3.90 4 -10 11 16.40 7.20 5 -10 11 27.30 7.20 5 -10 11 28.40 10.40 5 -10 11 17.10 6.40 5 -10 11 34.30 11.40 6 -10 11 48.60 13.20 6 -10 11 45.70 13.40 6 -10 11 36.40 8.70 6 -10 11 20.00 7.20 7 -10 11 101.49 18.90 7 -10 11 76.59 12.80 8 -10 11 -0.90 7.80 8 -10 11 -12.50 6.60 9 -10 11 7.80 10.70 9 -10 11 35.80 9.50 9 9 -11 51.99 7.30 9 9 -11 17.90 9.50 -9 -9 11 76.89 14.80 8 9 -11 -13.20 5.30 8 9 -11 2.20 3.20 -8 -9 11 5.00 6.60 7 9 -11 57.59 6.40 7 9 -11 43.20 8.30 -7 -9 11 54.49 11.80 6 9 -11 2.10 2.10 6 9 -11 7.40 4.10 -6 -9 11 -1.80 5.50 5 9 -11 57.49 8.80 5 9 -11 56.09 4.20 -5 -9 11 53.59 10.80 4 9 -11 2.50 3.40 -4 -9 11 10.50 5.30 3 9 -11 213.98 14.40 -3 -9 11 198.98 16.20 2 9 -11 0.10 3.10 -2 -9 11 3.20 1.20 -2 -9 11 0.90 3.00 -2 -9 11 0.00 1.00 -1 -9 11 9.60 4.10 -1 -9 11 13.90 2.70 -1 -9 11 10.20 3.20 0 -9 11 17.00 3.70 0 -9 11 10.30 4.40 0 -9 11 9.90 2.90 1 -9 11 38.00 8.30 1 -9 11 35.30 5.20 2 -9 11 69.09 8.50 2 -9 11 55.89 7.60 2 -9 11 59.89 11.00 3 -9 11 110.29 10.50 3 -9 11 104.09 9.80 3 -9 11 123.99 16.70 4 -9 11 56.89 12.00 4 -9 11 89.39 16.10 4 -9 11 76.39 10.90 5 -9 11 31.20 11.40 5 -9 11 53.19 9.90 6 -9 11 75.89 16.00 6 -9 11 101.59 18.90 6 -9 11 71.59 12.10 7 -9 11 13.10 9.60 7 -9 11 4.80 5.00 7 -9 11 8.90 10.30 8 -9 11 123.69 17.00 8 -9 11 102.39 20.70 9 -9 11 11.00 10.30 9 -9 11 -10.90 7.10 9 8 -11 29.40 6.90 9 8 -11 27.60 9.20 -9 -8 11 21.70 10.40 8 8 -11 119.79 9.20 8 8 -11 83.39 13.40 -8 -8 11 97.19 16.00 7 8 -11 31.80 7.90 7 8 -11 18.90 4.00 -7 -8 11 18.60 7.70 6 8 -11 54.49 5.10 6 8 -11 54.19 9.00 -6 -8 11 38.00 11.10 5 8 -11 41.00 3.30 5 8 -11 39.90 8.00 -5 -8 11 46.60 10.90 4 8 -11 0.00 3.00 -4 -8 11 1.90 6.30 3 8 -11 98.49 10.10 -3 -8 11 130.69 13.40 2 8 -11 6.20 5.00 -2 -8 11 11.10 4.90 1 8 -11 359.46 20.90 -1 -8 11 325.27 9.30 -1 -8 11 360.56 19.10 -1 -8 11 322.17 9.60 0 -8 11 880.71 32.90 0 -8 11 833.62 23.10 0 -8 11 882.21 23.60 1 -8 11 920.21 27.20 1 -8 11 952.20 35.80 1 -8 11 906.41 27.20 2 -8 11 238.68 18.10 2 -8 11 242.58 13.20 2 -8 11 258.67 13.70 3 -8 11 610.94 24.50 3 -8 11 605.84 31.70 4 -8 11 130.39 11.70 4 -8 11 129.79 18.90 4 -8 11 91.89 15.40 5 -8 11 8.50 8.50 5 -8 11 1.40 4.90 5 -8 11 11.70 4.90 6 -8 11 18.50 6.30 6 -8 11 12.50 7.40 6 -8 11 15.40 10.10 7 -8 11 6.50 10.30 7 -8 11 15.40 6.30 7 -8 11 1.90 7.30 8 -8 11 203.98 19.50 8 -8 11 225.38 30.00 9 -8 11 -1.40 7.50 9 -8 11 10.10 8.00 10 7 -11 -1.30 10.60 10 7 -11 2.00 4.80 -10 -7 11 -1.90 9.20 9 7 -11 67.59 8.60 9 7 -11 54.89 12.20 -9 -7 11 88.99 17.40 8 7 -11 25.30 5.10 8 7 -11 31.60 8.60 -8 -7 11 28.30 9.10 7 7 -11 13.50 5.60 7 7 -11 26.60 4.70 -7 -7 11 35.50 10.00 6 7 -11 -1.80 3.90 6 7 -11 0.60 1.70 -6 -7 11 5.40 7.50 5 7 -11 23.00 6.40 5 7 -11 24.30 3.00 -5 -7 11 13.60 7.00 4 7 -11 81.89 10.70 -4 -7 11 86.09 12.80 3 7 -11 188.28 13.50 -3 -7 11 147.19 14.10 2 7 -11 123.49 11.10 -2 -7 11 111.89 11.40 1 7 -11 193.28 15.00 -1 -7 11 199.18 14.10 0 7 -11 44.20 9.10 0 -7 11 27.70 6.50 0 -7 11 31.00 3.70 0 -7 11 37.70 4.20 1 -7 11 371.46 14.40 1 -7 11 375.36 20.80 1 -7 11 360.86 14.30 2 -7 11 30.60 7.90 2 -7 11 47.80 6.70 3 -7 11 255.87 14.60 3 -7 11 264.37 19.90 4 -7 11 65.79 9.70 4 -7 11 66.29 12.90 5 -7 11 13.40 7.20 5 -7 11 0.20 3.70 5 -7 11 6.10 7.20 6 -7 11 46.40 13.50 6 -7 11 28.30 11.40 6 -7 11 36.10 8.60 7 -7 11 16.70 6.70 7 -7 11 34.90 12.70 7 -7 11 17.60 8.10 8 -7 11 39.50 13.70 8 -7 11 32.80 9.10 9 -7 11 3.80 8.60 9 -7 11 10.20 7.60 10 -7 11 43.00 18.00 10 -7 11 19.50 10.10 10 6 -11 7.90 5.00 -10 -6 11 9.90 11.20 9 6 -11 2.30 3.30 9 6 -11 -10.90 6.70 -9 -6 11 8.80 10.70 8 6 -11 5.40 3.20 8 6 -11 -5.40 5.90 -8 -6 11 2.20 7.20 7 6 -11 80.19 6.90 7 6 -11 65.29 11.20 -7 -6 11 45.50 12.50 6 6 -11 224.18 10.10 -6 -6 11 231.28 21.90 5 6 -11 282.57 17.80 5 6 -11 260.97 9.10 -5 -6 11 237.38 20.40 4 6 -11 2.70 3.40 -4 -6 11 -0.70 6.10 3 6 -11 383.46 19.70 -3 -6 11 391.76 22.20 2 6 -11 526.95 23.50 -2 -6 11 521.65 24.50 1 6 -11 206.38 14.50 -1 -6 11 213.38 14.40 0 6 -11 2.30 3.30 0 -6 11 2.40 2.30 0 -6 11 2.60 1.50 0 -6 11 -1.20 2.60 1 -6 11 679.83 20.60 1 -6 11 676.03 28.80 2 -6 11 11.60 5.20 2 -6 11 5.60 3.40 3 -6 11 804.42 28.00 3 -6 11 810.22 36.20 4 -6 11 2.20 3.20 4 -6 11 13.60 6.80 5 -6 11 246.68 22.50 5 -6 11 230.48 21.20 5 -6 11 229.18 16.10 6 -6 11 235.08 17.40 6 -6 11 204.08 25.20 7 -6 11 21.80 9.10 7 -6 11 15.80 6.40 7 -6 11 30.80 17.10 8 -6 11 42.50 13.80 8 -6 11 34.00 11.40 8 -6 11 27.80 8.40 9 -6 11 95.49 16.10 9 -6 11 73.19 18.60 10 -6 11 28.30 8.90 10 -6 11 10.30 10.70 10 5 -11 28.50 6.30 10 5 -11 32.80 12.80 -10 -5 11 49.00 12.80 9 5 -11 1.80 3.50 9 5 -11 -13.90 6.30 -9 -5 11 14.40 8.90 8 5 -11 -1.50 5.70 8 5 -11 -3.10 2.80 -8 -5 11 10.20 9.30 7 5 -11 145.79 9.50 7 5 -11 151.78 15.70 -7 -5 11 129.39 19.40 6 5 -11 110.09 7.40 6 5 -11 117.79 14.50 -6 -5 11 113.19 18.30 5 5 -11 111.49 11.70 5 5 -11 105.09 5.70 -5 -5 11 87.09 14.90 4 5 -11 35.50 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13 199.18 20.90 6 -8 13 33.90 8.10 6 -8 13 51.29 13.30 6 -8 13 45.90 12.60 7 -8 13 26.80 8.40 7 -8 13 20.20 9.30 8 -8 13 4.20 8.50 8 -8 13 -2.30 6.20 9 -8 13 16.70 7.90 9 -8 13 5.20 8.40 9 7 -13 3.70 3.70 9 7 -13 -0.30 4.20 -9 -7 13 -5.00 8.10 8 7 -13 201.98 19.30 8 7 -13 188.68 10.10 8 7 -13 200.28 10.90 7 7 -13 3.70 1.80 7 7 -13 2.20 2.20 7 7 -13 3.70 4.60 -7 -7 13 3.20 5.90 6 7 -13 84.49 12.70 -6 -7 13 105.99 17.70 5 7 -13 36.30 8.20 -5 -7 13 16.70 8.70 4 7 -13 8.50 4.60 -4 -7 13 15.60 8.00 3 7 -13 33.00 7.50 -3 -7 13 43.20 10.10 2 7 -13 49.20 9.10 -2 -7 13 48.40 9.80 1 7 -13 49.10 9.70 -1 -7 13 49.20 9.00 0 7 -13 46.40 9.10 0 -7 13 37.30 3.40 0 -7 13 26.70 7.00 1 -7 13 4.70 2.50 1 -7 13 4.30 2.90 2 -7 13 223.98 12.40 2 -7 13 259.67 19.20 3 -7 13 29.20 6.00 3 -7 13 25.60 8.00 4 -7 13 1.80 3.90 4 -7 13 -2.10 3.80 5 -7 13 25.80 13.90 5 -7 13 12.90 8.40 5 -7 13 15.30 5.60 6 -7 13 5.20 8.40 6 -7 13 8.00 8.00 7 -7 13 66.29 17.10 7 -7 13 57.19 14.70 7 -7 13 87.19 13.90 8 -7 13 58.99 15.80 8 -7 13 65.19 11.90 9 -7 13 43.80 15.70 9 -7 13 53.79 16.10 10 6 -13 84.49 9.80 10 6 -13 46.30 8.60 -10 -6 13 123.19 21.60 9 6 -13 -1.00 4.00 9 6 -13 2.60 3.20 9 6 -13 0.90 8.50 -9 -6 13 11.80 10.20 8 6 -13 76.69 7.10 8 6 -13 75.09 7.30 8 6 -13 79.19 14.40 -8 -6 13 83.39 16.60 7 6 -13 130.19 7.60 7 6 -13 120.59 7.70 7 6 -13 118.39 15.40 -7 -6 13 114.29 19.00 6 6 -13 145.79 17.10 6 6 -13 155.08 6.50 -6 -6 13 167.48 21.10 5 6 -13 32.70 7.70 -5 -6 13 50.79 12.20 4 6 -13 3.70 3.50 -4 -6 13 2.50 5.90 3 6 -13 9.10 5.10 -3 -6 13 25.00 7.60 2 6 -13 -0.70 2.00 -2 -6 13 -0.10 3.40 1 6 -13 11.90 5.40 -1 -6 13 17.60 6.10 0 6 -13 221.88 17.50 0 -6 13 214.78 8.10 0 -6 13 206.58 15.50 1 -6 13 28.70 4.40 1 -6 13 22.20 6.50 2 -6 13 243.28 18.30 2 -6 13 227.48 12.30 3 -6 13 118.69 10.10 3 -6 13 146.59 15.00 4 -6 13 71.89 9.70 4 -6 13 80.99 13.60 5 -6 13 30.40 11.10 5 -6 13 35.00 8.30 5 -6 13 36.10 10.20 6 -6 13 0.90 7.20 6 -6 13 3.20 4.60 6 -6 13 -0.90 4.80 7 -6 13 92.69 18.00 7 -6 13 47.70 13.20 7 -6 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9 -7 14 -3.70 11.00 9 -7 14 -8.50 7.30 10 6 -14 1.10 4.70 10 6 -14 2.90 5.00 -10 -6 14 24.80 14.40 9 6 -14 19.50 4.70 9 6 -14 -0.20 9.40 9 6 -14 16.60 4.90 8 6 -14 97.09 7.60 8 6 -14 83.89 16.00 -8 -6 14 103.39 19.50 7 6 -14 150.08 7.50 7 6 -14 140.89 7.00 7 6 -14 136.19 16.90 -7 -6 14 162.08 23.40 6 6 -14 177.88 16.50 -6 -6 14 188.78 23.60 5 6 -14 142.29 14.30 -5 -6 14 148.89 19.60 4 6 -14 25.60 7.10 -4 -6 14 27.30 9.10 3 6 -14 920.11 36.00 -3 -6 14 869.81 38.00 2 6 -14 1.80 3.20 -2 -6 14 15.20 6.70 1 6 -14 777.52 33.60 -1 -6 14 780.92 33.20 0 6 -14 110.89 14.40 0 -6 14 97.39 12.70 0 -6 14 97.79 5.30 1 -6 14 188.68 15.90 1 -6 14 166.28 9.20 2 -6 14 94.39 8.20 2 -6 14 99.49 13.80 3 -6 14 33.60 8.80 3 -6 14 21.00 5.60 4 -6 14 256.37 21.90 4 -6 14 290.87 16.70 5 -6 14 2.80 5.10 5 -6 14 4.90 4.70 6 -6 14 117.09 17.00 6 -6 14 156.08 21.30 6 -6 14 117.59 22.40 7 -6 14 48.70 14.70 7 -6 14 57.49 14.90 7 -6 14 52.19 10.70 8 -6 14 14.40 8.00 8 -6 14 29.80 11.10 9 -6 14 8.50 8.20 9 -6 14 -1.10 6.30 10 5 -14 -8.00 4.70 10 5 -14 2.80 4.70 -10 -5 14 21.20 11.40 9 5 -14 118.09 9.70 9 5 -14 115.59 10.50 9 5 -14 111.39 18.40 -9 -5 14 107.09 19.60 8 5 -14 14.50 8.30 8 5 -14 0.90 2.80 8 5 -14 6.70 2.80 -8 -5 14 -7.60 7.90 7 5 -14 236.38 10.70 7 5 -14 241.28 20.70 7 5 -14 231.38 10.80 -7 -5 14 212.58 26.60 6 5 -14 105.69 15.30 6 5 -14 106.29 5.30 -6 -5 14 96.99 18.10 5 5 -14 122.89 15.50 -5 -5 14 83.89 15.20 4 5 -14 40.50 8.30 -4 -5 14 34.10 10.40 3 5 -14 300.47 19.40 -3 -5 14 356.16 23.30 2 5 -14 4.10 3.60 -2 -5 14 8.50 5.20 1 5 -14 18.40 6.10 -1 -5 14 15.20 5.60 0 5 -14 14.50 5.70 0 -5 14 12.70 5.30 0 -5 14 16.60 2.80 -1 5 -14 31.30 5.00 -1 5 -14 23.80 8.10 1 -5 14 37.30 8.40 1 -5 14 30.00 4.50 -2 5 -14 9.00 4.20 2 -5 14 8.30 3.10 2 -5 14 9.00 4.90 -3 5 -14 7.50 4.60 3 -5 14 6.00 3.50 3 -5 14 8.90 5.30 -4 5 -14 0.60 4.10 4 -5 14 -0.50 3.90 4 -5 14 -4.30 3.00 -5 5 -14 121.69 15.20 5 -5 14 131.59 12.50 5 -5 14 108.89 19.90 -6 5 -14 -1.50 4.50 6 -5 14 13.70 8.10 6 -5 14 25.70 9.80 7 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52.79 13.10 0 -10 21 42.40 12.70 1 -10 21 57.49 12.50 1 -10 21 81.69 4.60 2 -10 21 94.19 7.80 2 -10 21 85.99 7.80 2 -10 21 79.19 15.40 3 -10 21 2.90 5.00 3 -10 21 28.40 8.60 3 -10 21 19.90 5.30 4 -10 21 55.89 9.80 4 -10 21 76.89 16.20 5 -10 21 236.48 17.30 5 -10 21 177.68 25.60 -7 -9 21 63.39 19.80 -6 -9 21 -3.70 10.60 5 9 -21 13.60 8.70 -5 -9 21 7.80 11.20 4 9 -21 2.90 7.30 -4 -9 21 9.10 8.40 3 9 -21 16.00 9.20 -3 -9 21 -2.50 7.40 -2 -9 21 -3.70 6.00 1 9 -21 24.50 12.00 -1 -9 21 15.60 8.50 0 -9 21 20.70 8.80 1 -9 21 46.80 5.10 1 -9 21 57.19 4.80 1 -9 21 30.80 9.50 2 -9 21 23.40 9.40 2 -9 21 21.00 4.80 3 -9 21 24.60 5.80 3 -9 21 17.60 7.90 4 -9 21 41.00 12.00 4 -9 21 48.30 8.70 5 -9 21 1.40 5.10 5 -9 21 9.70 8.10 6 -9 21 18.80 7.80 6 -9 21 16.90 9.90 -7 -8 21 20.50 12.20 -6 -8 21 0.30 10.10 5 8 -21 14.90 8.50 -5 -8 21 6.30 9.80 4 8 -21 43.20 10.80 -4 -8 21 39.10 13.80 -3 -8 21 61.09 14.90 2 8 -21 175.38 22.90 -2 -8 21 146.19 21.00 1 8 -21 118.19 21.80 -1 -8 21 117.39 18.00 0 8 -21 71.39 22.10 0 -8 21 100.59 16.30 1 -8 21 34.90 4.70 1 -8 21 33.40 10.30 2 -8 21 10.50 6.60 2 -8 21 16.10 4.30 3 -8 21 17.50 8.50 3 -8 21 20.40 5.10 4 -8 21 0.70 6.80 4 -8 21 5.80 4.50 5 -8 21 -1.20 4.90 6 -8 21 14.90 6.50 6 -8 21 -12.90 6.90 -7 -7 21 2.70 12.00 6 7 -21 49.30 13.00 -6 -7 21 81.89 18.50 5 7 -21 6.70 7.40 -5 -7 21 12.60 10.80 4 7 -21 15.40 9.60 -4 -7 21 34.30 10.30 3 7 -21 -3.90 4.80 -3 -7 21 3.90 8.10 2 7 -21 41.00 12.70 -2 -7 21 64.29 14.90 1 7 -21 65.49 13.90 -1 -7 21 63.39 13.20 0 7 -21 41.80 10.40 0 -7 21 24.70 3.00 0 -7 21 18.50 8.10 1 -7 21 23.10 8.20 1 -7 21 36.30 5.00 2 -7 21 61.19 13.80 2 -7 21 61.19 7.90 3 -7 21 74.09 14.80 3 -7 21 71.79 9.60 4 -7 21 80.59 15.80 4 -7 21 62.09 9.60 5 -7 21 6.90 7.70 5 -7 21 -5.10 4.90 6 -7 21 4.70 5.60 6 -7 21 1.50 8.50 -8 -6 21 38.90 21.50 -7 -6 21 -12.60 11.60 -6 -6 21 40.70 14.20 5 6 -21 8.80 8.20 -5 -6 21 30.50 11.90 -4 -6 21 29.90 11.00 3 6 -21 79.99 14.60 -3 -6 21 79.59 16.20 2 6 -21 245.48 22.00 -2 -6 21 182.78 23.60 1 6 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22.40 9.80 4 -5 21 22.10 7.20 5 -5 21 -2.00 5.80 5 -5 21 9.20 4.90 6 -5 21 1.50 6.60 6 -5 21 0.40 5.30 7 -5 21 2.70 9.10 -8 -4 21 -3.70 12.20 -7 -4 21 25.90 12.90 6 4 -21 110.29 16.80 -6 -4 21 125.79 22.40 5 4 -21 5.30 5.40 -5 -4 21 11.30 11.50 -4 -4 21 141.09 21.70 3 4 -21 16.90 7.10 -3 -4 21 33.50 10.50 2 4 -21 111.89 17.50 2 4 -21 102.69 6.10 -2 -4 21 103.09 17.20 -2 -4 21 102.39 5.90 1 4 -21 14.90 3.80 1 4 -21 23.40 8.70 -1 -4 21 19.50 8.20 -1 -4 21 17.40 3.80 0 4 -21 6.00 3.10 0 4 -21 -0.90 4.70 0 -4 21 12.20 6.60 0 -4 21 11.80 3.80 -1 4 -21 243.18 24.70 -1 4 -21 252.47 15.00 1 -4 21 287.67 23.50 1 -4 21 226.88 13.40 -2 4 -21 11.50 5.50 2 -4 21 10.90 6.60 2 -4 21 5.30 3.00 -3 4 -21 174.68 15.20 3 -4 21 154.38 12.80 3 -4 21 213.08 21.00 -4 4 -21 121.39 15.40 4 -4 21 108.69 18.70 4 -4 21 148.79 13.80 -5 4 -21 55.39 10.70 5 -4 21 55.39 10.10 5 -4 21 34.40 11.80 6 -4 21 101.89 14.50 6 -4 21 75.79 20.20 7 -4 21 27.60 10.80 7 -4 21 7.80 10.10 9 3 -21 12.10 4.50 9 3 -21 2.90 4.20 -9 -3 21 10.60 14.20 8 3 -21 8.60 3.80 8 3 -21 8.00 3.10 -8 -3 21 -10.20 12.80 7 3 -21 2.70 2.00 7 3 -21 0.80 2.10 -7 -3 21 2.30 11.10 6 3 -21 3.30 2.10 6 3 -21 -4.50 5.50 6 3 -21 6.20 2.30 -6 -3 21 5.20 9.00 5 3 -21 -3.60 6.60 -5 -3 21 16.60 10.40 4 3 -21 19.60 7.30 4 3 -21 19.80 3.00 -4 -3 21 40.10 13.60 3 3 -21 104.59 16.60 3 3 -21 105.79 6.60 -3 -3 21 93.69 17.10 2 3 -21 21.10 4.50 2 3 -21 34.10 10.20 -2 -3 21 23.90 4.30 1 3 -21 8.70 5.70 1 3 -21 15.60 4.00 -1 -3 21 7.00 5.10 -1 -3 21 18.50 3.70 0 3 -21 5.00 7.00 0 3 -21 -2.10 2.80 0 -3 21 3.10 2.50 0 -3 21 7.60 6.80 -1 3 -21 4.40 3.90 -1 3 -21 5.60 7.20 1 -3 21 14.00 7.10 1 -3 21 9.00 4.20 -2 3 -21 39.30 7.00 2 -3 21 45.60 12.00 2 -3 21 29.00 6.80 -3 3 -21 13.30 5.30 3 -3 21 19.80 5.40 3 -3 21 1.80 6.00 -4 3 -21 48.20 9.40 4 -3 21 64.89 10.30 4 -3 21 57.49 13.40 -5 3 -21 -7.80 6.40 5 -3 21 -13.00 5.00 5 -3 21 3.80 4.70 6 -3 21 38.60 9.90 6 -3 21 39.10 10.80 7 -3 21 6.60 7.80 7 -3 21 -7.40 6.80 9 2 -21 32.50 6.70 9 2 -21 33.40 6.30 -9 -2 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16.30 9 0 -21 247.48 17.00 -9 0 21 175.38 32.50 8 0 -21 87.59 10.30 8 0 -21 96.19 12.40 -8 0 21 73.09 25.00 7 0 -21 245.88 15.80 7 0 -21 246.18 15.00 -7 0 21 210.28 31.40 6 0 -21 34.20 7.00 -6 0 21 40.10 15.30 5 0 -21 94.49 10.30 5 0 -21 67.19 13.30 -5 0 21 72.59 17.80 4 0 -21 8.80 7.00 4 0 -21 14.10 4.30 -4 0 21 10.50 9.60 3 0 -21 56.99 12.40 3 0 -21 74.89 9.30 -3 0 21 84.29 10.20 -3 0 21 80.79 17.20 2 0 -21 8.80 3.70 2 0 -21 13.80 7.10 -2 0 21 15.20 5.30 -2 0 21 19.00 9.70 1 0 -21 265.47 22.70 1 0 -21 214.38 14.30 -1 0 21 194.28 24.10 -1 0 21 211.68 13.90 0 0 -21 94.59 16.10 0 0 -21 101.89 12.10 0 0 21 83.09 10.70 0 0 21 115.59 17.60 -1 0 -21 176.08 23.10 -1 0 -21 225.38 15.90 1 0 21 216.98 21.10 1 0 21 206.48 15.00 -2 0 -21 110.19 18.20 -2 0 -21 86.59 11.70 2 0 21 138.09 15.40 2 0 21 110.09 16.60 -3 0 -21 101.39 13.30 3 0 21 113.19 15.30 3 0 21 112.59 17.70 -4 0 -21 15.30 7.40 4 0 21 40.00 9.10 4 0 21 28.10 10.30 5 0 21 26.70 9.10 5 0 21 30.10 8.60 6 0 21 37.10 11.30 9 -1 -21 13.60 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6.30 -8 2 21 -6.40 11.70 7 -2 -21 10.40 4.50 -7 2 21 22.60 13.20 6 -2 -21 -0.10 4.60 -6 2 21 5.30 9.50 5 -2 -21 183.08 19.40 5 -2 -21 176.28 13.80 -5 2 21 116.69 22.30 4 -2 -21 -2.20 5.90 4 -2 -21 -1.20 4.10 -4 2 21 4.10 4.50 -4 2 21 8.60 10.30 3 -2 -21 94.09 11.70 3 -2 -21 86.59 14.50 -3 2 21 109.69 20.20 -3 2 21 90.89 12.00 2 -2 -21 3.30 3.50 2 -2 -21 -0.40 5.50 -2 2 21 3.10 6.60 -2 2 21 3.00 3.50 1 -2 -21 144.29 19.20 1 -2 -21 136.89 12.20 -1 2 21 119.69 18.70 -1 2 21 110.39 13.20 0 -2 -21 12.60 6.20 0 -2 -21 0.50 3.70 0 2 21 15.60 8.80 0 2 21 3.30 4.60 -1 -2 -21 118.19 19.10 -1 -2 -21 109.39 13.90 1 2 21 82.99 16.10 1 2 21 91.89 12.60 -2 -2 -21 35.00 10.70 -2 -2 -21 23.00 6.80 2 2 21 38.70 8.50 2 2 21 29.30 9.70 -3 -2 -21 -0.20 5.80 3 2 21 -4.50 5.30 3 2 21 1.80 4.80 4 2 21 205.58 21.00 4 2 21 200.38 17.60 5 2 21 43.90 12.30 5 2 21 13.20 7.30 6 2 21 191.78 18.60 6 2 21 165.48 21.90 8 -3 -21 7.80 7.20 8 -3 -21 10.00 6.50 -8 3 21 3.30 13.30 -7 3 21 32.70 16.40 6 -3 -21 12.50 5.30 -6 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3.90 4.80 -1 1 -26 26.90 8.70 1 -1 26 27.30 11.40 1 -1 26 24.90 7.10 -2 1 -26 25.60 8.30 2 -1 26 27.60 8.10 3 -1 26 8.30 7.10 3 -1 26 1.70 10.10 6 0 -26 4.90 5.30 -6 0 26 14.30 19.30 5 0 -26 16.80 5.80 -5 0 26 7.50 12.90 4 0 -26 10.80 5.50 -4 0 26 12.30 13.90 3 0 -26 8.00 5.50 -3 0 26 27.20 14.50 -3 0 26 5.80 5.40 2 0 -26 76.49 11.30 -2 0 26 87.89 12.30 -2 0 26 97.99 20.20 1 0 -26 37.20 7.80 -1 0 26 34.20 14.90 0 0 -26 33.70 8.70 0 0 26 34.00 12.60 0 0 26 32.10 8.10 -1 0 -26 29.40 8.10 1 0 26 29.60 12.10 1 0 26 42.60 9.90 2 0 26 1.30 6.30 3 0 26 18.80 8.40 3 0 26 47.80 15.80 6 -1 -26 -1.40 6.70 5 -1 -26 18.80 7.30 -5 1 26 16.40 15.80 4 -1 -26 -2.20 5.40 -4 1 26 -9.60 10.90 3 -1 -26 15.70 6.50 -3 1 26 5.90 6.40 -3 1 26 28.70 20.70 2 -1 -26 8.20 5.90 -2 1 26 8.50 10.00 -2 1 26 22.80 7.60 1 -1 -26 19.80 6.70 -1 1 26 22.70 6.80 -1 1 26 3.90 9.50 0 -1 -26 21.30 7.00 0 1 26 17.90 7.30 0 1 26 11.90 10.80 -1 -1 -26 28.40 8.40 1 1 26 38.00 12.70 1 1 26 32.10 8.70 2 1 26 -9.40 11.30 2 1 26 1.40 5.70 3 1 26 14.60 9.90 5 -2 -26 -3.10 7.20 -5 2 26 -2.50 12.70 4 -2 -26 -9.50 6.70 -4 2 26 -2.00 5.60 -4 2 26 -5.50 13.20 3 -2 -26 0.00 6.90 -3 2 26 6.60 5.60 2 -2 -26 39.30 11.00 -2 2 26 53.99 9.80 -2 2 26 45.50 17.30 1 -2 -26 44.50 9.80 -1 2 26 61.59 17.40 -1 2 26 60.39 11.60 0 -2 -26 88.79 13.20 0 2 26 49.90 14.50 0 2 26 90.69 13.90 1 2 26 11.80 7.00 1 2 26 -17.70 9.10 2 2 26 -15.90 10.60 2 2 26 10.00 6.00 5 -3 -26 4.60 8.40 -5 3 26 -5.10 12.80 4 -3 -26 9.50 8.30 -4 3 26 -2.50 13.70 -4 3 26 0.40 5.70 3 -3 -26 25.70 8.40 -3 3 26 -7.40 11.60 -3 3 26 13.40 7.40 2 -3 -26 13.40 7.70 -2 3 26 25.30 7.70 -1 3 26 3.90 6.00 -1 3 26 1.60 10.90 0 3 26 0.90 10.40 0 3 26 -1.70 6.20 1 3 26 5.40 6.50 -4 4 26 36.90 9.70 -4 4 26 27.10 14.10 -3 4 26 1.60 12.40 -3 4 26 16.60 8.40 -2 4 26 52.29 18.60 -2 4 26 76.49 13.70 -1 4 26 -1.50 6.30 -1 -9 27 -6.60 9.90 -3 -8 27 4.00 12.80 -2 -8 27 -7.70 10.10 -1 -8 27 59.39 15.00 0 -8 27 11.60 11.20 1 -8 27 4.80 2.80 1 -8 27 -12.90 9.80 -4 -7 27 -11.20 10.80 -3 -7 27 26.30 13.40 -2 -7 27 11.20 12.70 -1 -7 27 -6.00 9.50 0 -7 27 -0.10 9.50 1 -7 27 23.10 4.90 2 -7 27 16.80 5.70 -4 -6 27 -11.40 9.60 -3 -6 27 54.59 18.60 -2 -6 27 1.20 12.50 -1 -6 27 175.98 26.50 0 -6 27 122.79 21.70 1 -6 27 0.60 9.50 1 -6 27 7.60 4.30 2 -6 27 2.50 4.20 2 -6 27 -3.00 7.90 -5 -5 27 15.20 15.80 -4 -5 27 6.10 12.90 -3 -5 27 45.80 15.60 -2 -5 27 -4.00 11.10 -1 -5 27 16.20 11.60 0 5 -27 -5.10 4.20 0 -5 27 5.10 3.60 0 -5 27 -6.60 7.60 -1 5 -27 30.50 6.90 1 -5 27 14.00 10.80 1 -5 27 27.30 5.70 -2 5 -27 9.90 8.30 2 -5 27 9.20 10.50 2 -5 27 11.80 6.10 -3 5 -27 -2.90 10.90 -5 -4 27 -28.60 11.10 -4 -4 27 6.40 12.10 -3 -4 27 16.80 11.70 2 4 -27 0.60 3.00 -2 -4 27 -9.70 8.40 1 4 -27 4.00 4.20 -1 -4 27 6.10 8.70 -1 -4 27 4.40 3.40 0 -4 27 27.30 12.50 0 -4 27 46.00 7.20 -1 4 -27 16.30 7.50 1 -4 27 24.40 5.90 1 -4 27 8.80 10.40 -2 4 -27 83.59 13.80 2 -4 27 58.49 9.60 2 -4 27 68.19 17.20 -3 4 -27 6.00 9.30 3 -4 27 21.20 6.90 -5 -3 27 27.20 14.60 -4 -3 27 12.40 11.60 3 3 -27 119.99 8.40 -3 -3 27 78.29 19.70 2 3 -27 5.90 4.30 -2 -3 27 3.30 10.20 -2 -3 27 -2.30 3.20 1 3 -27 -5.20 5.60 -1 -3 27 -5.60 11.60 -1 -3 27 -6.90 3.50 0 3 -27 10.10 5.80 0 -3 27 -1.10 8.90 0 -3 27 6.60 5.40 -1 3 -27 -11.40 5.50 1 -3 27 -18.70 7.40 1 -3 27 3.80 5.40 -2 3 -27 32.10 11.20 2 -3 27 41.10 13.70 2 -3 27 47.60 9.10 -3 3 -27 -9.80 9.60 3 -3 27 3.80 5.70 3 -3 27 -20.60 14.20 5 2 -27 46.80 6.10 -5 -2 27 32.00 17.50 -4 -2 27 15.20 13.30 3 2 -27 23.50 6.40 -3 -2 27 44.50 17.60 -2 -2 27 -8.20 10.80 -2 -2 27 15.40 5.10 1 2 -27 64.09 9.60 -1 -2 27 72.09 20.90 -1 -2 27 74.99 10.50 0 2 -27 6.90 6.60 0 -2 27 0.30 9.50 0 -2 27 -0.40 4.50 -1 2 -27 116.99 15.40 1 -2 27 80.49 11.70 1 -2 27 95.79 19.80 -2 2 -27 15.00 8.70 2 -2 27 4.00 6.10 2 -2 27 -1.60 8.80 5 1 -27 14.50 5.50 -5 -1 27 -11.40 12.30 4 1 -27 -7.60 6.60 -4 -1 27 -13.10 12.70 3 1 -27 27.90 6.40 -3 -1 27 14.30 12.30 -3 -1 27 22.20 5.60 2 1 -27 29.10 7.00 -2 -1 27 32.20 7.40 -2 -1 27 32.90 15.10 1 1 -27 -5.70 5.20 -1 -1 27 -1.70 4.80 -1 -1 27 -12.00 9.70 0 1 -27 5.00 6.40 0 -1 27 2.70 9.60 0 -1 27 3.80 5.40 -1 1 -27 20.00 9.10 1 -1 27 12.90 10.60 1 -1 27 5.40 6.40 -2 1 -27 11.60 11.20 2 -1 27 -4.40 5.40 2 -1 27 -11.60 8.80 5 0 -27 0.10 6.20 -5 0 27 4.30 25.20 4 0 -27 8.50 6.20 -4 0 27 -6.00 11.80 3 0 -27 40.70 8.90 -3 0 27 36.30 7.70 -3 0 27 47.60 16.40 2 0 -27 5.60 6.20 -2 0 27 -20.30 9.50 1 0 -27 -0.60 6.30 -1 0 27 8.60 11.20 -1 0 27 4.70 5.50 0 0 -27 -6.80 12.90 0 0 27 11.20 7.10 0 0 27 6.90 11.20 -1 0 -27 8.40 7.60 1 0 27 11.40 11.30 1 0 27 2.20 6.40 2 0 27 -17.00 9.80 2 0 27 0.00 6.70 5 -1 -27 86.69 12.20 4 -1 -27 2.40 5.80 -4 1 27 3.80 13.60 3 -1 -27 6.10 6.70 -3 1 27 -15.80 10.90 -3 1 27 2.40 5.30 2 -1 -27 46.30 10.30 -2 1 27 70.79 11.40 -2 1 27 94.09 20.30 1 -1 -27 79.39 12.40 -1 1 27 58.29 11.00 -1 1 27 49.80 16.80 0 -1 -27 38.60 10.90 0 1 27 55.39 10.80 0 1 27 67.49 17.30 1 1 27 15.80 7.60 1 1 27 15.10 11.50 4 -2 -27 168.08 17.90 -4 2 27 177.18 29.70 3 -2 -27 -1.10 7.20 -3 2 27 -6.80 13.00 -3 2 27 10.90 6.50 2 -2 -27 148.39 17.70 -2 2 27 128.79 15.90 -2 2 27 138.89 26.50 1 -2 -27 -3.50 8.80 -1 2 27 -0.20 6.40 -1 2 27 3.20 11.30 0 2 27 77.69 19.50 0 2 27 71.79 13.60 -3 3 27 0.40 6.60 -3 3 27 -18.10 12.10 -2 3 27 1.90 6.60 -2 3 27 -16.80 11.60 -1 3 27 15.10 8.30 -1 3 27 11.70 13.00 -2 -7 28 4.30 15.90 -1 -7 28 67.19 25.90 -3 -6 28 80.49 23.00 -2 -6 28 -11.50 9.90 -1 -6 28 15.00 11.50 0 -6 28 -21.10 9.00 1 -6 28 169.08 12.30 -3 -5 28 44.10 19.10 -2 -5 28 163.88 26.70 -1 -5 28 32.40 4.30 -1 -5 28 24.70 13.50 0 5 -28 39.90 7.30 0 -5 28 35.20 6.30 0 -5 28 42.70 16.50 -1 5 -28 34.90 8.80 1 -5 28 34.90 6.90 -3 -4 28 -1.60 10.40 2 4 -28 299.47 11.90 -2 -4 28 374.96 35.90 1 4 -28 5.40 4.60 -1 -4 28 7.40 4.10 -1 -4 28 -10.60 10.60 0 4 -28 161.68 13.80 0 -4 28 158.68 25.70 0 -4 28 174.08 12.80 -1 4 -28 3.40 7.50 1 -4 28 1.20 12.10 1 -4 28 13.90 6.00 3 3 -28 0.00 3.60 -3 -3 28 -7.10 9.20 2 3 -28 20.00 5.10 -2 -3 28 11.50 11.60 -2 -3 28 27.20 5.40 1 3 -28 50.99 8.70 -1 -3 28 69.69 9.40 -1 -3 28 24.40 14.40 0 3 -28 3.60 6.20 0 -3 28 4.70 4.90 0 -3 28 1.50 10.60 -1 3 -28 15.10 8.40 1 -3 28 10.10 6.10 1 -3 28 15.00 11.70 4 2 -28 15.00 5.70 3 2 -28 17.20 5.80 -3 -2 28 29.00 16.40 2 2 -28 31.20 7.30 -2 -2 28 -7.00 10.70 -2 -2 28 50.89 8.20 1 2 -28 26.10 7.60 -1 -2 28 15.40 14.50 -1 -2 28 8.60 5.40 0 2 -28 -3.40 6.40 0 -2 28 -4.60 9.60 0 -2 28 -8.00 5.00 1 -2 28 22.20 8.00 1 -2 28 -9.90 10.70 4 1 -28 238.58 15.50 3 1 -28 52.59 8.90 -3 -1 28 82.19 23.80 2 1 -28 10.30 6.90 -2 -1 28 -1.70 12.40 -2 -1 28 14.50 5.70 1 1 -28 154.28 16.10 -1 -1 28 94.79 21.80 -1 -1 28 111.19 13.70 0 1 -28 113.69 15.50 0 -1 28 95.39 22.30 0 -1 28 130.49 15.50 -1 1 -28 4.60 8.70 1 -1 28 73.49 19.30 1 -1 28 28.30 9.10 3 0 -28 126.19 13.90 -3 0 28 117.79 24.70 2 0 -28 195.88 16.80 -2 0 28 201.78 16.00 -2 0 28 147.99 28.10 1 0 -28 43.20 17.40 -1 0 28 64.29 17.80 -1 0 28 78.99 12.70 0 0 -28 156.48 17.30 0 0 28 176.78 17.00 0 0 28 157.88 27.20 3 -1 -28 145.39 17.60 -3 1 28 123.99 14.00 2 -1 -28 5.20 8.10 -2 1 28 -5.20 12.80 -2 1 28 -8.90 5.30 1 -1 -28 42.80 10.30 -1 1 28 63.09 19.80 -1 1 28 27.70 9.10 2 3 -29 111.19 10.70 1 3 -29 46.50 9.40 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 84001 _shelx_res_file ; TITL sci14_a.res in P-1 REM Old TITL sci14 in P-1 #2 REM SHELXT solution in P-1 REM R1 0.118, Rweak 0.007, Alpha 0.061, Orientation as input REM Formula found by SHELXT: C40 N8 O6 S2 CELL 0.71073 8.4423 12.0126 20.3063 100.315 96.533 95.678 ZERR 4 0.0003 0.0004 0.0006 0.001 0.001 0.001 LATT 1 SFAC C H N O S UNIT 80 104 16 12 4 L.S. 4 0 0 PLAN 20 SIZE 0.03 0.16 0.28 TEMP -173.1(2) BOND $H list 4 fmap 2 53 ACTA OMIT 0 1 0 OMIT 9 9 2 REM REM REM WGHT 0.047000 0.583100 FVAR 0.51775 S1A 5 0.228971 0.271084 0.626351 11.00000 0.01088 0.01409 = 0.01302 0.00424 0.00159 0.00214 O1A 4 0.335266 0.368561 0.616885 11.00000 0.01812 0.02311 = 0.02045 0.00900 0.00105 -0.00352 O2A 4 0.251578 0.165563 0.582325 11.00000 0.02143 0.01931 = 0.01519 0.00065 0.00173 0.00727 O3A 4 0.061315 0.291610 0.622720 11.00000 0.01161 0.02322 = 0.02189 0.00736 0.00296 0.00586 C14A 1 0.284058 0.252020 0.710340 11.00000 0.01472 0.01521 = 0.01323 0.00379 0.00172 0.00187 C15A 1 0.231665 0.322964 0.763251 11.00000 0.04617 0.02908 = 0.01797 0.00575 0.00614 0.02356 AFIX 43 H15A 2 0.167418 0.380672 0.754543 11.00000 -1.20000 AFIX 0 C16A 1 0.274219 0.308550 0.828846 11.00000 0.06902 0.04042 = 0.01498 0.00317 0.00777 0.03062 AFIX 43 H16A 2 0.238288 0.357030 0.864994 11.00000 -1.20000 AFIX 0 C17A 1 0.368441 0.224680 0.843110 11.00000 0.04266 0.03390 = 0.01690 0.00928 0.00249 0.01146 C18A 1 0.416048 0.153629 0.789393 11.00000 0.02372 0.02579 = 0.02177 0.01088 0.00210 0.00768 AFIX 43 H18A 2 0.478496 0.094971 0.798087 11.00000 -1.20000 AFIX 0 C19A 1 0.374787 0.165859 0.722856 11.00000 0.01656 0.01960 = 0.01856 0.00567 0.00368 0.00593 AFIX 43 H19A 2 0.408209 0.116023 0.686615 11.00000 -1.20000 AFIX 0 C20A 1 0.412464 0.209720 0.915044 11.00000 0.07629 0.06204 = 0.01800 0.01531 0.00392 0.03346 AFIX 137 H20A 2 0.441164 0.284704 0.944600 11.00000 -1.50000 H20B 2 0.504137 0.165842 0.917399 11.00000 -1.50000 H20C 2 0.320613 0.168919 0.929741 11.00000 -1.50000 AFIX 0 S1B 5 0.761882 0.200102 0.373176 11.00000 0.01246 0.01444 = 0.01266 0.00379 0.00245 0.00213 O1B 4 0.900864 0.275401 0.410257 11.00000 0.02385 0.03045 = 0.01650 0.00781 -0.00317 -0.01069 O2B 4 0.787957 0.081374 0.360211 11.00000 0.02968 0.01860 = 0.01899 0.00624 0.00481 0.01145 O3B 4 0.615438 0.218798 0.403757 11.00000 0.01874 0.02734 = 0.02134 0.01047 0.01014 0.01013 C14B 1 0.729882 0.237920 0.292118 11.00000 0.01344 0.01806 = 0.01349 0.00476 0.00165 0.00012 C15B 1 0.784868 0.172208 0.237512 11.00000 0.02335 0.01647 = 0.01652 0.00194 0.00275 0.00172 AFIX 43 H15B 2 0.832875 0.105599 0.242972 11.00000 -1.20000 AFIX 0 C16B 1 0.768851 0.205016 0.174790 11.00000 0.02761 0.02425 = 0.01372 0.00130 0.00269 -0.00034 AFIX 43 H16B 2 0.806865 0.160299 0.137719 11.00000 -1.20000 AFIX 0 C17B 1 0.698657 0.301447 0.165500 11.00000 0.02087 0.02945 = 0.01711 0.00933 -0.00049 -0.00252 C18B 1 0.642415 0.365363 0.220522 11.00000 0.02498 0.02823 = 0.02655 0.01512 0.00418 0.00929 AFIX 43 H18B 2 0.592816 0.431211 0.214731 11.00000 -1.20000 AFIX 0 C19B 1 0.657408 0.334739 0.283672 11.00000 0.02267 0.02352 = 0.01998 0.00882 0.00671 0.00818 AFIX 43 H19B 2 0.618704 0.379293 0.320613 11.00000 -1.20000 AFIX 0 C20B 1 0.687339 0.339561 0.097979 11.00000 0.03938 0.04140 = 0.02053 0.01448 0.00269 0.00219 AFIX 137 H20D 2 0.781194 0.394201 0.097439 11.00000 -1.50000 H20E 2 0.589331 0.375854 0.091237 11.00000 -1.50000 H20F 2 0.684181 0.273244 0.061650 11.00000 -1.50000 AFIX 0 N1A 3 0.215924 0.527372 0.378603 11.00000 0.01166 0.01303 = 0.01378 0.00319 0.00127 0.00280 N2A 3 0.337977 0.450390 0.389827 11.00000 0.01347 0.01530 = 0.01615 0.00464 0.00206 0.00562 N3A 3 0.414822 0.356879 0.476637 11.00000 0.01721 0.01686 = 0.01594 0.00570 0.00401 0.00656 AFIX 93 H3AA 2 0.485505 0.323504 0.453865 11.00000 -1.20000 H3AB 2 0.402861 0.343721 0.517153 11.00000 -1.20000 AFIX 0 N4A 3 0.172585 0.510151 0.233630 11.00000 0.02268 0.01942 = 0.01230 0.00419 0.00239 -0.00078 C1A 1 0.325758 0.427456 0.449724 11.00000 0.01354 0.01274 = 0.01491 0.00246 0.00159 0.00091 C2A 1 0.201846 0.483182 0.486682 11.00000 0.01534 0.01730 = 0.01545 0.00548 0.00432 0.00411 AFIX 23 H2AA 2 0.243865 0.514670 0.534637 11.00000 -1.20000 H2AB 2 0.103299 0.429681 0.484091 11.00000 -1.20000 AFIX 0 C3A 1 0.172090 0.576658 0.447429 11.00000 0.01742 0.01798 = 0.01429 0.00268 0.00396 0.00617 AFIX 23 H3AC 2 0.241539 0.648496 0.468258 11.00000 -1.20000 H3AD 2 0.058254 0.590999 0.444334 11.00000 -1.20000 AFIX 0 C4A 1 0.071103 0.460403 0.333133 11.00000 0.01225 0.01677 = 0.01847 0.00496 0.00113 -0.00091 AFIX 23 H4AA 2 -0.014831 0.510103 0.328887 11.00000 -1.20000 H4AB 2 0.029833 0.396094 0.353371 11.00000 -1.20000 AFIX 0 C5A 1 0.114141 0.414878 0.263875 11.00000 0.02104 0.01524 = 0.01762 0.00321 0.00127 -0.00170 AFIX 23 H5AA 2 0.198314 0.363707 0.267763 11.00000 -1.20000 H5AB 2 0.018411 0.370437 0.234788 11.00000 -1.20000 AFIX 0 C6A 1 0.318324 0.573184 0.275343 11.00000 0.01908 0.01747 = 0.01655 0.00557 0.00544 0.00080 AFIX 23 H6AA 2 0.358988 0.636489 0.254167 11.00000 -1.20000 H6AB 2 0.402535 0.521770 0.278065 11.00000 -1.20000 AFIX 0 C7A 1 0.283585 0.620426 0.345525 11.00000 0.01480 0.01324 = 0.01651 0.00476 0.00184 0.00103 AFIX 23 H7AA 2 0.383940 0.660369 0.373304 11.00000 -1.20000 H7AB 2 0.205927 0.676597 0.342986 11.00000 -1.20000 AFIX 0 C8A 1 0.184566 0.485370 0.163274 11.00000 0.02946 0.02888 = 0.01442 0.00504 0.00350 0.00479 C9A 1 0.207250 0.576661 0.130142 11.00000 0.07988 0.03456 = 0.01926 0.00822 0.01397 0.01010 AFIX 43 H9A 2 0.217007 0.652571 0.154892 11.00000 -1.20000 AFIX 0 C10A 1 0.215630 0.557444 0.061553 11.00000 0.12538 0.05507 = 0.02316 0.01597 0.02024 0.00718 AFIX 43 H10A 2 0.230154 0.620239 0.039388 11.00000 -1.20000 AFIX 0 C11A 1 0.203026 0.447437 0.024927 11.00000 0.11091 0.06593 = 0.01469 0.00239 0.01651 0.00377 AFIX 43 H11A 2 0.209741 0.434566 -0.022160 11.00000 -1.20000 AFIX 0 C12A 1 0.180633 0.356533 0.057255 11.00000 0.06485 0.04644 = 0.02423 -0.00824 0.01249 -0.00289 AFIX 43 H12A 2 0.171728 0.280840 0.032263 11.00000 -1.20000 AFIX 0 C13A 1 0.171008 0.375021 0.126238 11.00000 0.03953 0.03162 = 0.02079 -0.00183 0.00667 -0.00006 AFIX 43 H13A 2 0.155109 0.311950 0.148080 11.00000 -1.20000 AFIX 0 N1B 3 0.806372 -0.003804 0.631265 11.00000 0.01246 0.01798 = 0.01366 0.00238 0.00295 0.00542 N2B 3 0.658245 0.048128 0.617632 11.00000 0.01133 0.01920 = 0.01489 0.00321 0.00315 0.00548 N3B 3 0.554948 0.138338 0.533144 11.00000 0.01728 0.01656 = 0.01556 0.00495 0.00309 0.00476 AFIX 93 H3BA 2 0.469975 0.151872 0.553287 11.00000 -1.20000 H3BB 2 0.565748 0.160839 0.494796 11.00000 -1.20000 AFIX 0 N4B 3 0.813434 -0.012321 0.774095 11.00000 0.01945 0.01831 = 0.01458 0.00353 0.00172 -0.00146 C1B 1 0.667389 0.083711 0.560739 11.00000 0.01476 0.01273 = 0.01311 0.00006 0.00178 -0.00016 C2B 1 0.815036 0.062181 0.528317 11.00000 0.01518 0.02036 = 0.01457 0.00235 0.00450 0.00339 AFIX 23 H2BA 2 0.892049 0.132317 0.535422 11.00000 -1.20000 H2BB 2 0.788271 0.031127 0.479301 11.00000 -1.20000 AFIX 0 C3B 1 0.879888 -0.025265 0.565967 11.00000 0.01726 0.02825 = 0.01441 0.00238 0.00651 0.01006 AFIX 23 H3BC 2 0.998679 -0.012910 0.574843 11.00000 -1.20000 H3BD 2 0.845043 -0.103753 0.540399 11.00000 -1.20000 AFIX 0 C4B 1 0.921425 0.075564 0.685875 11.00000 0.01349 0.01858 = 0.01653 0.00394 0.00143 0.00087 AFIX 23 H4BA 2 0.945497 0.149297 0.671573 11.00000 -1.20000 H4BB 2 1.023392 0.042299 0.692572 11.00000 -1.20000 AFIX 0 C5B 1 0.851825 0.095733 0.751759 11.00000 0.01868 0.01650 = 0.01665 0.00303 0.00228 -0.00137 AFIX 23 H5BA 2 0.930143 0.147334 0.786729 11.00000 -1.20000 H5BB 2 0.753144 0.133062 0.745820 11.00000 -1.20000 AFIX 0 C6B 1 0.700774 -0.091834 0.722485 11.00000 0.01885 0.01526 = 0.01598 0.00301 0.00019 -0.00117 AFIX 23 H6BA 2 0.597341 -0.060192 0.716425 11.00000 -1.20000 H6BB 2 0.680274 -0.165112 0.737722 11.00000 -1.20000 AFIX 0 C7B 1 0.766810 -0.112619 0.655765 11.00000 0.02066 0.01516 = 0.01702 0.00225 0.00043 0.00407 AFIX 23 H7BA 2 0.864974 -0.150730 0.660990 11.00000 -1.20000 H7BB 2 0.686657 -0.164290 0.621611 11.00000 -1.20000 AFIX 0 C8B 1 0.783652 -0.004145 0.841901 11.00000 0.01923 0.02301 = 0.01545 0.00532 0.00279 0.00242 C9B 1 0.662447 -0.075631 0.860208 11.00000 0.02619 0.02286 = 0.02033 0.00623 0.00487 -0.00005 AFIX 43 H9B 2 0.593983 -0.129535 0.826333 11.00000 -1.20000 AFIX 0 C10B 1 0.641201 -0.068419 0.927957 11.00000 0.03360 0.03431 = 0.02388 0.01168 0.00977 0.00099 AFIX 43 H10B 2 0.559151 -0.118495 0.939551 11.00000 -1.20000 AFIX 0 C11B 1 0.736257 0.009414 0.978122 11.00000 0.04508 0.04333 = 0.01646 0.00855 0.00866 0.00284 AFIX 43 H11B 2 0.720107 0.014227 1.024039 11.00000 -1.20000 AFIX 0 C12B 1 0.856624 0.081005 0.960251 11.00000 0.05764 0.05575 = 0.01604 0.00194 -0.00033 -0.02066 AFIX 43 H12B 2 0.923262 0.135640 0.994363 11.00000 -1.20000 AFIX 0 C13B 1 0.880878 0.073935 0.893588 11.00000 0.03877 0.04715 = 0.01702 0.00482 0.00070 -0.01699 AFIX 43 H13B 2 0.965136 0.123005 0.882659 11.00000 -1.20000 AFIX 0 HKLF 4 REM sci14_a.res in P-1 REM R1 = 0.0525 for 8283 Fo > 4sig(Fo) and 0.0921 for all 12050 data REM 507 parameters refined using 0 restraints END WGHT 0.0448 0.4907 REM Highest difference peak 0.440, deepest hole -0.506, 1-sigma level 0.071 Q1 1 0.7600 0.2315 0.3229 11.00000 0.05 0.44 Q2 1 0.7482 0.1772 0.2012 11.00000 0.05 0.36 Q3 1 0.3742 0.1856 0.8186 11.00000 0.05 0.34 Q4 1 0.6849 0.2791 0.2803 11.00000 0.05 0.32 Q5 1 0.2549 0.2897 0.6769 11.00000 0.05 0.31 Q6 1 0.7165 0.3007 0.2991 11.00000 0.05 0.31 Q7 1 -0.1928 0.5186 0.3007 11.00000 0.05 0.29 Q8 1 0.7928 0.2053 0.2782 11.00000 0.05 0.29 Q9 1 0.3639 0.3236 0.8208 11.00000 0.05 0.29 Q10 1 0.1945 0.5216 0.4660 11.00000 0.05 0.29 Q11 1 0.2826 0.5834 0.3012 11.00000 0.05 0.29 Q12 1 0.2533 0.2468 0.6767 11.00000 0.05 0.29 Q13 1 0.7574 -0.0598 0.8557 11.00000 0.05 0.29 Q14 1 0.2084 0.5589 0.4176 11.00000 0.05 0.28 Q15 1 0.2742 0.4649 0.4792 11.00000 0.05 0.28 Q16 1 0.7499 0.2620 0.1769 11.00000 0.05 0.27 Q17 1 0.1711 0.5226 0.1386 11.00000 0.05 0.27 Q18 1 0.7310 0.1969 0.2625 11.00000 0.05 0.27 Q19 1 0.5934 0.3003 0.4003 11.00000 0.05 0.27 Q20 1 0.1770 0.3176 0.8766 11.00000 0.05 0.27 ; _shelx_res_checksum 72968 _shelxl_version_number 2.014 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S S1A 0.22897(5) 0.27108(3) 0.62635(2) 0.01242(9) Uani d 1 . . O O1A 0.33527(16) 0.36856(11) 0.61689(6) 0.0205(3) Uani d 1 . . O O2A 0.25158(16) 0.16556(11) 0.58232(6) 0.0187(3) Uani d 1 . . O O3A 0.06131(15) 0.29161(11) 0.62272(6) 0.0182(3) Uani d 1 . . C C14A 0.2841(2) 0.25202(14) 0.71034(8) 0.0143(3) Uani d 1 . . C C15A 0.2317(3) 0.32296(18) 0.76325(10) 0.0295(5) Uani d 1 . . H H15A 0.1674 0.3807 0.7545 0.035 Uiso calc 1 . . C C16A 0.2742(4) 0.3086(2) 0.82885(10) 0.0399(6) Uani d 1 . . H H16A 0.2383 0.3570 0.8650 0.048 Uiso calc 1 . . C C17A 0.3684(3) 0.22468(19) 0.84311(10) 0.0303(5) Uani d 1 . . C C18A 0.4160(3) 0.15363(17) 0.78939(10) 0.0227(4) Uani d 1 . . H H18A 0.4785 0.0950 0.7981 0.027 Uiso calc 1 . . C C19A 0.3748(2) 0.16586(15) 0.72286(9) 0.0176(4) Uani d 1 . . H H19A 0.4082 0.1160 0.6866 0.021 Uiso calc 1 . . C C20A 0.4125(4) 0.2097(2) 0.91504(11) 0.0496(8) Uani d 1 . . H H20A 0.4412 0.2847 0.9446 0.074 Uiso calc 1 . . H H20B 0.5041 0.1658 0.9174 0.074 Uiso calc 1 . . H H20C 0.3206 0.1689 0.9297 0.074 Uiso calc 1 . . S S1B 0.76188(5) 0.20010(4) 0.37318(2) 0.01294(9) Uani d 1 . . O O1B 0.90086(17) 0.27540(12) 0.41026(6) 0.0246(3) Uani d 1 . . O O2B 0.78796(18) 0.08137(11) 0.36021(6) 0.0214(3) Uani d 1 . . O O3B 0.61544(16) 0.21880(11) 0.40376(7) 0.0207(3) Uani d 1 . . C C14B 0.7299(2) 0.23792(15) 0.29212(8) 0.0149(3) Uani d 1 . . C C15B 0.7849(2) 0.17221(15) 0.23751(9) 0.0190(4) Uani d 1 . . H H15B 0.8329 0.1056 0.2430 0.023 Uiso calc 1 . . C C16B 0.7689(3) 0.20502(17) 0.17479(9) 0.0224(4) Uani d 1 . . H H16B 0.8069 0.1603 0.1377 0.027 Uiso calc 1 . . C C17B 0.6987(2) 0.30145(17) 0.16550(9) 0.0225(4) Uani d 1 . . C C18B 0.6424(3) 0.36536(17) 0.22052(10) 0.0249(4) Uani d 1 . . H H18B 0.5928 0.4312 0.2147 0.030 Uiso calc 1 . . C C19B 0.6574(2) 0.33474(16) 0.28367(9) 0.0208(4) Uani d 1 . . H H19B 0.6187 0.3793 0.3206 0.025 Uiso calc 1 . . C C20B 0.6873(3) 0.3396(2) 0.09798(10) 0.0330(5) Uani d 1 . . H H20D 0.7812 0.3942 0.0974 0.049 Uiso calc 1 . . H H20E 0.5893 0.3759 0.0912 0.049 Uiso calc 1 . . H H20F 0.6842 0.2732 0.0617 0.049 Uiso calc 1 . . N N1A 0.21592(18) 0.52737(12) 0.37860(7) 0.0127(3) Uani d 1 . . N N2A 0.33798(18) 0.45039(12) 0.38983(7) 0.0145(3) Uani d 1 . . N N3A 0.41482(19) 0.35688(12) 0.47664(7) 0.0159(3) Uani d 1 . . H H3AA 0.4855 0.3235 0.4539 0.019 Uiso calc 1 . . H H3AB 0.4029 0.3437 0.5172 0.019 Uiso calc 1 . . N N4A 0.1726(2) 0.51015(13) 0.23363(7) 0.0182(3) Uani d 1 . . C C1A 0.3258(2) 0.42746(14) 0.44972(8) 0.0138(3) Uani d 1 . . C C2A 0.2018(2) 0.48318(15) 0.48668(9) 0.0154(3) Uani d 1 . . H H2AA 0.2439 0.5147 0.5346 0.018 Uiso calc 1 . . H H2AB 0.1033 0.4297 0.4841 0.018 Uiso calc 1 . . C C3A 0.1721(2) 0.57666(15) 0.44743(8) 0.0162(3) Uani d 1 . . H H3AC 0.2415 0.6485 0.4683 0.019 Uiso calc 1 . . H H3AD 0.0583 0.5910 0.4443 0.019 Uiso calc 1 . . C C4A 0.0711(2) 0.46040(15) 0.33313(9) 0.0159(3) Uani d 1 . . H H4AA -0.0148 0.5101 0.3289 0.019 Uiso calc 1 . . H H4AB 0.0298 0.3961 0.3534 0.019 Uiso calc 1 . . C C5A 0.1141(2) 0.41488(15) 0.26387(9) 0.0183(4) Uani d 1 . . H H5AA 0.1983 0.3637 0.2678 0.022 Uiso calc 1 . . H H5AB 0.0184 0.3704 0.2348 0.022 Uiso calc 1 . . C C6A 0.3183(2) 0.57318(15) 0.27534(9) 0.0173(4) Uani d 1 . . H H6AA 0.3590 0.6365 0.2542 0.021 Uiso calc 1 . . H H6AB 0.4025 0.5218 0.2781 0.021 Uiso calc 1 . . C C7A 0.2836(2) 0.62043(14) 0.34553(8) 0.0147(3) Uani d 1 . . H H7AA 0.3839 0.6604 0.3733 0.018 Uiso calc 1 . . H H7AB 0.2059 0.6766 0.3430 0.018 Uiso calc 1 . . C C8A 0.1846(3) 0.48537(17) 0.16327(9) 0.0240(4) Uani d 1 . . C C9A 0.2072(4) 0.5767(2) 0.13014(11) 0.0434(7) Uani d 1 . . H H9A 0.2170 0.6526 0.1549 0.052 Uiso calc 1 . . C C10A 0.2156(5) 0.5574(3) 0.06155(13) 0.0663(11) Uani d 1 . . H H10A 0.2302 0.6202 0.0394 0.080 Uiso calc 1 . . C C11A 0.2030(5) 0.4474(3) 0.02493(12) 0.0644(10) Uani d 1 . . H H11A 0.2097 0.4346 -0.0222 0.077 Uiso calc 1 . . C C12A 0.1806(4) 0.3565(2) 0.05725(12) 0.0472(7) Uani d 1 . . H H12A 0.1717 0.2808 0.0323 0.057 Uiso calc 1 . . C C13A 0.1710(3) 0.37502(19) 0.12624(10) 0.0316(5) Uani d 1 . . H H13A 0.1551 0.3120 0.1481 0.038 Uiso calc 1 . . N N1B 0.80637(18) -0.00380(12) 0.63126(7) 0.0144(3) Uani d 1 . . N N2B 0.65824(18) 0.04813(12) 0.61763(7) 0.0148(3) Uani d 1 . . N N3B 0.55495(19) 0.13834(12) 0.53314(7) 0.0160(3) Uani d 1 . . H H3BA 0.4700 0.1519 0.5533 0.019 Uiso calc 1 . . H H3BB 0.5657 0.1608 0.4948 0.019 Uiso calc 1 . . N N4B 0.81343(19) -0.01232(13) 0.77410(7) 0.0177(3) Uani d 1 . . C C1B 0.6674(2) 0.08371(14) 0.56074(8) 0.0140(3) Uani d 1 . . C C2B 0.8150(2) 0.06218(15) 0.52832(9) 0.0166(3) Uani d 1 . . H H2BA 0.8920 0.1323 0.5354 0.020 Uiso calc 1 . . H H2BB 0.7883 0.0311 0.4793 0.020 Uiso calc 1 . . C C3B 0.8799(2) -0.02526(17) 0.56597(9) 0.0193(4) Uani d 1 . . H H3BC 0.9987 -0.0129 0.5748 0.023 Uiso calc 1 . . H H3BD 0.8450 -0.1038 0.5404 0.023 Uiso calc 1 . . C C4B 0.9214(2) 0.07556(15) 0.68588(9) 0.0162(3) Uani d 1 . . H H4BA 0.9455 0.1493 0.6716 0.019 Uiso calc 1 . . H H4BB 1.0234 0.0423 0.6926 0.019 Uiso calc 1 . . C C5B 0.8518(2) 0.09573(15) 0.75176(9) 0.0175(4) Uani d 1 . . H H5BA 0.9301 0.1473 0.7867 0.021 Uiso calc 1 . . H H5BB 0.7531 0.1331 0.7458 0.021 Uiso calc 1 . . C C6B 0.7008(2) -0.09183(15) 0.72248(9) 0.0171(4) Uani d 1 . . H H6BA 0.5973 -0.0602 0.7164 0.021 Uiso calc 1 . . H H6BB 0.6803 -0.1651 0.7377 0.021 Uiso calc 1 . . C C7B 0.7668(2) -0.11262(15) 0.65576(9) 0.0178(4) Uani d 1 . . H H7BA 0.8650 -0.1507 0.6610 0.021 Uiso calc 1 . . H H7BB 0.6867 -0.1643 0.6216 0.021 Uiso calc 1 . . C C8B 0.7837(2) -0.00414(16) 0.84190(9) 0.0190(4) Uani d 1 . . C C9B 0.6624(3) -0.07563(17) 0.86021(10) 0.0229(4) Uani d 1 . . H H9B 0.5940 -0.1295 0.8263 0.028 Uiso calc 1 . . C C10B 0.6412(3) -0.06842(19) 0.92796(10) 0.0296(5) Uani d 1 . . H H10B 0.5592 -0.1185 0.9396 0.036 Uiso calc 1 . . C C11B 0.7363(3) 0.0094(2) 0.97812(10) 0.0344(5) Uani d 1 . . H H11B 0.7201 0.0142 1.0240 0.041 Uiso calc 1 . . C C12B 0.8566(4) 0.0810(2) 0.96025(11) 0.0461(7) Uani d 1 . . H H12B 0.9233 0.1356 0.9944 0.055 Uiso calc 1 . . C C13B 0.8809(3) 0.0739(2) 0.89359(10) 0.0362(6) Uani d 1 . . H H13B 0.9651 0.1230 0.8827 0.043 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S1A 0.0109(2) 0.01409(19) 0.01302(19) 0.00214(15) 0.00159(15) 0.00424(15) O1A 0.0181(7) 0.0231(7) 0.0205(6) -0.0035(5) 0.0010(5) 0.0090(5) O2A 0.0214(7) 0.0193(6) 0.0152(6) 0.0073(5) 0.0017(5) 0.0006(5) O3A 0.0116(6) 0.0232(6) 0.0219(6) 0.0059(5) 0.0030(5) 0.0074(5) C14A 0.0147(9) 0.0152(8) 0.0132(7) 0.0019(6) 0.0017(6) 0.0038(6) C15A 0.0462(14) 0.0291(10) 0.0180(9) 0.0236(10) 0.0061(9) 0.0058(8) C16A 0.0690(19) 0.0404(13) 0.0150(9) 0.0306(13) 0.0078(11) 0.0032(9) C17A 0.0427(14) 0.0339(11) 0.0169(9) 0.0115(10) 0.0025(9) 0.0093(8) C18A 0.0237(11) 0.0258(10) 0.0218(9) 0.0077(8) 0.0021(8) 0.0109(8) C19A 0.0166(9) 0.0196(8) 0.0186(8) 0.0059(7) 0.0037(7) 0.0057(7) C20A 0.076(2) 0.0620(17) 0.0180(10) 0.0335(16) 0.0039(12) 0.0153(11) S1B 0.0125(2) 0.01444(19) 0.01266(19) 0.00213(15) 0.00245(15) 0.00379(15) O1B 0.0239(8) 0.0305(7) 0.0165(6) -0.0107(6) -0.0032(5) 0.0078(6) O2B 0.0297(8) 0.0186(6) 0.0190(6) 0.0114(6) 0.0048(6) 0.0062(5) O3B 0.0187(7) 0.0273(7) 0.0213(6) 0.0101(6) 0.0101(5) 0.0105(5) C14B 0.0134(9) 0.0181(8) 0.0135(8) 0.0001(7) 0.0016(6) 0.0048(6) C15B 0.0234(10) 0.0165(8) 0.0165(8) 0.0017(7) 0.0027(7) 0.0019(7) C16B 0.0276(11) 0.0242(9) 0.0137(8) -0.0003(8) 0.0027(7) 0.0013(7) C17B 0.0209(10) 0.0294(10) 0.0171(8) -0.0025(8) -0.0005(7) 0.0093(8) C18B 0.0250(11) 0.0282(10) 0.0266(10) 0.0093(8) 0.0042(8) 0.0151(8) C19B 0.0227(10) 0.0235(9) 0.0200(9) 0.0082(8) 0.0067(8) 0.0088(7) C20B 0.0394(14) 0.0414(13) 0.0205(10) 0.0022(10) 0.0027(9) 0.0145(9) N1A 0.0117(7) 0.0130(6) 0.0138(7) 0.0028(5) 0.0013(5) 0.0032(5) N2A 0.0135(7) 0.0153(7) 0.0162(7) 0.0056(6) 0.0021(6) 0.0046(5) N3A 0.0172(8) 0.0169(7) 0.0159(7) 0.0066(6) 0.0040(6) 0.0057(6) N4A 0.0227(9) 0.0194(7) 0.0123(7) -0.0008(6) 0.0024(6) 0.0042(6) C1A 0.0135(8) 0.0127(7) 0.0149(8) 0.0009(6) 0.0016(6) 0.0025(6) C2A 0.0153(9) 0.0173(8) 0.0155(8) 0.0041(7) 0.0043(7) 0.0055(6) C3A 0.0174(9) 0.0180(8) 0.0143(8) 0.0062(7) 0.0040(7) 0.0027(6) C4A 0.0122(8) 0.0168(8) 0.0185(8) -0.0009(7) 0.0011(7) 0.0050(7) C5A 0.0210(10) 0.0152(8) 0.0176(8) -0.0017(7) 0.0013(7) 0.0032(7) C6A 0.0191(9) 0.0175(8) 0.0165(8) 0.0008(7) 0.0054(7) 0.0056(7) C7A 0.0148(9) 0.0132(8) 0.0165(8) 0.0010(6) 0.0018(6) 0.0048(6) C8A 0.0295(11) 0.0289(10) 0.0144(8) 0.0048(9) 0.0035(8) 0.0050(7) C9A 0.080(2) 0.0346(12) 0.0193(10) 0.0101(13) 0.0140(12) 0.0082(9) C10A 0.125(3) 0.0551(17) 0.0232(12) 0.0072(19) 0.0202(16) 0.0160(12) C11A 0.111(3) 0.0659(19) 0.0147(11) 0.004(2) 0.0165(15) 0.0024(12) C12A 0.065(2) 0.0464(15) 0.0242(11) -0.0029(14) 0.0125(12) -0.0082(10) C13A 0.0395(14) 0.0316(11) 0.0208(10) -0.0001(10) 0.0067(9) -0.0018(8) N1B 0.0125(7) 0.0180(7) 0.0137(7) 0.0054(6) 0.0030(6) 0.0024(5) N2B 0.0113(7) 0.0192(7) 0.0149(7) 0.0055(6) 0.0032(6) 0.0032(6) N3B 0.0173(8) 0.0166(7) 0.0156(7) 0.0048(6) 0.0031(6) 0.0049(6) N4B 0.0194(8) 0.0183(7) 0.0146(7) -0.0015(6) 0.0017(6) 0.0035(6) C1B 0.0148(9) 0.0127(8) 0.0131(7) -0.0002(6) 0.0018(6) 0.0001(6) C2B 0.0152(9) 0.0204(8) 0.0146(8) 0.0034(7) 0.0045(7) 0.0023(7) C3B 0.0173(9) 0.0283(10) 0.0144(8) 0.0101(8) 0.0065(7) 0.0024(7) C4B 0.0135(9) 0.0186(8) 0.0165(8) 0.0009(7) 0.0014(7) 0.0039(7) C5B 0.0187(9) 0.0165(8) 0.0167(8) -0.0014(7) 0.0023(7) 0.0030(7) C6B 0.0189(9) 0.0153(8) 0.0160(8) -0.0012(7) 0.0002(7) 0.0030(6) C7B 0.0207(10) 0.0152(8) 0.0170(8) 0.0041(7) 0.0004(7) 0.0022(6) C8B 0.0192(10) 0.0230(9) 0.0154(8) 0.0024(7) 0.0028(7) 0.0053(7) C9B 0.0262(11) 0.0229(9) 0.0203(9) -0.0001(8) 0.0049(8) 0.0062(7) C10B 0.0336(13) 0.0343(11) 0.0239(10) 0.0010(10) 0.0098(9) 0.0117(9) C11B 0.0451(15) 0.0433(13) 0.0165(9) 0.0028(11) 0.0087(9) 0.0086(9) C12B 0.0576(18) 0.0558(16) 0.0160(10) -0.0207(14) -0.0003(10) 0.0019(10) C13B 0.0388(14) 0.0472(14) 0.0170(9) -0.0170(11) 0.0007(9) 0.0048(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1A S1A C14A . . 106.64(8) ? O2A S1A O1A . . 112.46(8) ? O2A S1A C14A . . 106.20(8) ? O3A S1A O1A . . 112.85(8) ? O3A S1A O2A . . 112.69(8) ? O3A S1A C14A . . 105.32(8) ? C15A C14A S1A . . 118.94(15) ? C19A C14A S1A . . 120.59(14) ? C19A C14A C15A . . 120.45(17) ? C14A C15A H15A . . 120.4 ? C16A C15A C14A . . 119.2(2) ? C16A C15A H15A . . 120.4 ? C15A C16A H16A . . 119.2 ? C15A C16A C17A . . 121.6(2) ? C17A C16A H16A . . 119.2 ? C16A C17A C20A . . 120.8(2) ? C18A C17A C16A . . 117.95(19) ? C18A C17A C20A . . 121.2(2) ? C17A C18A H18A . . 119.1 ? C17A C18A C19A . . 121.72(19) ? C19A C18A H18A . . 119.1 ? C14A C19A C18A . . 118.99(18) ? C14A C19A H19A . . 120.5 ? C18A C19A H19A . . 120.5 ? C17A C20A H20A . . 109.5 ? C17A C20A H20B . . 109.5 ? C17A C20A H20C . . 109.5 ? H20A C20A H20B . . 109.5 ? H20A C20A H20C . . 109.5 ? H20B C20A H20C . . 109.5 ? O1B S1B O3B . . 112.20(8) ? O1B S1B C14B . . 106.29(8) ? O2B S1B O1B . . 113.37(9) ? O2B S1B O3B . . 112.74(8) ? O2B S1B C14B . . 105.47(8) ? O3B S1B C14B . . 106.04(8) ? C15B C14B S1B . . 119.11(14) ? C15B C14B C19B . . 120.08(16) ? C19B C14B S1B . . 120.75(14) ? C14B C15B H15B . . 120.2 ? C14B C15B C16B . . 119.50(18) ? C16B C15B H15B . . 120.2 ? C15B C16B H16B . . 119.3 ? C17B C16B C15B . . 121.32(19) ? C17B C16B H16B . . 119.3 ? C16B C17B C18B . . 118.38(17) ? C16B C17B C20B . . 121.21(19) ? C18B C17B C20B . . 120.4(2) ? C17B C18B H18B . . 119.3 ? C19B C18B C17B . . 121.45(19) ? C19B C18B H18B . . 119.3 ? C14B C19B H19B . . 120.4 ? C18B C19B C14B . . 119.26(18) ? C18B C19B H19B . . 120.4 ? C17B C20B H20D . . 109.5 ? C17B C20B H20E . . 109.5 ? C17B C20B H20F . . 109.5 ? H20D C20B H20E . . 109.5 ? H20D C20B H20F . . 109.5 ? H20E C20B H20F . . 109.5 ? N2A N1A C3A . . 106.90(12) ? N2A N1A C4A . . 109.30(13) ? N2A N1A C7A . . 109.84(13) ? C4A N1A C3A . . 110.90(13) ? C7A N1A C3A . . 110.76(13) ? C7A N1A C4A . . 109.11(13) ? C1A N2A N1A . . 105.54(14) ? H3AA N3A H3AB . . 120.0 ? C1A N3A H3AA . . 120.0 ? C1A N3A H3AB . . 120.0 ? C5A N4A C6A . . 109.75(14) ? C8A N4A C5A . . 116.75(15) ? C8A N4A C6A . . 114.11(15) ? N2A C1A N3A . . 122.85(17) ? N2A C1A C2A . . 116.04(16) ? N3A C1A C2A . . 121.09(15) ? C1A C2A H2AA . . 111.6 ? C1A C2A H2AB . . 111.6 ? C1A C2A C3A . . 100.69(14) ? H2AA C2A H2AB . . 109.4 ? C3A C2A H2AA . . 111.6 ? C3A C2A H2AB . . 111.6 ? N1A C3A H3AC . . 111.3 ? N1A C3A H3AD . . 111.3 ? C2A C3A N1A . . 102.33(14) ? C2A C3A H3AC . . 111.3 ? C2A C3A H3AD . . 111.3 ? H3AC C3A H3AD . . 109.2 ? N1A C4A H4AA . . 109.5 ? N1A C4A H4AB . . 109.5 ? N1A C4A C5A . . 110.69(14) ? H4AA C4A H4AB . . 108.1 ? C5A C4A H4AA . . 109.5 ? C5A C4A H4AB . . 109.5 ? N4A C5A C4A . . 109.40(14) ? N4A C5A H5AA . . 109.8 ? N4A C5A H5AB . . 109.8 ? C4A C5A H5AA . . 109.8 ? C4A C5A H5AB . . 109.8 ? H5AA C5A H5AB . . 108.2 ? N4A C6A H6AA . . 109.5 ? N4A C6A H6AB . . 109.5 ? N4A C6A C7A . . 110.58(15) ? H6AA C6A H6AB . . 108.1 ? C7A C6A H6AA . . 109.5 ? C7A C6A H6AB . . 109.5 ? N1A C7A C6A . . 111.26(13) ? N1A C7A H7AA . . 109.4 ? N1A C7A H7AB . . 109.4 ? C6A C7A H7AA . . 109.4 ? C6A C7A H7AB . . 109.4 ? H7AA C7A H7AB . . 108.0 ? C9A C8A N4A . . 118.02(18) ? C13A C8A N4A . . 123.05(18) ? C13A C8A C9A . . 118.92(19) ? C8A C9A H9A . . 119.8 ? C10A C9A C8A . . 120.4(2) ? C10A C9A H9A . . 119.8 ? C9A C10A H10A . . 119.8 ? C9A C10A C11A . . 120.5(3) ? C11A C10A H10A . . 119.8 ? C10A C11A H11A . . 120.2 ? C12A C11A C10A . . 119.5(2) ? C12A C11A H11A . . 120.2 ? C11A C12A H12A . . 119.8 ? C11A C12A C13A . . 120.4(2) ? C13A C12A H12A . . 119.8 ? C8A C13A C12A . . 120.2(2) ? C8A C13A H13A . . 119.9 ? C12A C13A H13A . . 119.9 ? N2B N1B C3B . . 107.54(13) ? N2B N1B C4B . . 109.94(13) ? N2B N1B C7B . . 109.48(13) ? C4B N1B C3B . . 110.48(14) ? C7B N1B C3B . . 111.39(14) ? C7B N1B C4B . . 108.02(13) ? C1B N2B N1B . . 105.85(14) ? H3BA N3B H3BB . . 120.0 ? C1B N3B H3BA . . 120.0 ? C1B N3B H3BB . . 120.0 ? C6B N4B C5B . . 110.79(14) ? C8B N4B C5B . . 116.43(14) ? C8B N4B C6B . . 116.90(14) ? N2B C1B N3B . . 122.89(17) ? N2B C1B C2B . . 116.08(16) ? N3B C1B C2B . . 121.01(15) ? C1B C2B H2BA . . 111.5 ? C1B C2B H2BB . . 111.5 ? C1B C2B C3B . . 101.15(14) ? H2BA C2B H2BB . . 109.4 ? C3B C2B H2BA . . 111.5 ? C3B C2B H2BB . . 111.5 ? N1B C3B H3BC . . 111.2 ? N1B C3B H3BD . . 111.2 ? C2B C3B N1B . . 102.81(14) ? C2B C3B H3BC . . 111.2 ? C2B C3B H3BD . . 111.2 ? H3BC C3B H3BD . . 109.1 ? N1B C4B H4BA . . 109.4 ? N1B C4B H4BB . . 109.4 ? N1B C4B C5B . . 111.23(14) ? H4BA C4B H4BB . . 108.0 ? C5B C4B H4BA . . 109.4 ? C5B C4B H4BB . . 109.4 ? N4B C5B C4B . . 110.74(15) ? N4B C5B H5BA . . 109.5 ? N4B C5B H5BB . . 109.5 ? C4B C5B H5BA . . 109.5 ? C4B C5B H5BB . . 109.5 ? H5BA C5B H5BB . . 108.1 ? N4B C6B H6BA . . 109.4 ? N4B C6B H6BB . . 109.4 ? N4B C6B C7B . . 111.11(15) ? H6BA C6B H6BB . . 108.0 ? C7B C6B H6BA . . 109.4 ? C7B C6B H6BB . . 109.4 ? N1B C7B C6B . . 111.94(14) ? N1B C7B H7BA . . 109.2 ? N1B C7B H7BB . . 109.2 ? C6B C7B H7BA . . 109.2 ? C6B C7B H7BB . . 109.2 ? H7BA C7B H7BB . . 107.9 ? C9B C8B N4B . . 122.07(16) ? C9B C8B C13B . . 117.59(17) ? C13B C8B N4B . . 120.29(17) ? C8B C9B H9B . . 119.8 ? C10B C9B C8B . . 120.44(18) ? C10B C9B H9B . . 119.8 ? C9B C10B H10B . . 119.3 ? C11B C10B C9B . . 121.40(19) ? C11B C10B H10B . . 119.3 ? C10B C11B H11B . . 120.8 ? C10B C11B C12B . . 118.45(19) ? C12B C11B H11B . . 120.8 ? C11B C12B H12B . . 119.5 ? C13B C12B C11B . . 120.9(2) ? C13B C12B H12B . . 119.5 ? C8B C13B H13B . . 119.4 ? C12B C13B C8B . . 121.2(2) ? C12B C13B H13B . . 119.4 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag S1A O1A . 1.4578(13) ? S1A O2A . 1.4572(13) ? S1A O3A . 1.4565(14) ? S1A C14A . 1.7771(17) ? C14A C15A . 1.390(3) ? C14A C19A . 1.389(3) ? C15A H15A . 0.9500 ? C15A C16A . 1.385(3) ? C16A H16A . 0.9500 ? C16A C17A . 1.394(3) ? C17A C18A . 1.383(3) ? C17A C20A . 1.513(3) ? C18A H18A . 0.9500 ? C18A C19A . 1.394(2) ? C19A H19A . 0.9500 ? C20A H20A . 0.9800 ? C20A H20B . 0.9800 ? C20A H20C . 0.9800 ? S1B O1B . 1.4515(13) ? S1B O2B . 1.4466(13) ? S1B O3B . 1.4643(14) ? S1B C14B . 1.7831(17) ? C14B C15B . 1.394(3) ? C14B C19B . 1.395(3) ? C15B H15B . 0.9500 ? C15B C16B . 1.395(3) ? C16B H16B . 0.9500 ? C16B C17B . 1.385(3) ? C17B C18B . 1.396(3) ? C17B C20B . 1.517(3) ? C18B H18B . 0.9500 ? C18B C19B . 1.392(3) ? C19B H19B . 0.9500 ? C20B H20D . 0.9800 ? C20B H20E . 0.9800 ? C20B H20F . 0.9800 ? N1A N2A . 1.476(2) ? N1A C3A . 1.518(2) ? N1A C4A . 1.509(2) ? N1A C7A . 1.502(2) ? N2A C1A . 1.307(2) ? N3A H3AA . 0.8800 ? N3A H3AB . 0.8800 ? N3A C1A . 1.335(2) ? N4A C5A . 1.463(2) ? N4A C6A . 1.467(2) ? N4A C8A . 1.424(2) ? C1A C2A . 1.498(2) ? C2A H2AA . 0.9900 ? C2A H2AB . 0.9900 ? C2A C3A . 1.513(2) ? C3A H3AC . 0.9900 ? C3A H3AD . 0.9900 ? C4A H4AA . 0.9900 ? C4A H4AB . 0.9900 ? C4A C5A . 1.513(2) ? C5A H5AA . 0.9900 ? C5A H5AB . 0.9900 ? C6A H6AA . 0.9900 ? C6A H6AB . 0.9900 ? C6A C7A . 1.509(2) ? C7A H7AA . 0.9900 ? C7A H7AB . 0.9900 ? C8A C9A . 1.394(3) ? C8A C13A . 1.389(3) ? C9A H9A . 0.9500 ? C9A C10A . 1.382(3) ? C10A H10A . 0.9500 ? C10A C11A . 1.383(4) ? C11A H11A . 0.9500 ? C11A C12A . 1.380(4) ? C12A H12A . 0.9500 ? C12A C13A . 1.391(3) ? C13A H13A . 0.9500 ? N1B N2B . 1.472(2) ? N1B C3B . 1.519(2) ? N1B C4B . 1.508(2) ? N1B C7B . 1.501(2) ? N2B C1B . 1.309(2) ? N3B H3BA . 0.8800 ? N3B H3BB . 0.8800 ? N3B C1B . 1.334(2) ? N4B C5B . 1.469(2) ? N4B C6B . 1.466(2) ? N4B C8B . 1.416(2) ? C1B C2B . 1.498(3) ? C2B H2BA . 0.9900 ? C2B H2BB . 0.9900 ? C2B C3B . 1.515(3) ? C3B H3BC . 0.9900 ? C3B H3BD . 0.9900 ? C4B H4BA . 0.9900 ? C4B H4BB . 0.9900 ? C4B C5B . 1.512(2) ? C5B H5BA . 0.9900 ? C5B H5BB . 0.9900 ? C6B H6BA . 0.9900 ? C6B H6BB . 0.9900 ? C6B C7B . 1.512(2) ? C7B H7BA . 0.9900 ? C7B H7BB . 0.9900 ? C8B C9B . 1.396(3) ? C8B C13B . 1.398(3) ? C9B H9B . 0.9500 ? C9B C10B . 1.396(3) ? C10B H10B . 0.9500 ? C10B C11B . 1.371(3) ? C11B H11B . 0.9500 ? C11B C12B . 1.388(3) ? C12B H12B . 0.9500 ? C12B C13B . 1.381(3) ? C13B H13B . 0.9500 ? _cod_database_fobs_code 2022665