#------------------------------------------------------------------------------ #$Date: 2026-10-23 23:24:20 +0200 (Fri, 23 Oct 2026) $ #$Revision: 306996 $ #$URL: svn://www.crystallography.net/cod/cif/1/57/74/1577493.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1577493 loop_ _publ_author_name 'Kelani, Monsuru T.' 'Hosten, Eric C.' 'Muller, Alfred' 'Lammertsma, Koop' _publ_section_title ; Bis[(2-bromophenyl)dicyclohexylphosphane-\k2 Br,P]dichloridoruthenium(II) methanol 1.6-solvate ; _journal_coeditor_code BH4108 _journal_issue 10 _journal_name_full IUCrData _journal_paper_doi 10.1107/S2414314626010862 _journal_volume 11 _journal_year 2026 _chemical_formula_iupac '[Ru Cl2 (C18 H26 Br P)2], 1.6C H4 O' _chemical_formula_moiety 'C36 H52 Br2 Cl2 P2 Ru, 1.6(C H4 O)' _chemical_formula_sum 'C37.6 H58.4 Br2 Cl2 O1.6 P2 Ru' _chemical_formula_weight 929.77 _chemical_name_systematic 'Bis[(2-bromophenyl)dicyclohexylphosphane-\k^2^Br,P]dichloridoruthenium(II) methanol 1.6-solvate' _space_group_crystal_system monoclinic _space_group_IT_number 13 _space_group_name_Hall '-P 2yac' _space_group_name_H-M_alt 'P 1 2/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2025/1 _cell_angle_alpha 90 _cell_angle_beta 98.8370(10) _cell_angle_gamma 90 _cell_formula_units_Z 10 _cell_length_a 22.3929(8) _cell_length_b 10.2987(3) _cell_length_c 44.7559(16) _cell_measurement_reflns_used 7366 _cell_measurement_temperature 273(2) _cell_measurement_theta_max 22.41 _cell_measurement_theta_min 2.21 _cell_volume 10199.0(6) _computing_cell_refinement ; SAINT (Bruker, 2010) ; _computing_data_collection ; APEX2 (Bruker, 2010) ; _computing_data_reduction ; SAINT (Bruker, 2010) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012); Mercury (Macrae et al., 2020) ; _computing_publication_material ; PublCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 273(2) _diffrn_detector_area_resol_mean 8.3333 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_source 'sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1564 _diffrn_reflns_av_unetI/netI 0.1039 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_h_min -29 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 59 _diffrn_reflns_limit_l_min -57 _diffrn_reflns_number 199859 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.291 _diffrn_reflns_theta_min 1.538 _exptl_absorpt_coefficient_mu 2.582 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.6084 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.514 _exptl_crystal_description block _exptl_crystal_F_000 4748 _exptl_crystal_size_max 0.235 _exptl_crystal_size_mid 0.145 _exptl_crystal_size_min 0.132 _refine_diff_density_max 1.173 _refine_diff_density_min -1.289 _refine_ls_extinction_coef 0.00025(3) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL (Sheldrick, 2015b) ; _refine_ls_goodness_of_fit_ref 1.015 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1050 _refine_ls_number_reflns 25316 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.015 _refine_ls_R_factor_all 0.1242 _refine_ls_R_factor_gt 0.0564 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0383P)^2^+9.2315P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1020 _refine_ls_wR_factor_ref 0.1268 _reflns_number_gt 14549 _reflns_number_total 25316 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file bh4108.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'P 2/n' _cod_original_formula_sum 'C37.6 H58.4 Br2 Cl2 O1.6 P2 Ru1' _cod_database_code 1577493 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24.60 8 -12 4 32.00 29.70 8 -12 4 111.59 58.59 8 12 4 28.40 21.00 8 12 4 3.00 25.90 -8 12 -4 46.40 30.30 9 -12 4 130.69 58.89 9 -12 4 129.39 42.70 -9 -12 -4 136.29 46.20 9 12 4 103.49 42.10 -9 12 -4 120.39 43.40 -10 -12 -4 7.80 25.80 10 -12 4 6.80 26.20 10 -12 4 42.30 48.50 -10 12 -4 -2.50 26.10 10 12 4 1.20 29.70 11 -12 4 -10.60 28.50 -11 -12 -4 65.39 31.20 11 -12 4 -13.60 32.90 11 12 4 66.99 43.10 -11 12 -4 8.90 29.90 12 -12 4 -3.70 23.50 12 -12 4 -16.20 41.20 -12 12 -4 -14.10 25.70 12 12 4 23.90 44.40 13 -12 4 6.80 29.00 13 -12 4 -34.50 33.00 13 12 4 13.40 38.00 -13 12 -4 35.20 41.30 9 -13 -4 -26.50 25.80 -9 -13 4 19.80 31.10 9 13 -4 -39.40 18.60 -9 13 4 13.30 26.80 8 -13 -4 15.80 29.60 8 -13 -4 47.10 54.19 -8 -13 4 42.30 41.40 8 13 -4 2.20 35.30 -7 -13 4 24.20 34.40 7 -13 -4 62.09 54.79 7 -13 -4 34.70 30.10 -7 13 4 135.59 47.90 6 -13 -4 -10.50 31.10 -6 -13 4 -4.00 24.70 6 -13 -4 -38.80 16.60 -6 13 4 -7.40 21.50 6 13 -4 3.70 30.10 5 -13 -4 17.30 28.90 -5 -13 4 5.70 32.30 5 -13 -4 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21.70 11.10 7 0 -5 15.50 14.80 -7 0 5 7.40 8.80 7 0 -5 14.20 7.70 -7 0 5 10.70 12.90 7 0 -5 16.80 9.70 -7 0 5 21.40 10.40 6 0 -5 18.80 7.90 6 0 -5 14.50 8.40 6 0 -5 8.00 10.40 -6 0 5 -2.00 4.70 6 0 -5 8.10 5.50 -6 0 5 -2.30 10.00 6 0 -5 3.30 6.60 -6 0 5 3.90 6.40 -6 0 5 4.30 8.00 5 0 -5 411.16 31.00 5 0 -5 354.56 32.40 5 0 -5 428.56 47.00 -5 0 5 378.16 33.40 -5 0 5 448.06 32.10 -5 0 5 427.56 31.60 5 0 -5 446.06 30.70 5 0 -5 428.36 28.60 -5 0 5 434.46 54.09 4 0 -5 -0.80 3.80 -4 0 5 2.90 4.10 -4 0 5 2.60 4.60 -4 0 5 1.60 5.10 4 0 -5 -1.80 2.90 4 0 -5 -1.10 4.70 4 0 -5 6.60 8.60 -4 0 5 -2.10 4.70 -4 0 5 -0.90 6.60 4 0 -5 8.00 4.40 3 0 -5 580.44 42.40 -3 0 5 579.44 34.10 3 0 -5 553.14 36.40 -3 0 5 623.54 42.30 3 0 -5 532.65 33.50 -3 0 5 533.85 34.50 3 0 -5 555.64 34.40 -3 0 5 588.34 39.60 3 0 -5 587.34 39.40 -2 0 5 5.20 5.10 2 0 -5 -4.40 3.10 2 0 -5 -2.90 3.70 -2 0 5 1.60 2.90 2 0 -5 0.60 2.40 -2 0 5 1.90 4.50 -2 0 5 -2.10 1.90 1 0 -5 10.30 4.00 -1 0 5 12.90 3.60 1 0 -5 16.30 5.30 -1 0 5 16.70 5.70 1 0 -5 8.20 5.30 0 0 -5 11.40 5.40 0 0 -5 7.70 3.70 0 0 5 6.30 3.20 0 0 5 1.20 2.80 0 0 5 7.10 4.30 -1 0 -5 710.73 43.70 1 0 5 794.32 46.10 -1 0 -5 756.92 45.70 1 0 5 814.72 44.40 1 0 5 721.13 44.90 -1 0 -5 760.52 45.90 -1 0 -5 802.42 45.80 -2 0 -5 10.50 5.80 -2 0 -5 2.40 3.60 2 0 5 4.90 4.80 -2 0 -5 -1.30 3.40 2 0 5 -2.50 3.60 2 0 5 3.70 4.50 2 0 5 -1.80 3.00 -2 0 -5 -0.20 4.30 3 0 5 91.39 16.30 -3 0 -5 103.79 15.50 3 0 5 110.09 17.20 -3 0 -5 121.19 14.30 -3 0 -5 105.89 17.40 3 0 5 123.69 15.00 -3 0 -5 151.58 20.30 3 0 5 123.59 14.80 -4 0 -5 8.80 5.60 4 0 5 6.40 7.70 -4 0 -5 -2.80 5.80 4 0 5 1.60 4.20 -4 0 -5 9.20 8.50 -4 0 -5 12.70 7.20 4 0 5 1.70 6.30 4 0 5 0.00 4.70 -5 0 -5 1372.26 87.49 5 0 5 1371.56 79.49 5 0 5 1331.77 82.29 -5 0 -5 1308.47 79.49 5 0 5 1328.57 88.09 -5 0 -5 1427.56 90.39 5 0 5 1389.26 87.29 -5 0 -5 1395.06 80.19 6 0 5 -1.80 5.20 -6 0 -5 -2.10 5.20 6 0 5 6.50 6.20 6 0 5 1.60 9.00 6 0 5 -1.60 5.60 6 0 5 7.00 8.70 -6 0 -5 -2.50 7.00 -6 0 -5 7.00 11.00 -6 0 -5 2.20 5.10 -7 0 -5 469.85 49.10 -7 0 -5 388.46 33.30 7 0 5 384.46 32.90 7 0 5 494.85 42.90 7 0 5 412.56 33.40 -7 0 -5 423.16 33.90 7 0 5 408.56 54.89 7 0 5 401.26 33.10 -7 0 -5 378.26 50.29 -8 0 -5 -22.60 7.70 8 0 5 -3.20 6.70 8 0 5 -0.80 6.80 -8 0 -5 5.30 7.30 8 0 5 -3.50 6.60 -8 0 -5 1.10 6.70 8 0 5 2.10 11.60 -8 0 -5 -4.80 7.40 8 0 5 28.80 14.80 9 0 5 7.90 11.50 9 0 5 -0.50 5.60 -9 0 -5 7.20 13.00 9 0 5 12.20 9.90 9 0 5 27.70 11.10 -9 0 -5 -0.90 12.30 -9 0 -5 -3.10 8.10 9 0 5 6.20 15.00 -10 0 -5 -5.40 10.70 10 0 5 11.90 17.00 10 0 5 -13.00 7.30 -10 0 -5 7.90 15.90 -10 0 -5 -1.10 8.50 10 0 5 3.10 10.00 10 0 5 5.70 11.10 10 0 5 4.00 8.30 -11 0 -5 1833.62 140.99 -11 0 -5 1915.71 142.79 11 0 5 1783.22 116.49 11 0 5 2021.50 139.89 -11 0 -5 2001.60 120.99 11 0 5 2014.10 118.99 11 0 5 2024.60 130.99 -12 0 -5 15.50 15.90 12 0 5 11.20 18.90 12 0 5 11.80 11.10 12 0 5 14.10 14.20 -12 0 -5 29.70 19.90 -12 0 -5 3.70 11.60 12 0 5 -15.60 9.00 12 0 5 -9.40 10.90 -13 0 -5 807.92 89.99 13 0 5 742.83 60.69 13 0 5 735.33 61.39 13 0 5 897.81 98.39 -13 0 -5 851.21 108.99 13 0 5 891.21 64.79 14 0 5 34.30 26.60 14 0 5 14.00 12.70 14 0 5 2.10 9.00 14 0 5 13.20 13.00 14 0 5 -0.90 13.90 -14 0 -5 -1.20 16.20 -15 0 -5 -7.10 16.10 15 0 5 5.90 16.40 15 0 5 8.20 16.40 15 0 5 2.70 13.10 15 0 5 12.20 11.70 15 0 5 -1.70 16.40 16 0 5 -5.70 12.40 16 0 5 20.30 14.80 16 0 5 -13.60 20.30 16 0 5 -4.50 8.60 -16 0 -5 6.30 20.10 17 0 5 51.59 30.70 17 0 5 10.90 12.90 17 0 5 -0.60 12.90 -17 0 -5 12.90 24.20 17 0 5 12.50 14.20 18 0 5 -14.50 15.40 18 0 5 -2.10 14.00 -18 0 -5 -12.20 17.80 18 0 5 -18.70 22.90 19 0 5 4.80 13.60 19 0 5 8.00 18.30 19 0 5 57.19 36.00 19 0 5 40.50 22.20 -19 0 -5 20.20 26.60 20 0 5 -7.40 30.90 20 0 5 34.50 20.50 20 0 5 -29.70 16.30 20 0 5 2.70 12.90 -20 0 -5 -32.30 13.00 21 0 5 325.37 78.99 -21 0 -5 192.28 57.29 21 0 5 232.28 42.70 21 0 5 259.67 47.30 21 0 5 216.18 40.50 22 0 5 82.19 48.30 22 0 5 -3.50 22.90 -22 0 -5 21.60 31.60 22 0 5 0.30 15.60 22 0 5 -5.40 11.40 23 0 5 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7 4 -28 51.29 16.80 -7 4 28 22.50 19.50 -7 4 28 69.89 19.70 -6 -4 28 -11.60 15.20 -6 -4 28 5.70 13.80 -6 -4 28 1.60 11.00 -6 4 28 9.00 23.30 6 4 -28 -9.40 7.10 6 4 -28 12.20 21.60 -6 4 28 10.80 12.70 -6 4 28 8.50 15.00 -6 4 28 12.50 15.70 -5 -4 28 429.96 46.20 -5 -4 28 455.25 54.99 -5 -4 28 483.55 74.39 5 4 -28 387.66 43.30 -5 4 28 487.35 58.49 -5 4 28 434.96 77.19 -5 4 28 404.06 43.40 5 4 -28 328.77 62.39 -5 4 28 318.57 47.50 -4 -4 28 260.67 36.40 -4 -4 28 264.57 41.10 -4 -4 28 182.68 48.30 -4 4 28 257.17 43.50 -4 4 28 237.78 31.40 -4 4 28 205.28 49.90 4 4 -28 216.98 46.70 -3 -4 28 43.90 17.20 -3 -4 28 52.59 30.90 -3 -4 28 69.19 22.50 -3 4 28 54.39 30.90 -3 4 28 70.79 25.00 -3 4 28 50.19 17.00 3 4 -28 59.79 28.30 -2 -4 28 37.50 25.00 -2 -4 28 10.40 16.50 -2 -4 28 30.40 15.20 -2 4 28 25.40 18.90 -2 4 28 46.10 16.20 2 4 -28 17.30 19.70 -2 4 28 56.89 21.60 -1 -4 28 54.09 30.90 -1 -4 28 42.00 19.60 -1 -4 28 67.59 23.70 -1 4 28 68.79 31.10 1 4 -28 118.29 34.60 -1 4 28 106.59 27.90 -1 4 28 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21 -5 -28 0.60 27.10 -21 -5 28 30.00 29.50 -21 -5 28 -2.40 21.60 -21 5 28 3.90 28.60 21 5 -28 -3.10 45.50 -21 5 28 -3.00 37.40 21 5 -28 -11.10 10.70 20 -5 -28 -36.60 18.30 -20 -5 28 2.00 25.20 -20 -5 28 58.69 36.80 -20 5 28 -10.10 25.00 -20 5 28 -9.50 22.90 20 5 -28 -6.90 37.40 20 5 -28 5.40 12.00 19 -5 -28 10.60 34.20 -19 -5 28 8.80 23.60 -19 -5 28 40.60 28.80 19 5 -28 -6.20 38.20 -19 5 28 -10.80 21.50 -19 5 28 -6.90 29.20 19 5 -28 -3.40 10.40 -18 -5 28 157.18 50.79 18 -5 -28 230.88 58.09 -18 -5 28 139.79 42.40 -18 5 28 163.78 46.90 -18 5 28 144.19 49.90 18 5 -28 125.09 19.80 -18 5 28 131.59 58.99 18 5 -28 120.49 22.60 18 5 -28 136.69 58.99 -17 -5 28 131.09 42.80 -17 -5 28 55.89 32.20 17 -5 -28 44.40 36.60 -17 5 28 0.20 28.40 17 5 -28 115.99 54.19 -17 5 28 121.39 51.19 17 5 -28 102.89 21.60 17 5 -28 83.19 16.60 -17 5 28 42.50 35.40 16 -5 -28 70.39 38.80 -16 -5 28 83.99 32.00 -16 -5 28 60.49 36.60 16 5 -28 62.99 17.50 16 5 -28 78.79 16.20 16 5 -28 109.19 55.09 -16 5 28 47.00 27.50 -16 5 28 -5.20 27.10 15 -5 -28 135.69 46.70 -15 -5 28 67.29 29.80 -15 -5 28 195.78 53.89 -15 5 28 217.38 64.79 -15 5 28 111.19 33.50 15 5 -28 85.79 53.49 -15 5 28 193.58 53.19 15 5 -28 161.18 26.10 15 5 -28 156.08 22.20 -14 -5 28 20.60 25.40 -14 -5 28 87.49 32.40 14 -5 -28 44.60 36.80 -14 5 28 104.29 41.70 14 5 -28 118.99 51.49 -14 5 28 84.19 28.90 14 5 -28 49.10 14.20 14 5 -28 87.09 20.90 -14 5 28 43.00 33.40 -13 -5 28 201.18 27.10 -13 -5 28 268.87 59.19 13 -5 -28 179.88 52.29 -13 -5 28 198.08 40.90 13 5 -28 172.78 24.20 -13 5 28 179.38 47.20 13 5 -28 183.78 30.20 -13 5 28 206.98 62.59 -13 5 28 169.48 35.40 13 5 -28 113.79 51.39 -13 5 28 181.68 50.29 -12 -5 28 328.17 34.90 -12 -5 28 347.67 72.19 12 -5 -28 444.06 77.99 -12 -5 28 314.47 53.79 -12 5 28 357.76 46.40 -12 5 28 379.86 60.49 12 5 -28 385.06 43.20 -12 5 28 640.34 103.29 -12 5 28 516.35 76.29 12 5 -28 286.77 70.79 12 5 -28 351.06 35.60 11 -5 -28 56.89 32.80 -11 -5 28 12.10 17.80 -11 -5 28 8.20 11.10 -11 -5 28 32.10 25.60 -11 5 28 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32.80 30.80 -19 6 28 59.89 50.29 19 6 -28 37.10 45.80 -18 -6 28 -3.20 22.60 -18 -6 28 23.30 23.90 18 -6 -28 -13.60 22.50 -18 6 28 24.20 33.20 18 6 -28 -38.50 25.10 -18 6 28 44.90 34.70 -17 -6 28 55.89 30.00 -17 -6 28 15.40 27.00 17 -6 -28 -8.00 32.00 -17 6 28 -34.60 16.60 -17 6 28 -31.90 16.70 17 6 -28 -33.00 25.60 -17 6 28 35.30 31.60 16 -6 -28 44.40 36.70 -16 -6 28 80.59 40.00 -16 -6 28 33.00 24.60 16 6 -28 95.69 54.39 -16 6 28 76.79 39.80 -16 6 28 -18.80 21.20 -16 6 28 45.90 26.90 -15 -6 28 137.59 47.20 15 -6 -28 134.49 46.70 -15 6 28 180.48 59.09 -15 6 28 58.19 28.80 -15 6 28 139.29 48.40 15 6 -28 14.60 30.00 14 -6 -28 148.49 81.39 -14 -6 28 138.79 48.30 14 6 -28 131.49 16.70 -14 6 28 139.99 46.10 -14 6 28 190.68 99.79 -14 6 28 128.59 37.30 14 6 -28 145.79 16.20 14 6 -28 78.89 49.10 13 -6 -28 68.19 38.30 -13 -6 28 125.59 45.10 -13 -6 28 122.09 43.90 -13 6 28 187.58 52.29 -13 6 28 145.39 55.39 13 6 -28 64.49 41.70 13 6 -28 145.39 20.10 -13 6 28 177.38 38.60 13 6 -28 155.68 18.30 -12 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6 28 275.77 69.09 -8 6 28 224.38 43.00 -7 -6 28 21.60 25.70 -7 -6 28 13.90 19.50 7 -6 -28 -2.50 22.00 -7 -6 28 25.90 13.50 -7 6 28 38.80 15.70 -7 6 28 39.30 24.60 7 6 -28 13.20 28.50 7 6 -28 53.29 15.80 -7 6 28 3.20 19.80 -7 6 28 17.10 25.90 -6 -6 28 129.09 44.90 -6 -6 28 131.29 23.50 -6 -6 28 142.69 31.60 6 -6 -28 111.79 38.60 -6 6 28 30.80 24.80 6 6 -28 143.79 24.90 6 6 -28 138.89 46.70 -6 6 28 170.58 25.10 -6 6 28 127.19 30.90 -6 6 28 112.29 46.00 6 6 -28 149.49 39.00 -5 -6 28 158.58 27.90 5 -6 -28 113.29 41.80 -5 -6 28 179.18 36.20 -5 -6 28 132.59 44.90 5 6 -28 142.09 25.50 5 6 -28 108.99 41.60 -5 6 28 126.99 35.10 -5 6 28 174.48 49.70 5 6 -28 157.38 39.30 -5 6 28 167.28 32.60 -5 6 28 190.88 26.20 -4 -6 28 46.60 21.60 -4 -6 28 162.18 48.40 -4 -6 28 77.89 21.00 4 -6 -28 65.39 32.60 4 6 -28 43.90 26.70 -4 6 28 43.00 15.50 -4 6 28 29.00 31.60 4 6 -28 99.09 40.60 -4 6 28 53.49 25.40 -4 6 28 93.49 23.90 -3 -6 28 970.60 121.09 -3 -6 28 951.30 77.89 -3 -6 28 928.41 69.89 3 6 -28 1125.49 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26.10 3 -6 28 2.60 28.10 3 -6 28 35.30 21.30 3 -6 28 26.50 19.60 3 6 28 56.69 20.80 3 6 28 43.40 23.60 3 6 28 3.90 14.60 3 6 28 52.39 30.60 -3 6 -28 65.29 30.70 4 -6 28 107.89 31.90 4 -6 28 120.69 32.30 4 -6 28 128.99 49.00 4 6 28 99.59 29.70 4 6 28 165.68 42.90 4 6 28 67.29 24.00 4 6 28 60.09 23.70 -4 6 -28 105.79 40.00 5 -6 28 -11.90 14.80 5 -6 28 -18.70 15.00 5 -6 28 46.00 38.50 -5 6 -28 -2.70 22.50 5 6 28 -4.50 18.40 5 6 28 7.60 19.20 5 6 28 -8.20 11.90 5 6 28 13.30 21.40 6 -6 28 57.39 39.30 6 -6 28 40.00 26.00 6 6 28 46.40 22.70 6 6 28 28.90 23.40 -6 6 -28 19.70 28.70 6 6 28 74.49 28.40 6 6 28 77.19 30.80 7 -6 28 7.40 18.60 7 -6 28 3.40 26.60 -7 -6 -28 8.70 14.10 7 -6 28 42.80 27.40 7 6 28 3.60 15.90 7 6 28 -13.80 14.40 7 6 28 -20.00 11.70 7 6 28 24.00 23.80 -7 6 -28 11.40 25.90 8 -6 28 276.17 50.09 8 -6 28 232.68 67.89 8 -6 28 260.97 47.70 -8 -6 -28 283.87 43.40 8 6 28 199.08 43.00 8 6 28 260.97 45.90 -8 6 -28 212.58 56.49 8 6 28 171.78 43.10 8 6 28 189.08 39.90 9 -6 28 -8.00 18.30 9 -6 28 42.10 27.00 9 -6 28 26.60 35.20 -9 -6 -28 30.70 18.00 -9 -6 -28 33.20 19.20 9 6 28 40.50 23.00 -9 6 -28 77.59 40.20 9 6 28 15.80 19.00 9 6 28 50.09 29.30 9 6 28 17.90 22.00 -10 -6 -28 27.50 16.90 10 -6 28 -28.70 17.60 10 -6 28 -24.30 15.20 10 -6 28 -6.10 29.10 -10 -6 -28 11.00 11.80 10 6 28 20.20 23.00 10 6 28 18.20 15.20 10 6 28 49.30 26.30 -10 6 -28 19.00 31.50 11 -6 28 7.30 27.90 11 -6 28 8.70 32.80 -11 -6 -28 18.60 11.70 11 -6 28 5.90 21.70 -11 -6 -28 62.79 19.90 -11 6 -28 87.99 41.10 11 6 28 27.20 24.30 11 6 28 15.00 21.80 11 6 28 15.10 23.70 11 6 28 -16.60 21.20 12 -6 28 18.20 35.40 12 -6 28 -2.10 23.10 12 -6 28 -8.80 21.70 -12 6 -28 58.89 36.80 12 6 28 56.19 28.80 12 6 28 22.00 28.40 12 6 28 80.69 33.30 13 -6 28 58.39 32.80 13 -6 28 85.69 35.20 13 6 28 54.79 34.90 13 6 28 35.10 26.40 -13 6 -28 32.30 33.30 13 6 28 26.70 25.20 14 -6 28 -32.00 19.80 14 -6 28 -38.40 16.00 14 -6 28 1.90 28.70 14 6 28 4.00 32.20 -14 6 -28 -10.60 27.60 14 6 28 23.20 23.90 14 6 28 22.60 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38.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 77736 _shelx_res_file ; TITL shelxt_a.res in P2/n 23mt_RupdcycBrhex.res created by SHELXL-2025/1 at 16:52:45 on 28-Jul-2026 CELL 0.71073 22.3929 10.2987 44.7559 90.000 98.837 90.000 ZERR 2.00 0.0008 0.0003 0.0016 0.000 0.001 0.000 LATT 1 SYMM 1/2 - X, Y, 1/2 - Z SFAC C H Br Cl Ru P O UNIT 376 584 20 20 10 20 16 OMIT 0 1 1 EQIV $1 1/2-x,y,3/2-z HTAB O1 Cl2 HTAB O2 O1 HTAB O3 Cl1 HTAB O4 O2 HTAB C6 Cl2 HTAB C11 Cl5_$1 HTAB C20 Cl1 HTAB C24 Br1 HTAB C26 Cl2 HTAB C30 Br2 HTAB C36 Cl1 HTAB C42 Cl4 HTAB C56 Cl3 HTAB C60 Br3 HTAB C62 Cl4 HTAB C66 Br4 HTAB C68 Cl3 HTAB C78 Cl5 HTAB C90 Cl5_$1 ACTA BOND $H CONF FMAP 2 HTAB L.S. 20 LIST 4 PLAN 20 TEMP 0 REM WGHT 0.038300 9.245200 REM WGHT 0.038300 9.203100 REM WGHT 0.038300 9.240200 REM WGHT 0.038300 9.203100 WGHT 0.038300 9.231500 EXTI 0.000251 FVAR 0.14648 RU1 5 0.455031 0.706387 0.625670 11.00000 0.02840 0.02407 = 0.02875 -0.00126 0.00281 0.00062 RU2 5 0.903810 0.230918 0.606243 11.00000 0.03508 0.02670 = 0.02883 0.00085 0.00984 0.00205 RU3 5 0.250000 0.085485 0.750000 10.50000 0.03638 0.03878 = 0.03814 0.00000 0.00280 0.00000 BR1 3 0.419055 0.516680 0.652683 11.00000 0.04621 0.02637 = 0.04115 0.00151 0.00171 -0.00556 BR2 3 0.356080 0.809782 0.631612 11.00000 0.03559 0.03586 = 0.04231 -0.00807 0.00525 0.00538 BR3 3 0.815230 0.081289 0.592289 11.00000 0.04283 0.03929 = 0.04548 -0.00654 0.01395 -0.00349 BR4 3 0.851759 0.380664 0.566010 11.00000 0.04464 0.03504 = 0.03878 0.00192 0.00901 0.01057 BR5 3 0.300472 -0.097851 0.725606 11.00000 0.04040 0.05349 = 0.04702 0.00073 0.00359 0.01019 CL1 4 0.545838 0.600563 0.617262 11.00000 0.03416 0.05502 = 0.04447 -0.01029 0.00344 0.00932 CL2 4 0.489758 0.893860 0.602032 11.00000 0.05459 0.03741 = 0.03553 0.00352 0.00560 -0.01077 CL3 4 0.955021 0.081313 0.642069 11.00000 0.05134 0.04131 = 0.03380 0.00713 0.01049 0.01036 CL4 4 0.985660 0.378630 0.620057 11.00000 0.05020 0.04110 = 0.04093 -0.00650 0.01266 -0.00892 CL5 4 0.197310 0.252784 0.771834 11.00000 0.06560 0.06109 = 0.05747 -0.01214 0.00123 0.02339 P1 6 0.399513 0.637399 0.578725 11.00000 0.02930 0.02956 = 0.03193 -0.00284 0.00197 0.00224 P2 6 0.500361 0.766829 0.675280 11.00000 0.03263 0.02285 = 0.03046 -0.00075 0.00378 0.00002 P3 6 0.951165 0.154270 0.566222 11.00000 0.03257 0.02590 = 0.02887 0.00043 0.00848 0.00245 P4 6 0.844647 0.305656 0.642765 11.00000 0.03839 0.02956 = 0.03319 0.00127 0.01266 0.00472 P5 6 0.183522 0.072265 0.702759 11.00000 0.03226 0.04048 = 0.03962 0.00472 0.00256 0.00148 O1 7 0.566644 0.779806 0.552102 11.00000 0.20464 0.14383 = 0.12385 0.05359 0.10216 0.07772 AFIX 147 H1 2 0.550219 0.787057 0.567178 11.00000 -1.50000 AFIX 0 O2 7 0.640157 0.585594 0.537650 11.00000 0.12958 0.15482 = 0.10291 0.01337 0.04488 0.03196 AFIX 147 H2 2 0.646819 0.663398 0.540235 11.00000 -1.50000 AFIX 0 O3 7 0.683087 0.707913 0.637102 11.00000 0.08126 0.22291 = 0.20258 -0.01718 0.01241 -0.01390 AFIX 147 H3 2 0.649325 0.675398 0.633465 11.00000 -1.50000 AFIX 0 O4 7 0.727164 0.611968 0.501364 11.00000 0.19848 0.16265 = 0.14715 -0.04012 0.08160 -0.02974 AFIX 147 H4 2 0.691889 0.630702 0.495053 11.00000 -1.50000 AFIX 0 C1 1 0.388751 0.749988 0.545674 11.00000 0.03496 0.03713 = 0.03096 0.00114 0.00174 -0.00497 AFIX 13 H1A 2 0.429133 0.776049 0.542076 11.00000 -1.20000 AFIX 0 C2 1 0.356480 0.690504 0.516015 11.00000 0.05797 0.04517 = 0.04048 -0.00647 -0.00074 0.00353 AFIX 23 H2A 2 0.378430 0.614170 0.511112 11.00000 -1.20000 H2B 2 0.316154 0.663409 0.518692 11.00000 -1.20000 AFIX 0 C3 1 0.352135 0.786945 0.490003 11.00000 0.07997 0.07759 = 0.03201 0.00066 -0.00115 0.00271 AFIX 23 H3A 2 0.392483 0.807348 0.486049 11.00000 -1.20000 H3B 2 0.330097 0.747460 0.471924 11.00000 -1.20000 AFIX 0 C4 1 0.320667 0.911155 0.496800 11.00000 0.07528 0.05669 = 0.04126 0.01492 -0.00315 -0.01116 AFIX 23 H4A 2 0.278731 0.892828 0.498276 11.00000 -1.20000 H4B 2 0.321561 0.972531 0.480435 11.00000 -1.20000 AFIX 0 C5 1 0.351407 0.970138 0.526169 11.00000 0.06485 0.04040 = 0.05219 0.00920 -0.00085 -0.00413 AFIX 23 H5A 2 0.328942 1.046100 0.530833 11.00000 -1.20000 H5B 2 0.391744 0.998109 0.523738 11.00000 -1.20000 AFIX 0 C6 1 0.355710 0.874145 0.552500 11.00000 0.05221 0.03923 = 0.03591 0.00172 -0.00418 -0.00325 AFIX 23 H6A 2 0.315365 0.852321 0.556230 11.00000 -1.20000 H6B 2 0.377131 0.914454 0.570625 11.00000 -1.20000 AFIX 0 C7 1 0.451826 0.697283 0.700835 11.00000 0.03033 0.03256 = 0.03635 0.00191 0.00519 0.00417 C8 1 0.451021 0.740985 0.730395 11.00000 0.03893 0.04180 = 0.04196 0.00155 0.00940 0.00458 AFIX 43 H8 2 0.472478 0.815312 0.737213 11.00000 -1.20000 AFIX 0 C9 1 0.418609 0.674797 0.749650 11.00000 0.06037 0.05986 = 0.03724 0.00495 0.01745 0.01121 AFIX 43 H9 2 0.418133 0.705871 0.769122 11.00000 -1.20000 AFIX 0 C10 1 0.387427 0.564536 0.740280 11.00000 0.05551 0.05620 = 0.05757 0.02589 0.02333 0.00359 AFIX 43 H10 2 0.366098 0.520622 0.753422 11.00000 -1.20000 AFIX 0 C11 1 0.387453 0.518082 0.711404 11.00000 0.05496 0.03525 = 0.04496 0.00845 0.01108 -0.00529 AFIX 43 H11 2 0.366251 0.443249 0.704735 11.00000 -1.20000 AFIX 0 C12 1 0.419717 0.585585 0.692774 11.00000 0.03649 0.03675 = 0.03525 0.00812 0.00429 0.00065 C13 1 0.321213 0.616825 0.586110 11.00000 0.03215 0.02498 = 0.03401 0.00631 0.00059 0.00238 C14 1 0.279780 0.527635 0.571088 11.00000 0.03379 0.03756 = 0.04335 0.00163 0.00250 0.00073 AFIX 43 H14 2 0.291481 0.474357 0.556239 11.00000 -1.20000 AFIX 0 C15 1 0.221784 0.517432 0.577954 11.00000 0.03316 0.04743 = 0.05277 0.00204 -0.00549 -0.01242 AFIX 43 H15 2 0.195128 0.456705 0.567977 11.00000 -1.20000 AFIX 0 C16 1 0.203520 0.597009 0.599517 11.00000 0.03209 0.07617 = 0.06182 0.00151 0.00851 -0.00764 AFIX 43 H16 2 0.164149 0.591121 0.603637 11.00000 -1.20000 AFIX 0 C17 1 0.242721 0.685193 0.615069 11.00000 0.03694 0.05586 = 0.05190 -0.00185 0.01119 0.00340 AFIX 43 H17 2 0.230678 0.738451 0.629833 11.00000 -1.20000 AFIX 0 C18 1 0.300451 0.691983 0.608040 11.00000 0.02995 0.03437 = 0.04057 0.00246 -0.00282 -0.00245 C19 1 0.415845 0.478878 0.562176 11.00000 0.04080 0.03477 = 0.04040 -0.01499 -0.00165 0.00269 AFIX 13 H19 2 0.381884 0.458337 0.546329 11.00000 -1.20000 AFIX 0 C20 1 0.473201 0.484939 0.547215 11.00000 0.04064 0.07804 = 0.05003 -0.02694 0.00141 0.01585 AFIX 23 H20A 2 0.469219 0.552989 0.532055 11.00000 -1.20000 H20B 2 0.507984 0.504483 0.562289 11.00000 -1.20000 AFIX 0 C21 1 0.481993 0.353505 0.532449 11.00000 0.07673 0.10563 = 0.07086 -0.04199 -0.00587 0.04048 AFIX 23 H21A 2 0.449060 0.339149 0.515999 11.00000 -1.20000 H21B 2 0.519361 0.355107 0.523995 11.00000 -1.20000 AFIX 0 C22 1 0.484081 0.243868 0.554509 11.00000 0.11953 0.07224 = 0.10350 -0.04646 -0.03092 0.05554 AFIX 23 H22A 2 0.520184 0.252008 0.569434 11.00000 -1.20000 H22B 2 0.486629 0.162427 0.543891 11.00000 -1.20000 AFIX 0 C23 1 0.429112 0.240981 0.570512 11.00000 0.10089 0.03529 = 0.09370 -0.01846 -0.02082 0.01989 AFIX 23 H23A 2 0.393428 0.221287 0.556024 11.00000 -1.20000 H23B 2 0.433972 0.173052 0.585705 11.00000 -1.20000 AFIX 0 C24 1 0.420771 0.369699 0.585358 11.00000 0.05824 0.03789 = 0.05568 -0.00874 -0.00911 0.00207 AFIX 23 H24A 2 0.454827 0.385897 0.601104 11.00000 -1.20000 H24B 2 0.384418 0.367173 0.594663 11.00000 -1.20000 AFIX 0 C25 1 0.507418 0.940722 0.685287 11.00000 0.04921 0.02512 = 0.02920 -0.00289 0.00047 -0.00434 AFIX 13 H25 2 0.514951 0.946618 0.707400 11.00000 -1.20000 AFIX 0 C26 1 0.561421 1.002144 0.673512 11.00000 0.05691 0.03732 = 0.04652 -0.00181 0.00185 -0.01257 AFIX 23 H26A 2 0.598052 0.955925 0.681678 11.00000 -1.20000 H26B 2 0.556035 0.995224 0.651648 11.00000 -1.20000 AFIX 0 C27 1 0.567508 1.144179 0.682675 11.00000 0.07587 0.03464 = 0.07852 0.00695 -0.00882 -0.01352 AFIX 23 H27A 2 0.600960 1.182748 0.674410 11.00000 -1.20000 H27B 2 0.576171 1.150618 0.704535 11.00000 -1.20000 AFIX 0 C28 1 0.509635 1.218131 0.671207 11.00000 0.10157 0.02891 = 0.10810 0.01171 -0.03420 -0.01248 AFIX 23 H28A 2 0.514132 1.307870 0.677747 11.00000 -1.20000 H28B 2 0.502701 1.217109 0.649275 11.00000 -1.20000 AFIX 0 C29 1 0.456116 1.159332 0.682753 11.00000 0.08294 0.03341 = 0.07445 -0.00937 -0.01479 0.01687 AFIX 23 H29A 2 0.419736 1.205642 0.674242 11.00000 -1.20000 H29B 2 0.461143 1.168208 0.704573 11.00000 -1.20000 AFIX 0 C30 1 0.449328 1.015807 0.674283 11.00000 0.04988 0.02985 = 0.04220 -0.00063 0.00122 0.00942 AFIX 23 H30A 2 0.439430 1.007654 0.652492 11.00000 -1.20000 H30B 2 0.416365 0.978711 0.683207 11.00000 -1.20000 AFIX 0 C31 1 0.574744 0.698340 0.691822 11.00000 0.03292 0.02950 = 0.03621 -0.00144 -0.00105 -0.00053 AFIX 13 H31 2 0.603071 0.721287 0.678016 11.00000 -1.20000 AFIX 0 C32 1 0.602408 0.749376 0.723256 11.00000 0.05388 0.03975 = 0.04075 -0.00916 -0.01052 0.00140 AFIX 23 H32A 2 0.604577 0.843393 0.722686 11.00000 -1.20000 H32B 2 0.576538 0.725448 0.737875 11.00000 -1.20000 AFIX 0 C33 1 0.665979 0.693857 0.733270 11.00000 0.05096 0.07082 = 0.06930 -0.00876 -0.01907 -0.00117 AFIX 23 H33A 2 0.692828 0.723712 0.719639 11.00000 -1.20000 H33B 2 0.681604 0.724829 0.753425 11.00000 -1.20000 AFIX 0 C34 1 0.664250 0.546469 0.733252 11.00000 0.05788 0.07222 = 0.08457 -0.00231 -0.02811 0.02024 AFIX 23 H34A 2 0.705020 0.513019 0.738434 11.00000 -1.20000 H34B 2 0.640894 0.516711 0.748472 11.00000 -1.20000 AFIX 0 C35 1 0.636567 0.494596 0.702810 11.00000 0.05073 0.04743 = 0.08061 -0.00584 -0.01004 0.01776 AFIX 23 H35A 2 0.634479 0.400625 0.703693 11.00000 -1.20000 H35B 2 0.661906 0.517693 0.687890 11.00000 -1.20000 AFIX 0 C36 1 0.573561 0.549260 0.693304 11.00000 0.04234 0.03055 = 0.04638 0.00309 -0.00224 0.00615 AFIX 23 H36A 2 0.547663 0.522141 0.707648 11.00000 -1.20000 H36B 2 0.556819 0.514883 0.673615 11.00000 -1.20000 AFIX 0 C37 1 1.016299 0.246339 0.555048 11.00000 0.02927 0.02766 = 0.02671 0.00586 0.00318 0.00508 AFIX 13 H37 2 1.047546 0.250198 0.572942 11.00000 -1.20000 AFIX 0 C38 1 1.045179 0.183029 0.529853 11.00000 0.04544 0.03113 = 0.04077 -0.00033 0.01690 0.00216 AFIX 23 H38A 2 1.056036 0.094136 0.535431 11.00000 -1.20000 H38B 2 1.016035 0.181039 0.511430 11.00000 -1.20000 AFIX 0 C39 1 1.101273 0.256118 0.524028 11.00000 0.04192 0.04542 = 0.04744 -0.00213 0.02257 0.00180 AFIX 23 H39A 2 1.131946 0.250514 0.541816 11.00000 -1.20000 H39B 2 1.117213 0.215437 0.507365 11.00000 -1.20000 AFIX 0 C40 1 1.087900 0.398014 0.516536 11.00000 0.04840 0.04493 = 0.04524 0.00142 0.01895 -0.01066 AFIX 23 H40A 2 1.062144 0.404486 0.497082 11.00000 -1.20000 H40B 2 1.125347 0.443355 0.515157 11.00000 -1.20000 AFIX 0 C41 1 1.056645 0.461563 0.540768 11.00000 0.04254 0.03152 = 0.05072 0.00117 0.00833 -0.00293 AFIX 23 H41A 2 1.045455 0.549783 0.534710 11.00000 -1.20000 H41B 2 1.084589 0.465503 0.559590 11.00000 -1.20000 AFIX 0 C42 1 1.000242 0.386793 0.545843 11.00000 0.03735 0.03552 = 0.03545 0.00174 0.00611 0.00052 AFIX 23 H42A 2 0.971093 0.387412 0.527416 11.00000 -1.20000 H42B 2 0.981945 0.428867 0.561588 11.00000 -1.20000 AFIX 0 C43 1 0.765273 0.279451 0.626027 11.00000 0.04410 0.04281 = 0.03299 0.01184 0.01101 0.01128 C44 1 0.716458 0.346603 0.634696 11.00000 0.04848 0.05947 = 0.05214 0.00703 0.01530 0.01596 AFIX 43 H44 2 0.723657 0.417168 0.647718 11.00000 -1.20000 AFIX 0 C45 1 0.657907 0.309787 0.624237 11.00000 0.04160 0.08441 = 0.06700 0.00892 0.01446 0.02983 AFIX 43 H45 2 0.626143 0.357091 0.629961 11.00000 -1.20000 AFIX 0 C46 1 0.645577 0.204775 0.605557 11.00000 0.03763 0.10007 = 0.07185 0.00520 0.00001 0.00584 AFIX 43 H46 2 0.605821 0.178452 0.599540 11.00000 -1.20000 AFIX 0 C47 1 0.692249 0.138166 0.595691 11.00000 0.04160 0.07018 = 0.04772 0.00628 -0.00023 -0.00439 AFIX 43 H47 2 0.684541 0.068475 0.582446 11.00000 -1.20000 AFIX 0 C48 1 0.750780 0.177562 0.605980 11.00000 0.03595 0.04395 = 0.03991 0.00717 0.01098 0.00352 C49 1 0.895115 0.175959 0.531852 11.00000 0.03001 0.03489 = 0.03297 0.00001 0.00929 -0.00155 C50 1 0.893007 0.100057 0.505942 11.00000 0.04188 0.04333 = 0.03433 -0.00530 0.00470 -0.00415 AFIX 43 H50 2 0.918304 0.028245 0.506369 11.00000 -1.20000 AFIX 0 C51 1 0.854396 0.128547 0.479657 11.00000 0.04979 0.06075 = 0.03723 -0.00585 0.00762 0.00121 AFIX 43 H51 2 0.853461 0.075798 0.462726 11.00000 -1.20000 AFIX 0 C52 1 0.817150 0.235881 0.478652 11.00000 0.04130 0.06488 = 0.03493 0.00373 -0.00451 -0.00290 AFIX 43 H52 2 0.792012 0.256763 0.460775 11.00000 -1.20000 AFIX 0 C53 1 0.816920 0.312880 0.504108 11.00000 0.03685 0.04774 = 0.04763 0.00656 -0.00076 0.00450 AFIX 43 H53 2 0.791804 0.384995 0.503671 11.00000 -1.20000 AFIX 0 C54 1 0.855171 0.278769 0.530025 11.00000 0.03468 0.03512 = 0.03754 0.00087 0.00490 -0.00559 C55 1 0.975946 -0.017097 0.564931 11.00000 0.03839 0.02700 = 0.03122 -0.00192 0.01277 0.00050 AFIX 13 H55 2 0.983899 -0.035160 0.544407 11.00000 -1.20000 AFIX 0 C56 1 1.035129 -0.039575 0.586951 11.00000 0.04402 0.03623 = 0.03885 0.00273 0.01232 0.00595 AFIX 23 H56A 2 1.066275 0.017793 0.581706 11.00000 -1.20000 H56B 2 1.028771 -0.018953 0.607374 11.00000 -1.20000 AFIX 0 C57 1 1.055949 -0.179642 0.585690 11.00000 0.06787 0.03963 = 0.05514 0.01081 0.02091 0.01923 AFIX 23 H57A 2 1.065531 -0.197948 0.565701 11.00000 -1.20000 H57B 2 1.092405 -0.192012 0.600188 11.00000 -1.20000 AFIX 0 C58 1 1.007782 -0.273356 0.592656 11.00000 0.09896 0.02808 = 0.05977 0.01147 0.02943 0.01678 AFIX 23 H58A 2 1.021633 -0.361816 0.590808 11.00000 -1.20000 H58B 2 1.000772 -0.260502 0.613306 11.00000 -1.20000 AFIX 0 C59 1 0.950113 -0.253134 0.571522 11.00000 0.08689 0.02789 = 0.06572 -0.00177 0.03614 -0.00904 AFIX 23 H59A 2 0.919513 -0.311108 0.577100 11.00000 -1.20000 H59B 2 0.956331 -0.275226 0.551157 11.00000 -1.20000 AFIX 0 C60 1 0.927110 -0.111681 0.571899 11.00000 0.05757 0.03246 = 0.04859 -0.00853 0.01685 -0.00680 AFIX 23 H60A 2 0.891143 -0.101681 0.556960 11.00000 -1.20000 H60B 2 0.916476 -0.092034 0.591616 11.00000 -1.20000 AFIX 0 C61 1 0.848830 0.476950 0.655114 11.00000 0.04929 0.02937 = 0.04104 0.00191 0.01418 0.00761 AFIX 13 H61 2 0.814780 0.493268 0.665987 11.00000 -1.20000 AFIX 0 C62 1 0.906627 0.501450 0.676877 11.00000 0.05572 0.03629 = 0.03884 -0.00610 0.01243 0.00495 AFIX 23 H62A 2 0.941064 0.480711 0.666991 11.00000 -1.20000 H62B 2 0.907792 0.444757 0.694264 11.00000 -1.20000 AFIX 0 C63 1 0.911352 0.643355 0.687585 11.00000 0.06285 0.04645 = 0.05952 -0.01534 0.01639 -0.00311 AFIX 23 H63A 2 0.879031 0.662304 0.699078 11.00000 -1.20000 H63B 2 0.949555 0.656698 0.700697 11.00000 -1.20000 AFIX 0 C64 1 0.907075 0.733827 0.660794 11.00000 0.09958 0.03380 = 0.08528 -0.01066 0.04525 -0.01044 AFIX 23 H64A 2 0.941361 0.719640 0.650325 11.00000 -1.20000 H64B 2 0.908540 0.823041 0.667817 11.00000 -1.20000 AFIX 0 C65 1 0.849132 0.711875 0.639121 11.00000 0.11152 0.03038 = 0.07332 0.01725 0.04124 0.01572 AFIX 23 H65A 2 0.848268 0.768972 0.621824 11.00000 -1.20000 H65B 2 0.814910 0.733390 0.649099 11.00000 -1.20000 AFIX 0 C66 1 0.843596 0.572260 0.628368 11.00000 0.06571 0.03862 = 0.05038 0.00776 0.01670 0.01061 AFIX 23 H66A 2 0.875143 0.553785 0.616357 11.00000 -1.20000 H66B 2 0.804907 0.560167 0.615591 11.00000 -1.20000 AFIX 0 C67 1 0.846784 0.212153 0.678501 11.00000 0.04284 0.03637 = 0.02874 0.00328 0.01280 -0.00032 AFIX 13 H67 2 0.889434 0.207109 0.687567 11.00000 -1.20000 AFIX 0 C68 1 0.825196 0.071768 0.673267 11.00000 0.05811 0.03658 = 0.04120 0.00529 0.02004 -0.00021 AFIX 23 H68A 2 0.782275 0.071372 0.665560 11.00000 -1.20000 H68B 2 0.846103 0.031975 0.658170 11.00000 -1.20000 AFIX 0 C69 1 0.836685 -0.006923 0.702077 11.00000 0.06745 0.05014 = 0.04899 0.01449 0.02523 0.01099 AFIX 23 H69A 2 0.879851 -0.012669 0.708933 11.00000 -1.20000 H69B 2 0.821289 -0.094295 0.698142 11.00000 -1.20000 AFIX 0 C70 1 0.806269 0.054768 0.726569 11.00000 0.08872 0.05861 = 0.04923 0.01712 0.03588 0.00691 AFIX 23 H70A 2 0.817030 0.006711 0.745260 11.00000 -1.20000 H70B 2 0.762766 0.049734 0.720815 11.00000 -1.20000 AFIX 0 C71 1 0.824741 0.196168 0.731792 11.00000 0.05942 0.07008 = 0.04083 0.00990 0.02306 0.01008 AFIX 23 H71A 2 0.801829 0.234402 0.746279 11.00000 -1.20000 H71B 2 0.867262 0.200568 0.740233 11.00000 -1.20000 AFIX 0 C72 1 0.813661 0.273258 0.702471 11.00000 0.05342 0.04664 = 0.03845 -0.00126 0.01666 0.00193 AFIX 23 H72A 2 0.827578 0.361768 0.706294 11.00000 -1.20000 H72B 2 0.770651 0.275872 0.695018 11.00000 -1.20000 AFIX 0 C73 1 0.104056 0.122500 0.701310 11.00000 0.03209 0.04222 = 0.04811 0.00321 0.00614 0.00415 AFIX 13 H73 2 0.080878 0.091360 0.682300 11.00000 -1.20000 AFIX 0 C74 1 0.076875 0.063098 0.727735 11.00000 0.04781 0.04527 = 0.04402 0.00464 0.00425 -0.00054 AFIX 23 H74A 2 0.076090 -0.030727 0.725817 11.00000 -1.20000 H74B 2 0.102138 0.085016 0.746656 11.00000 -1.20000 AFIX 0 C75 1 0.013356 0.112574 0.728224 11.00000 0.03624 0.06221 = 0.05002 0.00377 0.00912 -0.00067 AFIX 23 H75A 2 -0.002365 0.075115 0.745319 11.00000 -1.20000 H75B 2 -0.012586 0.085544 0.709904 11.00000 -1.20000 AFIX 0 C76 1 0.012616 0.259789 0.730568 11.00000 0.04862 0.06928 = 0.04735 0.00006 0.00844 0.01424 AFIX 23 H76A 2 -0.028420 0.289524 0.730777 11.00000 -1.20000 H76B 2 0.037109 0.286888 0.749309 11.00000 -1.20000 AFIX 0 C77 1 0.036996 0.319658 0.704127 11.00000 0.04534 0.05242 = 0.05421 -0.00215 -0.00073 0.01386 AFIX 23 H77A 2 0.037616 0.413376 0.706312 11.00000 -1.20000 H77B 2 0.010280 0.298484 0.685595 11.00000 -1.20000 AFIX 0 C78 1 0.100601 0.271877 0.701802 11.00000 0.03979 0.04698 = 0.05302 0.00788 -0.00312 0.00172 AFIX 23 H78A 2 0.128501 0.304510 0.718882 11.00000 -1.20000 H78B 2 0.112897 0.306117 0.683494 11.00000 -1.20000 AFIX 0 C79 1 0.179897 -0.102009 0.692942 11.00000 0.04560 0.04310 = 0.03193 0.00084 0.00813 -0.00640 C80 1 0.129602 -0.164831 0.676956 11.00000 0.05421 0.04698 = 0.03724 0.00092 0.00884 -0.01005 AFIX 43 H80 2 0.095674 -0.116417 0.669219 11.00000 -1.20000 AFIX 0 C81 1 0.129318 -0.298499 0.672391 11.00000 0.07564 0.05195 = 0.04944 -0.00640 0.00777 -0.02234 AFIX 43 H81 2 0.095059 -0.338832 0.662092 11.00000 -1.20000 AFIX 0 C82 1 0.179298 -0.370527 0.683019 11.00000 0.09571 0.04148 = 0.05798 -0.00096 0.01769 -0.00444 AFIX 43 H82 2 0.179037 -0.459867 0.679975 11.00000 -1.20000 AFIX 0 C83 1 0.230599 -0.310270 0.698399 11.00000 0.06888 0.05022 = 0.05179 -0.00722 0.01467 0.00692 AFIX 43 H83 2 0.264852 -0.358863 0.705500 11.00000 -1.20000 AFIX 0 C84 1 0.230250 -0.179351 0.702978 11.00000 0.06573 0.03635 = 0.03619 -0.00274 0.01217 0.00346 C85 1 0.205381 0.145788 0.667980 11.00000 0.03942 0.05261 = 0.04592 0.00998 0.00507 -0.00158 AFIX 13 H85 2 0.210586 0.238956 0.672016 11.00000 -1.20000 AFIX 0 C86 1 0.157401 0.133239 0.639913 11.00000 0.04560 0.09469 = 0.04783 0.01962 -0.00298 -0.01122 AFIX 23 H86A 2 0.119487 0.169205 0.644062 11.00000 -1.20000 H86B 2 0.150969 0.042262 0.634798 11.00000 -1.20000 AFIX 0 C87 1 0.177742 0.205849 0.613102 11.00000 0.05922 0.12568 = 0.04535 0.03743 -0.00268 -0.01058 AFIX 23 H87A 2 0.147413 0.195205 0.595315 11.00000 -1.20000 H87B 2 0.181193 0.297807 0.617733 11.00000 -1.20000 AFIX 0 C88 1 0.238560 0.155194 0.606327 11.00000 0.08162 0.10090 = 0.04799 0.01622 0.01696 0.00159 AFIX 23 H88A 2 0.234489 0.065171 0.599967 11.00000 -1.20000 H88B 2 0.251116 0.205261 0.590016 11.00000 -1.20000 AFIX 0 C89 1 0.285219 0.166186 0.634062 11.00000 0.05117 0.08168 = 0.06105 0.01510 0.01720 0.00347 AFIX 23 H89A 2 0.291982 0.257180 0.639068 11.00000 -1.20000 H89B 2 0.323029 0.129892 0.629859 11.00000 -1.20000 AFIX 0 C90 1 0.266190 0.095614 0.661167 11.00000 0.03896 0.06693 = 0.04194 0.00832 0.00643 0.00350 AFIX 23 H90A 2 0.296785 0.108292 0.678764 11.00000 -1.20000 H90B 2 0.263159 0.003250 0.656964 11.00000 -1.20000 AFIX 0 C91 1 0.561773 0.890933 0.536819 11.00000 0.15175 0.07966 = 0.11435 0.02527 0.06698 -0.00034 AFIX 137 H91A 2 0.585947 0.886844 0.520891 11.00000 -1.50000 H91B 2 0.575582 0.961117 0.550236 11.00000 -1.50000 H91C 2 0.520273 0.905101 0.528292 11.00000 -1.50000 AFIX 0 C92 1 0.662037 0.520290 0.563119 11.00000 0.19843 0.14076 = 0.08864 0.03136 0.04239 0.07547 AFIX 137 H92A 2 0.629606 0.475535 0.570473 11.00000 -1.50000 H92B 2 0.680399 0.580351 0.578194 11.00000 -1.50000 H92C 2 0.691675 0.458517 0.558815 11.00000 -1.50000 AFIX 0 C93 1 0.681867 0.829794 0.624736 11.00000 0.22003 0.05097 = 0.34534 0.03743 0.09063 -0.04386 AFIX 137 H93A 2 0.697253 0.891404 0.640104 11.00000 -1.50000 H93B 2 0.641033 0.852103 0.616481 11.00000 -1.50000 H93C 2 0.706461 0.831257 0.608959 11.00000 -1.50000 AFIX 0 C94 1 0.756929 0.716558 0.510386 11.00000 0.14287 0.10768 = 0.42177 -0.05509 0.13852 -0.04234 AFIX 137 H94A 2 0.768626 0.760530 0.493278 11.00000 -1.50000 H94B 2 0.792378 0.693808 0.524315 11.00000 -1.50000 H94C 2 0.731795 0.772690 0.520238 11.00000 -1.50000 REM REM 23mt_RupdcycBrhex.hkl REM AFIX 0 HKLF 4 REM shelxt_a.res in P2/n REM wR2 = 0.1268, GooF = S = 1.015, Restrained GooF = 1.015 for all data REM R1 = 0.0564 for 14549 Fo > 4sig(Fo) and 0.1242 for all 25316 data REM 1050 parameters refined using 0 restraints END WGHT 0.0383 9.2206 REM Instructions for potential hydrogen bonds HTAB O1 Cl1 HTAB O1 Cl2 HTAB O2 O1 HTAB O3 Cl1 HTAB C6 Br2 HTAB C6 Cl2 HTAB C11 Cl5_$1 HTAB C20 Cl1 HTAB C24 Br1 HTAB C26 Cl2 HTAB C30 Br2 HTAB C30 Cl2 HTAB C36 Br1 HTAB C36 Cl1 HTAB C42 Br4 HTAB C42 Cl4 HTAB C56 Cl3 HTAB C60 Br3 HTAB C60 Cl3 HTAB C62 Cl4 HTAB C66 Br4 HTAB C68 Br3 HTAB C68 Cl3 HTAB C74 Br5_$1 HTAB C74 Cl5 HTAB C78 Cl5 HTAB C90 Br5 HTAB C90 Cl5_$1 REM Highest difference peak 1.173, deepest hole -1.289, 1-sigma level 0.120 Q1 1 0.2864 -0.1597 0.7086 11.00000 0.05 1.17 Q2 1 0.9659 0.3819 0.6019 11.00000 0.05 0.65 Q3 1 0.3780 0.8153 0.6243 11.00000 0.05 0.60 Q4 1 0.1280 -0.4117 0.6772 11.00000 0.05 0.56 Q5 1 0.5894 0.8851 0.5646 11.00000 0.05 0.55 Q6 1 0.1757 -0.0270 0.6957 11.00000 0.05 0.54 Q7 1 0.4430 0.5127 0.6458 11.00000 0.05 0.54 Q8 1 0.8411 0.2599 0.7285 11.00000 0.05 0.53 Q9 1 0.4111 0.5584 0.6469 11.00000 0.05 0.52 Q10 1 0.7006 0.6607 0.5611 11.00000 0.05 0.52 Q11 1 0.9297 0.4289 0.6200 11.00000 0.05 0.51 Q12 1 0.4990 0.7406 0.6508 11.00000 0.05 0.51 Q13 1 0.4449 0.7477 0.6190 11.00000 0.05 0.51 Q14 1 1.0876 0.3749 0.4892 11.00000 0.05 0.49 Q15 1 0.7400 0.5990 0.5607 11.00000 0.05 0.49 Q16 1 0.2563 -0.0350 0.7348 11.00000 0.05 0.48 Q17 1 0.6260 0.9022 0.6196 11.00000 0.05 0.48 Q18 1 0.6605 0.0159 0.5782 11.00000 0.05 0.47 Q19 1 0.4744 0.5953 0.5251 11.00000 0.05 0.47 Q20 1 0.0419 0.1221 0.7330 11.00000 0.05 0.47 ; _shelx_res_checksum 16868 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru Ru1 0.45503(2) 0.70639(4) 0.62567(2) 0.02724(10) Uani d 1 . . Ru Ru2 0.90381(2) 0.23092(4) 0.60624(2) 0.02968(11) Uani d 1 . . Ru Ru3 0.250000 0.08549(6) 0.750000 0.03808(16) Uani d 1 . . Br Br1 0.41905(3) 0.51668(5) 0.65268(2) 0.03843(14) Uani d 1 . . Br Br2 0.35608(2) 0.80978(5) 0.63161(2) 0.03800(14) Uani d 1 . . Br Br3 0.81523(3) 0.08129(5) 0.59229(2) 0.04178(15) Uani d 1 . . Br Br4 0.85176(3) 0.38066(5) 0.56601(2) 0.03921(15) Uani d 1 . . Br Br5 0.30047(3) -0.09785(6) 0.72561(2) 0.04730(16) Uani d 1 . . Cl Cl1 0.54584(6) 0.60056(14) 0.61726(3) 0.0448(4) Uani d 1 . . Cl Cl2 0.48976(7) 0.89386(13) 0.60203(3) 0.0426(3) Uani d 1 . . Cl Cl3 0.95502(7) 0.08131(13) 0.64207(3) 0.0417(3) Uani d 1 . . Cl Cl4 0.98566(7) 0.37863(13) 0.62006(3) 0.0435(4) Uani d 1 . . Cl Cl5 0.19731(8) 0.25278(16) 0.77183(4) 0.0622(5) Uani d 1 . . P P1 0.39951(6) 0.63740(13) 0.57873(3) 0.0306(3) Uani d 1 . . P P2 0.50036(6) 0.76683(12) 0.67528(3) 0.0288(3) Uani d 1 . . P P3 0.95116(6) 0.15427(12) 0.56622(3) 0.0287(3) Uani d 1 . . P P4 0.84465(7) 0.30566(13) 0.64276(3) 0.0330(3) Uani d 1 . . P P5 0.18352(7) 0.07226(14) 0.70276(3) 0.0378(4) Uani d 1 . . O O1 0.5666(4) 0.7798(7) 0.55210(18) 0.149(3) Uani d 1 . . H H1 0.550219 0.787057 0.567178 0.224 Uiso calc 1 . . O O2 0.6402(4) 0.5856(7) 0.53765(16) 0.126(2) Uani d 1 . . H H2 0.646819 0.663398 0.540235 0.189 Uiso calc 1 . . O O3 0.6831(3) 0.7079(10) 0.6371(2) 0.170(3) Uani d 1 . . H H3 0.649325 0.675398 0.633465 0.255 Uiso calc 1 . . O O4 0.7272(4) 0.6120(8) 0.5014(2) 0.164(3) Uani d 1 . . H H4 0.691889 0.630702 0.495053 0.245 Uiso calc 1 . . C C1 0.3888(2) 0.7500(5) 0.54567(12) 0.0347(13) Uani d 1 . . H H1A 0.429133 0.776049 0.542076 0.042 Uiso calc 1 . . C C2 0.3565(3) 0.6905(6) 0.51601(13) 0.0487(16) Uani d 1 . . H H2A 0.378430 0.614170 0.511112 0.058 Uiso calc 1 . . H H2B 0.316154 0.663409 0.518692 0.058 Uiso calc 1 . . C C3 0.3521(3) 0.7869(7) 0.49000(14) 0.064(2) Uani d 1 . . H H3A 0.392483 0.807348 0.486049 0.077 Uiso calc 1 . . H H3B 0.330097 0.747460 0.471924 0.077 Uiso calc 1 . . C C4 0.3207(3) 0.9112(6) 0.49680(14) 0.0590(19) Uani d 1 . . H H4A 0.278731 0.892828 0.498276 0.071 Uiso calc 1 . . H H4B 0.321561 0.972531 0.480435 0.071 Uiso calc 1 . . C C5 0.3514(3) 0.9701(6) 0.52617(14) 0.0535(17) Uani d 1 . . H H5A 0.328942 1.046100 0.530833 0.064 Uiso calc 1 . . H H5B 0.391744 0.998109 0.523738 0.064 Uiso calc 1 . . C C6 0.3557(3) 0.8741(5) 0.55250(13) 0.0436(15) Uani d 1 . . H H6A 0.315365 0.852321 0.556230 0.052 Uiso calc 1 . . H H6B 0.377131 0.914454 0.570625 0.052 Uiso calc 1 . . C C7 0.4518(2) 0.6973(5) 0.70083(12) 0.0331(12) Uani d 1 . . C C8 0.4510(2) 0.7410(5) 0.73039(13) 0.0406(14) Uani d 1 . . H H8 0.472478 0.815312 0.737213 0.049 Uiso calc 1 . . C C9 0.4186(3) 0.6748(6) 0.74965(14) 0.0514(16) Uani d 1 . . H H9 0.418133 0.705871 0.769122 0.062 Uiso calc 1 . . C C10 0.3874(3) 0.5645(6) 0.74028(15) 0.0549(18) Uani d 1 . . H H10 0.366098 0.520622 0.753422 0.066 Uiso calc 1 . . C C11 0.3875(3) 0.5181(5) 0.71140(14) 0.0447(15) Uani d 1 . . H H11 0.366251 0.443249 0.704735 0.054 Uiso calc 1 . . C C12 0.4197(2) 0.5856(5) 0.69277(12) 0.0363(13) Uani d 1 . . C C13 0.3212(2) 0.6168(5) 0.58611(12) 0.0309(12) Uani d 1 . . C C14 0.2798(2) 0.5276(5) 0.57109(13) 0.0386(14) Uani d 1 . . H H14 0.291481 0.474357 0.556239 0.046 Uiso calc 1 . . C C15 0.2218(3) 0.5174(6) 0.57795(14) 0.0457(15) Uani d 1 . . H H15 0.195128 0.456705 0.567977 0.055 Uiso calc 1 . . C C16 0.2035(3) 0.5970(6) 0.59952(15) 0.0566(18) Uani d 1 . . H H16 0.164149 0.591121 0.603637 0.068 Uiso calc 1 . . C C17 0.2427(3) 0.6852(6) 0.61507(14) 0.0478(15) Uani d 1 . . H H17 0.230678 0.738451 0.629833 0.057 Uiso calc 1 . . C C18 0.3005(2) 0.6920(5) 0.60804(12) 0.0358(13) Uani d 1 . . C C19 0.4158(3) 0.4789(5) 0.56218(13) 0.0395(14) Uani d 1 . . H H19 0.381884 0.458337 0.546329 0.047 Uiso calc 1 . . C C20 0.4732(3) 0.4849(6) 0.54722(14) 0.0568(18) Uani d 1 . . H H20A 0.469219 0.552989 0.532055 0.068 Uiso calc 1 . . H H20B 0.507984 0.504483 0.562289 0.068 Uiso calc 1 . . C C21 0.4820(4) 0.3535(8) 0.53245(18) 0.086(3) Uani d 1 . . H H21A 0.449060 0.339149 0.515999 0.103 Uiso calc 1 . . H H21B 0.519361 0.355107 0.523995 0.103 Uiso calc 1 . . C C22 0.4841(4) 0.2439(8) 0.5545(2) 0.103(4) Uani d 1 . . H H22A 0.520184 0.252008 0.569434 0.124 Uiso calc 1 . . H H22B 0.486629 0.162427 0.543891 0.124 Uiso calc 1 . . C C23 0.4291(4) 0.2410(6) 0.57051(18) 0.080(3) Uani d 1 . . H H23A 0.393428 0.221287 0.556024 0.096 Uiso calc 1 . . H H23B 0.433972 0.173052 0.585705 0.096 Uiso calc 1 . . C C24 0.4208(3) 0.3697(5) 0.58536(14) 0.0525(17) Uani d 1 . . H H24A 0.454827 0.385897 0.601104 0.063 Uiso calc 1 . . H H24B 0.384418 0.367173 0.594663 0.063 Uiso calc 1 . . C C25 0.5074(2) 0.9407(4) 0.68529(12) 0.0351(13) Uani d 1 . . H H25 0.514951 0.946618 0.707400 0.042 Uiso calc 1 . . C C26 0.5614(3) 1.0021(5) 0.67351(14) 0.0476(16) Uani d 1 . . H H26A 0.598052 0.955925 0.681678 0.057 Uiso calc 1 . . H H26B 0.556035 0.995224 0.651648 0.057 Uiso calc 1 . . C C27 0.5675(3) 1.1442(5) 0.68268(17) 0.065(2) Uani d 1 . . H H27A 0.600960 1.182748 0.674410 0.078 Uiso calc 1 . . H H27B 0.576171 1.150618 0.704535 0.078 Uiso calc 1 . . C C28 0.5096(4) 1.2181(6) 0.67121(19) 0.085(3) Uani d 1 . . H H28A 0.514132 1.307870 0.677747 0.102 Uiso calc 1 . . H H28B 0.502701 1.217109 0.649275 0.102 Uiso calc 1 . . C C29 0.4561(3) 1.1593(6) 0.68275(17) 0.066(2) Uani d 1 . . H H29A 0.419736 1.205642 0.674242 0.080 Uiso calc 1 . . H H29B 0.461143 1.168208 0.704573 0.080 Uiso calc 1 . . C C30 0.4493(3) 1.0158(5) 0.67428(13) 0.0413(14) Uani d 1 . . H H30A 0.439430 1.007654 0.652492 0.050 Uiso calc 1 . . H H30B 0.416365 0.978711 0.683207 0.050 Uiso calc 1 . . C C31 0.5747(2) 0.6983(5) 0.69182(12) 0.0335(12) Uani d 1 . . H H31 0.603071 0.721287 0.678016 0.040 Uiso calc 1 . . C C32 0.6024(3) 0.7494(5) 0.72326(13) 0.0467(16) Uani d 1 . . H H32A 0.604577 0.843393 0.722686 0.056 Uiso calc 1 . . H H32B 0.576538 0.725448 0.737875 0.056 Uiso calc 1 . . C C33 0.6660(3) 0.6939(7) 0.73327(16) 0.067(2) Uani d 1 . . H H33A 0.692828 0.723712 0.719639 0.080 Uiso calc 1 . . H H33B 0.681604 0.724829 0.753425 0.080 Uiso calc 1 . . C C34 0.6643(3) 0.5465(7) 0.73325(17) 0.076(2) Uani d 1 . . H H34A 0.705020 0.513019 0.738434 0.091 Uiso calc 1 . . H H34B 0.640894 0.516711 0.748472 0.091 Uiso calc 1 . . C C35 0.6366(3) 0.4946(6) 0.70281(16) 0.0617(19) Uani d 1 . . H H35A 0.634479 0.400625 0.703693 0.074 Uiso calc 1 . . H H35B 0.661906 0.517693 0.687890 0.074 Uiso calc 1 . . C C36 0.5736(2) 0.5493(5) 0.69330(13) 0.0407(14) Uani d 1 . . H H36A 0.547663 0.522141 0.707648 0.049 Uiso calc 1 . . H H36B 0.556819 0.514883 0.673615 0.049 Uiso calc 1 . . C C37 1.0163(2) 0.2463(4) 0.55505(11) 0.0280(11) Uani d 1 . . H H37 1.047546 0.250198 0.572942 0.034 Uiso calc 1 . . C C38 1.0452(2) 0.1830(5) 0.52985(12) 0.0380(13) Uani d 1 . . H H38A 1.056036 0.094136 0.535431 0.046 Uiso calc 1 . . H H38B 1.016035 0.181039 0.511430 0.046 Uiso calc 1 . . C C39 1.1013(3) 0.2561(5) 0.52403(14) 0.0433(15) Uani d 1 . . H H39A 1.131946 0.250514 0.541816 0.052 Uiso calc 1 . . H H39B 1.117213 0.215437 0.507365 0.052 Uiso calc 1 . . C C40 1.0879(3) 0.3980(5) 0.51654(13) 0.0450(15) Uani d 1 . . H H40A 1.062144 0.404486 0.497082 0.054 Uiso calc 1 . . H H40B 1.125347 0.443355 0.515157 0.054 Uiso calc 1 . . C C41 1.0566(2) 0.4616(5) 0.54077(13) 0.0415(14) Uani d 1 . . H H41A 1.045455 0.549783 0.534710 0.050 Uiso calc 1 . . H H41B 1.084589 0.465503 0.559590 0.050 Uiso calc 1 . . C C42 1.0002(2) 0.3868(5) 0.54584(12) 0.0361(13) Uani d 1 . . H H42A 0.971093 0.387412 0.527416 0.043 Uiso calc 1 . . H H42B 0.981945 0.428867 0.561588 0.043 Uiso calc 1 . . C C43 0.7653(3) 0.2795(5) 0.62603(12) 0.0394(14) Uani d 1 . . C C44 0.7165(3) 0.3466(6) 0.63470(14) 0.0526(17) Uani d 1 . . H H44 0.723657 0.417168 0.647718 0.063 Uiso calc 1 . . C C45 0.6579(3) 0.3098(7) 0.62424(16) 0.064(2) Uani d 1 . . H H45 0.626143 0.357091 0.629961 0.076 Uiso calc 1 . . C C46 0.6456(3) 0.2048(8) 0.60556(17) 0.071(2) Uani d 1 . . H H46 0.605821 0.178452 0.599540 0.085 Uiso calc 1 . . C C47 0.6922(3) 0.1382(7) 0.59569(14) 0.0539(17) Uani d 1 . . H H47 0.684541 0.068475 0.582446 0.065 Uiso calc 1 . . C C48 0.7508(3) 0.1776(5) 0.60598(13) 0.0394(14) Uani d 1 . . C C49 0.8951(2) 0.1760(5) 0.53185(12) 0.0322(12) Uani d 1 . . C C50 0.8930(3) 0.1001(5) 0.50594(12) 0.0400(14) Uani d 1 . . H H50 0.918304 0.028245 0.506369 0.048 Uiso calc 1 . . C C51 0.8544(3) 0.1285(6) 0.47966(14) 0.0492(16) Uani d 1 . . H H51 0.853461 0.075798 0.462726 0.059 Uiso calc 1 . . C C52 0.8172(3) 0.2359(6) 0.47865(14) 0.0481(16) Uani d 1 . . H H52 0.792012 0.256763 0.460775 0.058 Uiso calc 1 . . C C53 0.8169(3) 0.3129(6) 0.50411(13) 0.0448(15) Uani d 1 . . H H53 0.791804 0.384995 0.503671 0.054 Uiso calc 1 . . C C54 0.8552(2) 0.2788(5) 0.53002(12) 0.0358(13) Uani d 1 . . C C55 0.9759(2) -0.0171(4) 0.56493(12) 0.0314(12) Uani d 1 . . H H55 0.983899 -0.035160 0.544407 0.038 Uiso calc 1 . . C C56 1.0351(2) -0.0396(5) 0.58695(13) 0.0391(14) Uani d 1 . . H H56A 1.066275 0.017793 0.581706 0.047 Uiso calc 1 . . H H56B 1.028771 -0.018953 0.607374 0.047 Uiso calc 1 . . C C57 1.0559(3) -0.1796(5) 0.58569(15) 0.0530(17) Uani d 1 . . H H57A 1.065531 -0.197948 0.565701 0.064 Uiso calc 1 . . H H57B 1.092405 -0.192012 0.600188 0.064 Uiso calc 1 . . C C58 1.0078(3) -0.2734(5) 0.59266(15) 0.060(2) Uani d 1 . . H H58A 1.021633 -0.361816 0.590808 0.073 Uiso calc 1 . . H H58B 1.000772 -0.260502 0.613306 0.073 Uiso calc 1 . . C C59 0.9501(3) -0.2531(5) 0.57152(16) 0.0576(19) Uani d 1 . . H H59A 0.919513 -0.311108 0.577100 0.069 Uiso calc 1 . . H H59B 0.956331 -0.275226 0.551157 0.069 Uiso calc 1 . . C C60 0.9271(3) -0.1117(5) 0.57190(14) 0.0453(15) Uani d 1 . . H H60A 0.891143 -0.101681 0.556960 0.054 Uiso calc 1 . . H H60B 0.916476 -0.092034 0.591616 0.054 Uiso calc 1 . . C C61 0.8488(3) 0.4769(5) 0.65511(13) 0.0391(14) Uani d 1 . . H H61 0.814780 0.493268 0.665987 0.047 Uiso calc 1 . . C C62 0.9066(3) 0.5015(5) 0.67688(13) 0.0431(15) Uani d 1 . . H H62A 0.941064 0.480711 0.666991 0.052 Uiso calc 1 . . H H62B 0.907792 0.444757 0.694264 0.052 Uiso calc 1 . . C C63 0.9114(3) 0.6434(6) 0.68758(15) 0.0555(18) Uani d 1 . . H H63A 0.879031 0.662304 0.699078 0.067 Uiso calc 1 . . H H63B 0.949555 0.656698 0.700697 0.067 Uiso calc 1 . . C C64 0.9071(4) 0.7338(6) 0.66079(17) 0.070(2) Uani d 1 . . H H64A 0.941361 0.719640 0.650325 0.084 Uiso calc 1 . . H H64B 0.908540 0.823041 0.667817 0.084 Uiso calc 1 . . C C65 0.8491(4) 0.7119(6) 0.63912(17) 0.069(2) Uani d 1 . . H H65A 0.848268 0.768972 0.621824 0.083 Uiso calc 1 . . H H65B 0.814910 0.733390 0.649099 0.083 Uiso calc 1 . . C C66 0.8436(3) 0.5723(5) 0.62837(14) 0.0508(16) Uani d 1 . . H H66A 0.875143 0.553785 0.616357 0.061 Uiso calc 1 . . H H66B 0.804907 0.560167 0.615591 0.061 Uiso calc 1 . . C C67 0.8468(3) 0.2122(5) 0.67850(12) 0.0352(13) Uani d 1 . . H H67 0.889434 0.207109 0.687567 0.042 Uiso calc 1 . . C C68 0.8252(3) 0.0718(5) 0.67327(13) 0.0440(15) Uani d 1 . . H H68A 0.782275 0.071372 0.665560 0.053 Uiso calc 1 . . H H68B 0.846103 0.031975 0.658170 0.053 Uiso calc 1 . . C C69 0.8367(3) -0.0069(6) 0.70208(14) 0.0538(17) Uani d 1 . . H H69A 0.879851 -0.012669 0.708933 0.065 Uiso calc 1 . . H H69B 0.821289 -0.094295 0.698142 0.065 Uiso calc 1 . . C C70 0.8063(3) 0.0548(6) 0.72657(15) 0.063(2) Uani d 1 . . H H70A 0.817030 0.006711 0.745260 0.075 Uiso calc 1 . . H H70B 0.762766 0.049734 0.720815 0.075 Uiso calc 1 . . C C71 0.8247(3) 0.1962(6) 0.73179(14) 0.0552(17) Uani d 1 . . H H71A 0.801829 0.234402 0.746279 0.066 Uiso calc 1 . . H H71B 0.867262 0.200568 0.740233 0.066 Uiso calc 1 . . C C72 0.8137(3) 0.2733(5) 0.70247(13) 0.0452(15) Uani d 1 . . H H72A 0.827578 0.361768 0.706294 0.054 Uiso calc 1 . . H H72B 0.770651 0.275872 0.695018 0.054 Uiso calc 1 . . C C73 0.1041(2) 0.1225(5) 0.70131(14) 0.0408(14) Uani d 1 . . H H73 0.080878 0.091360 0.682300 0.049 Uiso calc 1 . . C C74 0.0769(3) 0.0631(6) 0.72773(13) 0.0460(15) Uani d 1 . . H H74A 0.076090 -0.030727 0.725817 0.055 Uiso calc 1 . . H H74B 0.102138 0.085016 0.746656 0.055 Uiso calc 1 . . C C75 0.0134(3) 0.1126(6) 0.72822(14) 0.0492(16) Uani d 1 . . H H75A -0.002365 0.075115 0.745319 0.059 Uiso calc 1 . . H H75B -0.012586 0.085544 0.709904 0.059 Uiso calc 1 . . C C76 0.0126(3) 0.2598(6) 0.73057(14) 0.0550(17) Uani d 1 . . H H76A -0.028420 0.289524 0.730777 0.066 Uiso calc 1 . . H H76B 0.037109 0.286888 0.749309 0.066 Uiso calc 1 . . C C77 0.0370(3) 0.3197(6) 0.70413(14) 0.0515(16) Uani d 1 . . H H77A 0.037616 0.413376 0.706312 0.062 Uiso calc 1 . . H H77B 0.010280 0.298484 0.685595 0.062 Uiso calc 1 . . C C78 0.1006(3) 0.2719(5) 0.70180(14) 0.0477(16) Uani d 1 . . H H78A 0.128501 0.304510 0.718882 0.057 Uiso calc 1 . . H H78B 0.112897 0.306117 0.683494 0.057 Uiso calc 1 . . C C79 0.1799(3) -0.1020(5) 0.69294(12) 0.0400(14) Uani d 1 . . C C80 0.1296(3) -0.1648(6) 0.67696(13) 0.0460(15) Uani d 1 . . H H80 0.095674 -0.116417 0.669219 0.055 Uiso calc 1 . . C C81 0.1293(3) -0.2985(6) 0.67239(15) 0.0592(18) Uani d 1 . . H H81 0.095059 -0.338832 0.662092 0.071 Uiso calc 1 . . C C82 0.1793(4) -0.3705(6) 0.68302(16) 0.064(2) Uani d 1 . . H H82 0.179037 -0.459867 0.679975 0.077 Uiso calc 1 . . C C83 0.2306(3) -0.3103(6) 0.69840(15) 0.0564(18) Uani d 1 . . H H83 0.264852 -0.358863 0.705500 0.068 Uiso calc 1 . . C C84 0.2303(3) -0.1794(5) 0.70298(13) 0.0456(15) Uani d 1 . . C C85 0.2054(3) 0.1458(6) 0.66798(13) 0.0461(15) Uani d 1 . . H H85 0.210586 0.238956 0.672016 0.055 Uiso calc 1 . . C C86 0.1574(3) 0.1332(7) 0.63991(14) 0.064(2) Uani d 1 . . H H86A 0.119487 0.169205 0.644062 0.077 Uiso calc 1 . . H H86B 0.150969 0.042262 0.634798 0.077 Uiso calc 1 . . C C87 0.1777(3) 0.2058(8) 0.61310(15) 0.078(2) Uani d 1 . . H H87A 0.147413 0.195205 0.595315 0.093 Uiso calc 1 . . H H87B 0.181193 0.297807 0.617733 0.093 Uiso calc 1 . . C C88 0.2386(3) 0.1552(8) 0.60633(16) 0.076(2) Uani d 1 . . H H88A 0.234489 0.065171 0.599967 0.091 Uiso calc 1 . . H H88B 0.251116 0.205261 0.590016 0.091 Uiso calc 1 . . C C89 0.2852(3) 0.1662(7) 0.63406(15) 0.0637(19) Uani d 1 . . H H89A 0.291982 0.257180 0.639068 0.076 Uiso calc 1 . . H H89B 0.323029 0.129892 0.629859 0.076 Uiso calc 1 . . C C90 0.2662(3) 0.0956(6) 0.66117(13) 0.0493(16) Uani d 1 . . H H90A 0.296785 0.108292 0.678764 0.059 Uiso calc 1 . . H H90B 0.263159 0.003250 0.656964 0.059 Uiso calc 1 . . C C91 0.5618(5) 0.8909(8) 0.5368(2) 0.110(3) Uani d 1 . . H H91A 0.585947 0.886844 0.520891 0.166 Uiso calc 1 . . H H91B 0.575582 0.961117 0.550236 0.166 Uiso calc 1 . . H H91C 0.520273 0.905101 0.528292 0.166 Uiso calc 1 . . C C92 0.6620(5) 0.5203(10) 0.5631(2) 0.140(5) Uani d 1 . . H H92A 0.629606 0.475535 0.570473 0.211 Uiso calc 1 . . H H92B 0.680399 0.580351 0.578194 0.211 Uiso calc 1 . . H H92C 0.691675 0.458517 0.558815 0.211 Uiso calc 1 . . C C93 0.6819(6) 0.8298(9) 0.6247(4) 0.200(8) Uani d 1 . . H H93A 0.697253 0.891404 0.640104 0.301 Uiso calc 1 . . H H93B 0.641033 0.852103 0.616481 0.301 Uiso calc 1 . . H H93C 0.706461 0.831257 0.608959 0.301 Uiso calc 1 . . C C94 0.7569(6) 0.7166(11) 0.5104(4) 0.214(9) Uani d 1 . . H H94A 0.768626 0.760530 0.493278 0.321 Uiso calc 1 . . H H94B 0.792378 0.693808 0.524315 0.321 Uiso calc 1 . . H H94C 0.731795 0.772690 0.520238 0.321 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Ru1 0.0284(2) 0.0241(2) 0.0287(2) 0.00062(17) 0.00281(18) -0.00126(17) Ru2 0.0351(3) 0.0267(2) 0.0288(2) 0.00205(19) 0.00984(19) 0.00085(17) Ru3 0.0364(4) 0.0388(4) 0.0381(4) 0.000 0.0028(3) 0.000 Br1 0.0462(3) 0.0264(3) 0.0411(3) -0.0056(2) 0.0017(3) 0.0015(2) Br2 0.0356(3) 0.0359(3) 0.0423(3) 0.0054(2) 0.0052(3) -0.0081(2) Br3 0.0428(3) 0.0393(3) 0.0455(4) -0.0035(3) 0.0139(3) -0.0065(3) Br4 0.0446(4) 0.0350(3) 0.0388(3) 0.0106(3) 0.0090(3) 0.0019(2) Br5 0.0404(4) 0.0535(4) 0.0470(4) 0.0102(3) 0.0036(3) 0.0007(3) Cl1 0.0342(8) 0.0550(9) 0.0445(9) 0.0093(7) 0.0034(7) -0.0103(7) Cl2 0.0546(9) 0.0374(7) 0.0355(8) -0.0108(7) 0.0056(7) 0.0035(6) Cl3 0.0513(9) 0.0413(8) 0.0338(8) 0.0104(7) 0.0105(7) 0.0071(6) Cl4 0.0502(9) 0.0411(8) 0.0409(9) -0.0089(7) 0.0127(7) -0.0065(6) Cl5 0.0656(11) 0.0611(10) 0.0575(11) 0.0234(9) 0.0012(9) -0.0121(8) P1 0.0293(8) 0.0296(7) 0.0319(8) 0.0022(6) 0.0020(6) -0.0028(6) P2 0.0326(8) 0.0228(6) 0.0305(8) 0.0000(6) 0.0038(6) -0.0008(5) P3 0.0326(8) 0.0259(7) 0.0289(8) 0.0025(6) 0.0085(6) 0.0004(6) P4 0.0384(8) 0.0296(7) 0.0332(8) 0.0047(6) 0.0127(7) 0.0013(6) P5 0.0323(8) 0.0405(8) 0.0396(9) 0.0015(7) 0.0026(7) 0.0047(7) O1 0.205(8) 0.144(6) 0.124(7) 0.078(6) 0.102(6) 0.054(5) O2 0.130(6) 0.155(6) 0.103(5) 0.032(6) 0.045(5) 0.013(5) O3 0.081(5) 0.223(10) 0.203(9) -0.014(6) 0.012(6) -0.017(8) O4 0.198(9) 0.163(8) 0.147(8) -0.030(7) 0.082(8) -0.040(6) C1 0.035(3) 0.037(3) 0.031(3) -0.005(2) 0.002(2) 0.001(2) C2 0.058(4) 0.045(3) 0.040(4) 0.004(3) -0.001(3) -0.006(3) C3 0.080(5) 0.078(5) 0.032(4) 0.003(4) -0.001(4) 0.001(3) C4 0.075(5) 0.057(4) 0.041(4) -0.011(4) -0.003(4) 0.015(3) C5 0.065(4) 0.040(3) 0.052(4) -0.004(3) -0.001(3) 0.009(3) C6 0.052(4) 0.039(3) 0.036(3) -0.003(3) -0.004(3) 0.002(3) C7 0.030(3) 0.033(3) 0.036(3) 0.004(2) 0.005(2) 0.002(2) C8 0.039(3) 0.042(3) 0.042(4) 0.005(3) 0.009(3) 0.002(3) C9 0.060(4) 0.060(4) 0.037(4) 0.011(3) 0.017(3) 0.005(3) C10 0.056(4) 0.056(4) 0.058(5) 0.004(3) 0.023(4) 0.026(3) C11 0.055(4) 0.035(3) 0.045(4) -0.005(3) 0.011(3) 0.008(3) C12 0.036(3) 0.037(3) 0.035(3) 0.001(3) 0.004(3) 0.008(2) C13 0.032(3) 0.025(3) 0.034(3) 0.002(2) 0.001(2) 0.006(2) C14 0.034(3) 0.038(3) 0.043(4) 0.001(3) 0.003(3) 0.002(3) C15 0.033(3) 0.047(4) 0.053(4) -0.012(3) -0.005(3) 0.002(3) C16 0.032(4) 0.076(5) 0.062(5) -0.008(3) 0.009(3) 0.002(4) C17 0.037(4) 0.056(4) 0.052(4) 0.003(3) 0.011(3) -0.002(3) C18 0.030(3) 0.034(3) 0.041(3) -0.002(2) -0.003(3) 0.002(3) C19 0.041(3) 0.035(3) 0.040(4) 0.003(3) -0.002(3) -0.015(3) C20 0.041(4) 0.078(5) 0.050(4) 0.016(3) 0.001(3) -0.027(4) C21 0.077(6) 0.106(7) 0.071(6) 0.040(5) -0.006(4) -0.042(5) C22 0.120(8) 0.072(6) 0.103(7) 0.056(6) -0.031(6) -0.046(5) C23 0.101(7) 0.035(4) 0.094(6) 0.020(4) -0.021(5) -0.018(4) C24 0.058(4) 0.038(3) 0.056(4) 0.002(3) -0.009(3) -0.009(3) C25 0.049(4) 0.025(3) 0.029(3) -0.004(2) 0.000(3) -0.003(2) C26 0.057(4) 0.037(3) 0.047(4) -0.013(3) 0.002(3) -0.002(3) C27 0.076(5) 0.035(3) 0.079(5) -0.014(3) -0.009(4) 0.007(3) C28 0.102(7) 0.029(3) 0.108(7) -0.012(4) -0.034(5) 0.012(4) C29 0.083(5) 0.033(3) 0.074(5) 0.017(4) -0.015(4) -0.009(3) C30 0.050(4) 0.030(3) 0.042(4) 0.009(3) 0.001(3) -0.001(3) C31 0.033(3) 0.030(3) 0.036(3) -0.001(2) -0.001(2) -0.001(2) C32 0.054(4) 0.040(3) 0.041(4) 0.001(3) -0.011(3) -0.009(3) C33 0.051(4) 0.071(5) 0.069(5) -0.001(4) -0.019(4) -0.009(4) C34 0.058(5) 0.072(5) 0.085(6) 0.020(4) -0.028(4) -0.002(4) C35 0.051(4) 0.047(4) 0.081(5) 0.018(3) -0.010(4) -0.006(4) C36 0.042(3) 0.031(3) 0.046(4) 0.006(3) -0.002(3) 0.003(3) C37 0.029(3) 0.028(3) 0.027(3) 0.005(2) 0.003(2) 0.006(2) C38 0.045(3) 0.031(3) 0.041(3) 0.002(3) 0.017(3) 0.000(2) C39 0.042(4) 0.045(3) 0.047(4) 0.002(3) 0.023(3) -0.002(3) C40 0.048(4) 0.045(3) 0.045(4) -0.011(3) 0.019(3) 0.001(3) C41 0.043(4) 0.032(3) 0.051(4) -0.003(3) 0.008(3) 0.001(3) C42 0.037(3) 0.036(3) 0.035(3) 0.001(3) 0.006(3) 0.002(2) C43 0.044(3) 0.043(3) 0.033(3) 0.011(3) 0.011(3) 0.012(3) C44 0.048(4) 0.059(4) 0.052(4) 0.016(3) 0.015(3) 0.007(3) C45 0.042(4) 0.084(5) 0.067(5) 0.030(4) 0.014(4) 0.009(4) C46 0.038(4) 0.100(6) 0.072(5) 0.006(4) 0.000(4) 0.005(5) C47 0.042(4) 0.070(4) 0.048(4) -0.004(3) 0.000(3) 0.006(3) C48 0.036(3) 0.044(3) 0.040(4) 0.004(3) 0.011(3) 0.007(3) C49 0.030(3) 0.035(3) 0.033(3) -0.002(2) 0.009(2) 0.000(2) C50 0.042(3) 0.043(3) 0.034(3) -0.004(3) 0.005(3) -0.005(3) C51 0.050(4) 0.061(4) 0.037(4) 0.001(3) 0.008(3) -0.006(3) C52 0.041(4) 0.065(4) 0.035(4) -0.003(3) -0.005(3) 0.004(3) C53 0.037(3) 0.048(4) 0.048(4) 0.005(3) -0.001(3) 0.007(3) C54 0.035(3) 0.035(3) 0.038(3) -0.006(3) 0.005(3) 0.001(2) C55 0.038(3) 0.027(3) 0.031(3) 0.001(2) 0.013(2) -0.002(2) C56 0.044(4) 0.036(3) 0.039(3) 0.006(3) 0.012(3) 0.003(3) C57 0.068(5) 0.040(3) 0.055(4) 0.019(3) 0.021(4) 0.011(3) C58 0.099(6) 0.028(3) 0.060(5) 0.017(3) 0.029(4) 0.011(3) C59 0.087(5) 0.028(3) 0.066(5) -0.009(3) 0.036(4) -0.002(3) C60 0.058(4) 0.032(3) 0.049(4) -0.007(3) 0.017(3) -0.009(3) C61 0.049(4) 0.029(3) 0.041(4) 0.008(3) 0.014(3) 0.002(2) C62 0.056(4) 0.036(3) 0.039(4) 0.005(3) 0.012(3) -0.006(3) C63 0.063(5) 0.046(4) 0.060(5) -0.003(3) 0.016(4) -0.015(3) C64 0.100(6) 0.034(4) 0.085(6) -0.010(4) 0.045(5) -0.011(4) C65 0.112(7) 0.030(3) 0.073(5) 0.016(4) 0.041(5) 0.017(3) C66 0.066(4) 0.039(3) 0.050(4) 0.011(3) 0.017(3) 0.008(3) C67 0.043(3) 0.036(3) 0.029(3) 0.000(3) 0.013(3) 0.003(2) C68 0.058(4) 0.037(3) 0.041(4) 0.000(3) 0.020(3) 0.005(3) C69 0.067(5) 0.050(4) 0.049(4) 0.011(3) 0.025(4) 0.014(3) C70 0.089(5) 0.059(4) 0.049(4) 0.007(4) 0.036(4) 0.017(3) C71 0.059(4) 0.070(4) 0.041(4) 0.010(4) 0.023(3) 0.010(3) C72 0.053(4) 0.047(3) 0.038(4) 0.002(3) 0.017(3) -0.001(3) C73 0.032(3) 0.042(3) 0.048(4) 0.004(3) 0.006(3) 0.003(3) C74 0.048(4) 0.045(3) 0.044(4) -0.001(3) 0.004(3) 0.005(3) C75 0.036(4) 0.062(4) 0.050(4) -0.001(3) 0.009(3) 0.004(3) C76 0.049(4) 0.069(4) 0.047(4) 0.014(3) 0.008(3) 0.000(3) C77 0.045(4) 0.052(4) 0.054(4) 0.014(3) -0.001(3) -0.002(3) C78 0.040(4) 0.047(4) 0.053(4) 0.002(3) -0.003(3) 0.008(3) C79 0.046(4) 0.043(3) 0.032(3) -0.006(3) 0.008(3) 0.001(3) C80 0.054(4) 0.047(4) 0.037(4) -0.010(3) 0.009(3) 0.001(3) C81 0.076(5) 0.052(4) 0.049(4) -0.022(4) 0.008(4) -0.006(3) C82 0.096(6) 0.041(4) 0.058(5) -0.004(4) 0.018(4) -0.001(3) C83 0.069(5) 0.050(4) 0.052(4) 0.007(4) 0.015(4) -0.007(3) C84 0.066(4) 0.036(3) 0.036(4) 0.003(3) 0.012(3) -0.003(3) C85 0.039(4) 0.053(4) 0.046(4) -0.002(3) 0.005(3) 0.010(3) C86 0.046(4) 0.095(5) 0.048(4) -0.011(4) -0.003(3) 0.020(4) C87 0.059(5) 0.126(7) 0.045(4) -0.011(5) -0.003(4) 0.037(5) C88 0.082(6) 0.101(6) 0.048(5) 0.002(5) 0.017(4) 0.016(4) C89 0.051(4) 0.082(5) 0.061(5) 0.003(4) 0.017(4) 0.015(4) C90 0.039(4) 0.067(4) 0.042(4) 0.003(3) 0.006(3) 0.008(3) C91 0.152(9) 0.080(6) 0.114(8) 0.000(6) 0.067(7) 0.025(6) C92 0.198(13) 0.141(10) 0.089(8) 0.075(9) 0.042(8) 0.031(7) C93 0.220(15) 0.051(6) 0.35(2) -0.044(8) 0.091(14) 0.037(9) C94 0.143(12) 0.108(10) 0.42(3) -0.042(9) 0.139(15) -0.055(13) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag P2 Ru1 P1 . . 173.08(5) yes P2 Ru1 Cl1 . . 90.86(5) yes P1 Ru1 Cl1 . . 93.82(5) yes P2 Ru1 Cl2 . . 94.63(5) yes P1 Ru1 Cl2 . . 90.67(5) yes Cl1 Ru1 Cl2 . . 87.48(5) yes P2 Ru1 Br1 . . 82.87(4) yes P1 Ru1 Br1 . . 91.73(4) yes Cl1 Ru1 Br1 . . 93.73(4) yes Cl2 Ru1 Br1 . . 177.22(4) yes P2 Ru1 Br2 . . 92.70(4) yes P1 Ru1 Br2 . . 82.54(4) yes Cl1 Ru1 Br2 . . 176.29(4) ? Cl2 Ru1 Br2 . . 93.26(4) ? Br1 Ru1 Br2 . . 85.69(2) ? P3 Ru2 P4 . . 173.11(5) ? P3 Ru2 Cl3 . . 93.94(5) ? P4 Ru2 Cl3 . . 90.46(5) ? P3 Ru2 Cl4 . . 89.60(5) ? P4 Ru2 Cl4 . . 95.86(5) ? Cl3 Ru2 Cl4 . . 88.10(5) ? P3 Ru2 Br3 . . 92.06(4) ? P4 Ru2 Br3 . . 82.41(4) ? Cl3 Ru2 Br3 . . 92.90(4) ? Cl4 Ru2 Br3 . . 178.00(4) ? P3 Ru2 Br4 . . 82.78(4) ? P4 Ru2 Br4 . . 92.73(4) ? Cl3 Ru2 Br4 . . 176.60(4) ? Cl4 Ru2 Br4 . . 92.73(4) ? Br3 Ru2 Br4 . . 86.38(2) ? Cl5 Ru3 Cl5 2_556 . 87.30(9) ? Cl5 Ru3 P5 2_556 2_556 97.09(6) ? Cl5 Ru3 P5 . 2_556 87.64(6) ? Cl5 Ru3 P5 2_556 . 87.64(6) ? Cl5 Ru3 P5 . . 97.09(6) ? P5 Ru3 P5 2_556 . 173.48(8) ? Cl5 Ru3 Br5 2_556 . 94.62(5) ? Cl5 Ru3 Br5 . . 176.85(5) ? P5 Ru3 Br5 2_556 . 94.60(4) ? P5 Ru3 Br5 . . 80.51(4) ? Cl5 Ru3 Br5 2_556 2_556 176.85(5) ? Cl5 Ru3 Br5 . 2_556 94.62(5) ? P5 Ru3 Br5 2_556 2_556 80.51(4) ? P5 Ru3 Br5 . 2_556 94.59(4) ? Br5 Ru3 Br5 . 2_556 83.58(4) ? C12 Br1 Ru1 . . 101.88(16) ? C18 Br2 Ru1 . . 100.45(16) ? C48 Br3 Ru2 . . 101.92(18) ? C54 Br4 Ru2 . . 100.96(16) ? C84 Br5 Ru3 . . 99.74(17) ? C13 P1 C19 . . 102.8(2) ? C13 P1 C1 . . 101.7(2) ? C19 P1 C1 . . 103.9(2) ? C13 P1 Ru1 . . 104.95(17) ? C19 P1 Ru1 . . 120.52(19) ? C1 P1 Ru1 . . 120.05(17) ? C7 P2 C25 . . 105.3(2) ? C7 P2 C31 . . 100.6(2) ? C25 P2 C31 . . 103.5(2) ? C7 P2 Ru1 . . 105.69(18) ? C25 P2 Ru1 . . 119.25(18) ? C31 P2 Ru1 . . 120.09(17) ? C49 P3 C55 . . 105.0(2) ? C49 P3 C37 . . 100.0(2) ? C55 P3 C37 . . 103.0(2) ? C49 P3 Ru2 . . 105.41(17) ? C55 P3 Ru2 . . 121.00(17) ? C37 P3 Ru2 . . 119.63(16) ? C43 P4 C61 . . 105.3(3) ? C43 P4 C67 . . 99.8(2) ? C61 P4 C67 . . 104.1(2) ? C43 P4 Ru2 . . 106.10(18) ? C61 P4 Ru2 . . 120.37(19) ? C67 P4 Ru2 . . 118.58(17) ? C73 P5 C79 . . 104.9(3) ? C73 P5 C85 . . 103.4(3) ? C79 P5 C85 . . 101.8(3) ? C73 P5 Ru3 . . 118.7(2) ? C79 P5 Ru3 . . 105.30(19) ? C85 P5 Ru3 . . 120.47(19) ? C91 O1 H1 . . 109.5 ? C92 O2 H2 . . 109.5 ? C93 O3 H3 . . 109.5 ? C94 O4 H4 . . 109.5 ? C6 C1 C2 . . 109.1(4) ? C6 C1 P1 . . 111.6(4) ? C2 C1 P1 . . 115.0(4) ? C6 C1 H1A . . 106.9 ? C2 C1 H1A . . 106.9 ? P1 C1 H1A . . 106.9 ? C3 C2 C1 . . 111.5(5) ? C3 C2 H2A . . 109.3 ? C1 C2 H2A . . 109.3 ? C3 C2 H2B . . 109.3 ? C1 C2 H2B . . 109.3 ? H2A C2 H2B . . 108.0 ? C4 C3 C2 . . 112.0(5) ? C4 C3 H3A . . 109.2 ? C2 C3 H3A . . 109.2 ? C4 C3 H3B . . 109.2 ? C2 C3 H3B . . 109.2 ? H3A C3 H3B . . 107.9 ? C3 C4 C5 . . 110.5(5) ? C3 C4 H4A . . 109.6 ? C5 C4 H4A . . 109.6 ? C3 C4 H4B . . 109.6 ? C5 C4 H4B . . 109.6 ? H4A C4 H4B . . 108.1 ? C4 C5 C6 . . 112.1(5) ? C4 C5 H5A . . 109.2 ? C6 C5 H5A . . 109.2 ? C4 C5 H5B . . 109.2 ? C6 C5 H5B . . 109.2 ? H5A C5 H5B . . 107.9 ? C5 C6 C1 . . 111.2(5) ? C5 C6 H6A . . 109.4 ? C1 C6 H6A . . 109.4 ? C5 C6 H6B . . 109.4 ? C1 C6 H6B . . 109.4 ? H6A C6 H6B . . 108.0 ? C12 C7 C8 . . 115.8(5) ? C12 C7 P2 . . 119.8(4) ? C8 C7 P2 . . 123.8(4) ? C9 C8 C7 . . 120.8(6) ? C9 C8 H8 . . 119.6 ? C7 C8 H8 . . 119.6 ? C10 C9 C8 . . 120.6(6) ? C10 C9 H9 . . 119.7 ? C8 C9 H9 . . 119.7 ? C9 C10 C11 . . 120.2(6) ? C9 C10 H10 . . 119.9 ? C11 C10 H10 . . 119.9 ? C12 C11 C10 . . 118.0(6) ? C12 C11 H11 . . 121.0 ? C10 C11 H11 . . 121.0 ? C11 C12 C7 . . 124.5(5) ? C11 C12 Br1 . . 116.7(4) ? C7 C12 Br1 . . 118.8(4) ? C18 C13 C14 . . 115.9(5) ? C18 C13 P1 . . 119.6(4) ? C14 C13 P1 . . 124.5(4) ? C15 C14 C13 . . 121.2(5) ? C15 C14 H14 . . 119.4 ? C13 C14 H14 . . 119.4 ? C16 C15 C14 . . 120.1(6) ? C16 C15 H15 . . 120.0 ? C14 C15 H15 . . 120.0 ? C15 C16 C17 . . 120.9(6) ? C15 C16 H16 . . 119.6 ? C17 C16 H16 . . 119.6 ? C16 C17 C18 . . 117.8(6) ? C16 C17 H17 . . 121.1 ? C18 C17 H17 . . 121.1 ? C17 C18 C13 . . 124.2(5) ? C17 C18 Br2 . . 117.1(4) ? C13 C18 Br2 . . 118.6(4) ? C24 C19 C20 . . 110.4(5) ? C24 C19 P1 . . 112.1(4) ? C20 C19 P1 . . 111.6(4) ? C24 C19 H19 . . 107.5 ? C20 C19 H19 . . 107.5 ? P1 C19 H19 . . 107.5 ? C21 C20 C19 . . 108.9(6) ? C21 C20 H20A . . 109.9 ? C19 C20 H20A . . 109.9 ? C21 C20 H20B . . 109.9 ? C19 C20 H20B . . 109.9 ? H20A C20 H20B . . 108.3 ? C22 C21 C20 . . 112.0(6) ? C22 C21 H21A . . 109.2 ? C20 C21 H21A . . 109.2 ? C22 C21 H21B . . 109.2 ? C20 C21 H21B . . 109.2 ? H21A C21 H21B . . 107.9 ? C21 C22 C23 . . 112.4(7) ? C21 C22 H22A . . 109.1 ? C23 C22 H22A . . 109.1 ? C21 C22 H22B . . 109.1 ? C23 C22 H22B . . 109.1 ? H22A C22 H22B . . 107.9 ? C24 C23 C22 . . 110.8(6) ? C24 C23 H23A . . 109.5 ? C22 C23 H23A . . 109.5 ? C24 C23 H23B . . 109.5 ? C22 C23 H23B . . 109.5 ? H23A C23 H23B . . 108.1 ? C23 C24 C19 . . 110.5(5) ? C23 C24 H24A . . 109.6 ? C19 C24 H24A . . 109.6 ? C23 C24 H24B . . 109.6 ? C19 C24 H24B . . 109.6 ? H24A C24 H24B . . 108.1 ? C30 C25 C26 . . 111.0(4) ? C30 C25 P2 . . 112.1(4) ? C26 C25 P2 . . 111.1(4) ? C30 C25 H25 . . 107.5 ? C26 C25 H25 . . 107.5 ? P2 C25 H25 . . 107.5 ? C27 C26 C25 . . 110.4(5) ? C27 C26 H26A . . 109.6 ? C25 C26 H26A . . 109.6 ? C27 C26 H26B . . 109.6 ? C25 C26 H26B . . 109.6 ? H26A C26 H26B . . 108.1 ? C26 C27 C28 . . 110.7(5) ? C26 C27 H27A . . 109.5 ? C28 C27 H27A . . 109.5 ? C26 C27 H27B . . 109.5 ? C28 C27 H27B . . 109.5 ? H27A C27 H27B . . 108.1 ? C29 C28 C27 . . 111.4(6) ? C29 C28 H28A . . 109.3 ? C27 C28 H28A . . 109.3 ? C29 C28 H28B . . 109.3 ? C27 C28 H28B . . 109.3 ? H28A C28 H28B . . 108.0 ? C28 C29 C30 . . 111.0(6) ? C28 C29 H29A . . 109.4 ? C30 C29 H29A . . 109.4 ? C28 C29 H29B . . 109.4 ? C30 C29 H29B . . 109.4 ? H29A C29 H29B . . 108.0 ? C29 C30 C25 . . 111.2(5) ? C29 C30 H30A . . 109.4 ? C25 C30 H30A . . 109.4 ? C29 C30 H30B . . 109.4 ? C25 C30 H30B . . 109.4 ? H30A C30 H30B . . 108.0 ? C36 C31 C32 . . 108.0(4) ? C36 C31 P2 . . 112.1(4) ? C32 C31 P2 . . 116.4(4) ? C36 C31 H31 . . 106.6 ? C32 C31 H31 . . 106.6 ? P2 C31 H31 . . 106.6 ? C33 C32 C31 . . 111.4(5) ? C33 C32 H32A . . 109.4 ? C31 C32 H32A . . 109.4 ? C33 C32 H32B . . 109.4 ? C31 C32 H32B . . 109.4 ? H32A C32 H32B . . 108.0 ? C34 C33 C32 . . 110.5(5) ? C34 C33 H33A . . 109.6 ? C32 C33 H33A . . 109.6 ? C34 C33 H33B . . 109.6 ? C32 C33 H33B . . 109.6 ? H33A C33 H33B . . 108.1 ? C35 C34 C33 . . 111.2(6) ? C35 C34 H34A . . 109.4 ? C33 C34 H34A . . 109.4 ? C35 C34 H34B . . 109.4 ? C33 C34 H34B . . 109.4 ? H34A C34 H34B . . 108.0 ? C34 C35 C36 . . 111.0(5) ? C34 C35 H35A . . 109.4 ? C36 C35 H35A . . 109.4 ? C34 C35 H35B . . 109.4 ? C36 C35 H35B . . 109.4 ? H35A C35 H35B . . 108.0 ? C35 C36 C31 . . 111.2(5) ? C35 C36 H36A . . 109.4 ? C31 C36 H36A . . 109.4 ? C35 C36 H36B . . 109.4 ? C31 C36 H36B . . 109.4 ? H36A C36 H36B . . 108.0 ? C38 C37 C42 . . 108.2(4) ? C38 C37 P3 . . 114.6(3) ? C42 C37 P3 . . 113.0(3) ? C38 C37 H37 . . 106.9 ? C42 C37 H37 . . 106.9 ? P3 C37 H37 . . 106.9 ? C39 C38 C37 . . 111.7(4) ? C39 C38 H38A . . 109.3 ? C37 C38 H38A . . 109.3 ? C39 C38 H38B . . 109.3 ? C37 C38 H38B . . 109.3 ? H38A C38 H38B . . 107.9 ? C40 C39 C38 . . 112.0(5) ? C40 C39 H39A . . 109.2 ? C38 C39 H39A . . 109.2 ? C40 C39 H39B . . 109.2 ? C38 C39 H39B . . 109.2 ? H39A C39 H39B . . 107.9 ? C39 C40 C41 . . 110.6(4) ? C39 C40 H40A . . 109.5 ? C41 C40 H40A . . 109.5 ? C39 C40 H40B . . 109.5 ? C41 C40 H40B . . 109.5 ? H40A C40 H40B . . 108.1 ? C40 C41 C42 . . 111.7(4) ? C40 C41 H41A . . 109.3 ? C42 C41 H41A . . 109.3 ? C40 C41 H41B . . 109.3 ? C42 C41 H41B . . 109.3 ? H41A C41 H41B . . 107.9 ? C41 C42 C37 . . 110.6(4) ? C41 C42 H42A . . 109.5 ? C37 C42 H42A . . 109.5 ? C41 C42 H42B . . 109.5 ? C37 C42 H42B . . 109.5 ? H42A C42 H42B . . 108.1 ? C48 C43 C44 . . 116.0(6) ? C48 C43 P4 . . 119.3(4) ? C44 C43 P4 . . 124.2(5) ? C45 C44 C43 . . 120.9(6) ? C45 C44 H44 . . 119.5 ? C43 C44 H44 . . 119.5 ? C46 C45 C44 . . 121.2(6) ? C46 C45 H45 . . 119.4 ? C44 C45 H45 . . 119.4 ? C45 C46 C47 . . 119.8(7) ? C45 C46 H46 . . 120.1 ? C47 C46 H46 . . 120.1 ? C46 C47 C48 . . 118.3(7) ? C46 C47 H47 . . 120.8 ? C48 C47 H47 . . 120.8 ? C47 C48 C43 . . 123.6(6) ? C47 C48 Br3 . . 117.5(5) ? C43 C48 Br3 . . 118.9(4) ? C54 C49 C50 . . 116.2(5) ? C54 C49 P3 . . 119.6(4) ? C50 C49 P3 . . 123.9(4) ? C51 C50 C49 . . 121.8(5) ? C51 C50 H50 . . 119.1 ? C49 C50 H50 . . 119.1 ? C50 C51 C52 . . 119.6(6) ? C50 C51 H51 . . 120.2 ? C52 C51 H51 . . 120.2 ? C51 C52 C53 . . 120.6(6) ? C51 C52 H52 . . 119.7 ? C53 C52 H52 . . 119.7 ? C54 C53 C52 . . 117.7(5) ? C54 C53 H53 . . 121.1 ? C52 C53 H53 . . 121.1 ? C53 C54 C49 . . 124.0(5) ? C53 C54 Br4 . . 117.6(4) ? C49 C54 Br4 . . 118.4(4) ? C60 C55 C56 . . 110.2(4) ? C60 C55 P3 . . 111.9(3) ? C56 C55 P3 . . 110.8(3) ? C60 C55 H55 . . 108.0 ? C56 C55 H55 . . 108.0 ? P3 C55 H55 . . 108.0 ? C57 C56 C55 . . 110.9(5) ? C57 C56 H56A . . 109.5 ? C55 C56 H56A . . 109.5 ? C57 C56 H56B . . 109.5 ? C55 C56 H56B . . 109.5 ? H56A C56 H56B . . 108.0 ? C58 C57 C56 . . 111.4(5) ? C58 C57 H57A . . 109.3 ? C56 C57 H57A . . 109.3 ? C58 C57 H57B . . 109.3 ? C56 C57 H57B . . 109.3 ? H57A C57 H57B . . 108.0 ? C59 C58 C57 . . 110.8(5) ? C59 C58 H58A . . 109.5 ? C57 C58 H58A . . 109.5 ? C59 C58 H58B . . 109.5 ? C57 C58 H58B . . 109.5 ? H58A C58 H58B . . 108.1 ? C58 C59 C60 . . 112.4(5) ? C58 C59 H59A . . 109.1 ? C60 C59 H59A . . 109.1 ? C58 C59 H59B . . 109.1 ? C60 C59 H59B . . 109.1 ? H59A C59 H59B . . 107.8 ? C55 C60 C59 . . 110.3(5) ? C55 C60 H60A . . 109.6 ? C59 C60 H60A . . 109.6 ? C55 C60 H60B . . 109.6 ? C59 C60 H60B . . 109.6 ? H60A C60 H60B . . 108.1 ? C62 C61 C66 . . 110.4(5) ? C62 C61 P4 . . 110.5(4) ? C66 C61 P4 . . 112.5(4) ? C62 C61 H61 . . 107.7 ? C66 C61 H61 . . 107.7 ? P4 C61 H61 . . 107.7 ? C61 C62 C63 . . 111.7(5) ? C61 C62 H62A . . 109.3 ? C63 C62 H62A . . 109.3 ? C61 C62 H62B . . 109.3 ? C63 C62 H62B . . 109.3 ? H62A C62 H62B . . 107.9 ? C64 C63 C62 . . 110.3(5) ? C64 C63 H63A . . 109.6 ? C62 C63 H63A . . 109.6 ? C64 C63 H63B . . 109.6 ? C62 C63 H63B . . 109.6 ? H63A C63 H63B . . 108.1 ? C63 C64 C65 . . 111.1(6) ? C63 C64 H64A . . 109.4 ? C65 C64 H64A . . 109.4 ? C63 C64 H64B . . 109.4 ? C65 C64 H64B . . 109.4 ? H64A C64 H64B . . 108.0 ? C64 C65 C66 . . 111.5(6) ? C64 C65 H65A . . 109.3 ? C66 C65 H65A . . 109.3 ? C64 C65 H65B . . 109.3 ? C66 C65 H65B . . 109.3 ? H65A C65 H65B . . 108.0 ? C65 C66 C61 . . 111.4(5) ? C65 C66 H66A . . 109.3 ? C61 C66 H66A . . 109.3 ? C65 C66 H66B . . 109.3 ? C61 C66 H66B . . 109.3 ? H66A C66 H66B . . 108.0 ? C72 C67 C68 . . 108.7(4) ? C72 C67 P4 . . 116.0(4) ? C68 C67 P4 . . 113.0(4) ? C72 C67 H67 . . 106.1 ? C68 C67 H67 . . 106.1 ? P4 C67 H67 . . 106.1 ? C69 C68 C67 . . 111.6(5) ? C69 C68 H68A . . 109.3 ? C67 C68 H68A . . 109.3 ? C69 C68 H68B . . 109.3 ? C67 C68 H68B . . 109.3 ? H68A C68 H68B . . 108.0 ? C68 C69 C70 . . 110.8(5) ? C68 C69 H69A . . 109.5 ? C70 C69 H69A . . 109.5 ? C68 C69 H69B . . 109.5 ? C70 C69 H69B . . 109.5 ? H69A C69 H69B . . 108.1 ? C69 C70 C71 . . 111.7(5) ? C69 C70 H70A . . 109.3 ? C71 C70 H70A . . 109.3 ? C69 C70 H70B . . 109.3 ? C71 C70 H70B . . 109.3 ? H70A C70 H70B . . 107.9 ? C72 C71 C70 . . 111.2(5) ? C72 C71 H71A . . 109.4 ? C70 C71 H71A . . 109.4 ? C72 C71 H71B . . 109.4 ? C70 C71 H71B . . 109.4 ? H71A C71 H71B . . 108.0 ? C71 C72 C67 . . 111.0(5) ? C71 C72 H72A . . 109.4 ? C67 C72 H72A . . 109.4 ? C71 C72 H72B . . 109.4 ? C67 C72 H72B . . 109.4 ? H72A C72 H72B . . 108.0 ? C74 C73 C78 . . 111.1(5) ? C74 C73 P5 . . 110.8(4) ? C78 C73 P5 . . 109.3(4) ? C74 C73 H73 . . 108.5 ? C78 C73 H73 . . 108.5 ? P5 C73 H73 . . 108.5 ? C75 C74 C73 . . 111.2(5) ? C75 C74 H74A . . 109.4 ? C73 C74 H74A . . 109.4 ? C75 C74 H74B . . 109.4 ? C73 C74 H74B . . 109.4 ? H74A C74 H74B . . 108.0 ? C74 C75 C76 . . 110.9(5) ? C74 C75 H75A . . 109.5 ? C76 C75 H75A . . 109.5 ? C74 C75 H75B . . 109.5 ? C76 C75 H75B . . 109.5 ? H75A C75 H75B . . 108.0 ? C77 C76 C75 . . 110.1(5) ? C77 C76 H76A . . 109.6 ? C75 C76 H76A . . 109.6 ? C77 C76 H76B . . 109.6 ? C75 C76 H76B . . 109.6 ? H76A C76 H76B . . 108.1 ? C76 C77 C78 . . 112.1(5) ? C76 C77 H77A . . 109.2 ? C78 C77 H77A . . 109.2 ? C76 C77 H77B . . 109.2 ? C78 C77 H77B . . 109.2 ? H77A C77 H77B . . 107.9 ? C77 C78 C73 . . 111.9(5) ? C77 C78 H78A . . 109.2 ? C73 C78 H78A . . 109.2 ? C77 C78 H78B . . 109.2 ? C73 C78 H78B . . 109.2 ? H78A C78 H78B . . 107.9 ? C80 C79 C84 . . 116.6(5) ? C80 C79 P5 . . 125.1(5) ? C84 C79 P5 . . 118.3(4) ? C81 C80 C79 . . 121.2(6) ? C81 C80 H80 . . 119.4 ? C79 C80 H80 . . 119.4 ? C82 C81 C80 . . 120.1(6) ? C82 C81 H81 . . 120.0 ? C80 C81 H81 . . 120.0 ? C81 C82 C83 . . 120.0(6) ? C81 C82 H82 . . 120.0 ? C83 C82 H82 . . 120.0 ? C84 C83 C82 . . 119.5(6) ? C84 C83 H83 . . 120.3 ? C82 C83 H83 . . 120.3 ? C83 C84 C79 . . 122.6(6) ? C83 C84 Br5 . . 119.1(5) ? C79 C84 Br5 . . 118.3(4) ? C86 C85 C90 . . 110.0(5) ? C86 C85 P5 . . 114.3(4) ? C90 C85 P5 . . 112.7(4) ? C86 C85 H85 . . 106.4 ? C90 C85 H85 . . 106.4 ? P5 C85 H85 . . 106.4 ? C85 C86 C87 . . 110.2(5) ? C85 C86 H86A . . 109.6 ? C87 C86 H86A . . 109.6 ? C85 C86 H86B . . 109.6 ? C87 C86 H86B . . 109.6 ? H86A C86 H86B . . 108.1 ? C88 C87 C86 . . 111.5(6) ? C88 C87 H87A . . 109.3 ? C86 C87 H87A . . 109.3 ? C88 C87 H87B . . 109.3 ? C86 C87 H87B . . 109.3 ? H87A C87 H87B . . 108.0 ? C89 C88 C87 . . 109.8(6) ? C89 C88 H88A . . 109.7 ? C87 C88 H88A . . 109.7 ? C89 C88 H88B . . 109.7 ? C87 C88 H88B . . 109.7 ? H88A C88 H88B . . 108.2 ? C88 C89 C90 . . 112.2(6) ? C88 C89 H89A . . 109.2 ? C90 C89 H89A . . 109.2 ? C88 C89 H89B . . 109.2 ? C90 C89 H89B . . 109.2 ? H89A C89 H89B . . 107.9 ? C89 C90 C85 . . 111.2(5) ? C89 C90 H90A . . 109.4 ? C85 C90 H90A . . 109.4 ? C89 C90 H90B . . 109.4 ? C85 C90 H90B . . 109.4 ? H90A C90 H90B . . 108.0 ? O1 C91 H91A . . 109.5 ? O1 C91 H91B . . 109.5 ? H91A C91 H91B . . 109.5 ? O1 C91 H91C . . 109.5 ? H91A C91 H91C . . 109.5 ? H91B C91 H91C . . 109.5 ? O2 C92 H92A . . 109.5 ? O2 C92 H92B . . 109.5 ? H92A C92 H92B . . 109.5 ? O2 C92 H92C . . 109.5 ? H92A C92 H92C . . 109.5 ? H92B C92 H92C . . 109.5 ? O3 C93 H93A . . 109.5 ? O3 C93 H93B . . 109.5 ? H93A C93 H93B . . 109.5 ? O3 C93 H93C . . 109.5 ? H93A C93 H93C . . 109.5 ? H93B C93 H93C . . 109.5 ? O4 C94 H94A . . 109.5 ? O4 C94 H94B . . 109.5 ? H94A C94 H94B . . 109.5 ? O4 C94 H94C . . 109.5 ? H94A C94 H94C . . 109.5 ? H94B C94 H94C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Ru1 P2 . 2.3781(14) ? Ru1 P1 . 2.3795(15) ? Ru1 Cl1 . 2.3873(14) ? Ru1 Cl2 . 2.3884(14) ? Ru1 Br1 . 2.4954(7) ? Ru1 Br2 . 2.5091(7) ? Ru2 P3 . 2.3536(14) ? Ru2 P4 . 2.3843(14) ? Ru2 Cl3 . 2.3864(14) ? Ru2 Cl4 . 2.3891(15) ? Ru2 Br3 . 2.5137(7) ? Ru2 Br4 . 2.5168(7) ? Ru3 Cl5 2_556 2.3811(16) ? Ru3 Cl5 . 2.3811(16) ? Ru3 P5 2_556 2.3954(15) ? Ru3 P5 . 2.3954(15) ? Ru3 Br5 . 2.5325(8) ? Ru3 Br5 2_556 2.5325(8) ? Br1 C12 . 1.927(6) ? Br2 C18 . 1.932(5) ? Br3 C48 . 1.927(5) ? Br4 C54 . 1.934(5) ? Br5 C84 . 1.927(6) ? P1 C13 . 1.846(5) ? P1 C19 . 1.852(5) ? P1 C1 . 1.866(5) ? P2 C7 . 1.840(5) ? P2 C25 . 1.847(5) ? P2 C31 . 1.855(5) ? P3 C49 . 1.843(5) ? P3 C55 . 1.854(5) ? P3 C37 . 1.871(5) ? P4 C43 . 1.840(6) ? P4 C61 . 1.847(5) ? P4 C67 . 1.861(5) ? P5 C73 . 1.845(5) ? P5 C79 . 1.847(6) ? P5 C85 . 1.863(6) ? O1 C91 . 1.329(9) ? O1 H1 . 0.8200 ? O2 C92 . 1.349(9) ? O2 H2 . 0.8200 ? O3 C93 . 1.370(11) ? O3 H3 . 0.8200 ? O4 C94 . 1.298(11) ? O4 H4 . 0.8200 ? C1 C6 . 1.531(7) ? C1 C2 . 1.538(7) ? C1 H1A . 0.9800 ? C2 C3 . 1.522(8) ? C2 H2A . 0.9700 ? C2 H2B . 0.9700 ? C3 C4 . 1.514(9) ? C3 H3A . 0.9700 ? C3 H3B . 0.9700 ? C4 C5 . 1.514(8) ? C4 H4A . 0.9700 ? C4 H4B . 0.9700 ? C5 C6 . 1.530(7) ? C5 H5A . 0.9700 ? C5 H5B . 0.9700 ? C6 H6A . 0.9700 ? C6 H6B . 0.9700 ? C7 C12 . 1.375(7) ? C7 C8 . 1.400(7) ? C8 C9 . 1.388(8) ? C8 H8 . 0.9300 ? C9 C10 . 1.365(8) ? C9 H9 . 0.9300 ? C10 C11 . 1.378(8) ? C10 H10 . 0.9300 ? C11 C12 . 1.373(7) ? C11 H11 . 0.9300 ? C13 C18 . 1.385(7) ? C13 C14 . 1.402(7) ? C14 C15 . 1.384(7) ? C14 H14 . 0.9300 ? C15 C16 . 1.375(8) ? C15 H15 . 0.9300 ? C16 C17 . 1.376(8) ? C16 H16 . 0.9300 ? C17 C18 . 1.378(7) ? C17 H17 . 0.9300 ? C19 C24 . 1.522(8) ? C19 C20 . 1.538(8) ? C19 H19 . 0.9800 ? C20 C21 . 1.532(9) ? C20 H20A . 0.9700 ? C20 H20B . 0.9700 ? C21 C22 . 1.496(11) ? C21 H21A . 0.9700 ? C21 H21B . 0.9700 ? C22 C23 . 1.517(11) ? C22 H22A . 0.9700 ? C22 H22B . 0.9700 ? C23 C24 . 1.507(8) ? C23 H23A . 0.9700 ? C23 H23B . 0.9700 ? C24 H24A . 0.9700 ? C24 H24B . 0.9700 ? C25 C30 . 1.528(7) ? C25 C26 . 1.528(7) ? C25 H25 . 0.9800 ? C26 C27 . 1.520(7) ? C26 H26A . 0.9700 ? C26 H26B . 0.9700 ? C27 C28 . 1.523(9) ? C27 H27A . 0.9700 ? C27 H27B . 0.9700 ? C28 C29 . 1.503(10) ? C28 H28A . 0.9700 ? C28 H28B . 0.9700 ? C29 C30 . 1.528(7) ? C29 H29A . 0.9700 ? C29 H29B . 0.9700 ? C30 H30A . 0.9700 ? C30 H30B . 0.9700 ? C31 C36 . 1.537(7) ? C31 C32 . 1.540(7) ? C31 H31 . 0.9800 ? C32 C33 . 1.536(8) ? C32 H32A . 0.9700 ? C32 H32B . 0.9700 ? C33 C34 . 1.518(9) ? C33 H33A . 0.9700 ? C33 H33B . 0.9700 ? C34 C35 . 1.505(9) ? C34 H34A . 0.9700 ? C34 H34B . 0.9700 ? C35 C36 . 1.518(7) ? C35 H35A . 0.9700 ? C35 H35B . 0.9700 ? C36 H36A . 0.9700 ? C36 H36B . 0.9700 ? C37 C38 . 1.529(7) ? C37 C42 . 1.532(6) ? C37 H37 . 0.9800 ? C38 C39 . 1.521(7) ? C38 H38A . 0.9700 ? C38 H38B . 0.9700 ? C39 C40 . 1.519(7) ? C39 H39A . 0.9700 ? C39 H39B . 0.9700 ? C40 C41 . 1.526(7) ? C40 H40A . 0.9700 ? C40 H40B . 0.9700 ? C41 C42 . 1.526(7) ? C41 H41A . 0.9700 ? C41 H41B . 0.9700 ? C42 H42A . 0.9700 ? C42 H42B . 0.9700 ? C43 C48 . 1.386(8) ? C43 C44 . 1.398(7) ? C44 C45 . 1.376(9) ? C44 H44 . 0.9300 ? C45 C46 . 1.369(9) ? C45 H45 . 0.9300 ? C46 C47 . 1.378(9) ? C46 H46 . 0.9300 ? C47 C48 . 1.382(8) ? C47 H47 . 0.9300 ? C49 C54 . 1.380(7) ? C49 C50 . 1.393(7) ? C50 C51 . 1.380(8) ? C50 H50 . 0.9300 ? C51 C52 . 1.381(8) ? C51 H51 . 0.9300 ? C52 C53 . 1.389(8) ? C52 H52 . 0.9300 ? C53 C54 . 1.377(7) ? C53 H53 . 0.9300 ? C55 C60 . 1.532(7) ? C55 C56 . 1.543(7) ? C55 H55 . 0.9800 ? C56 C57 . 1.520(7) ? C56 H56A . 0.9700 ? C56 H56B . 0.9700 ? C57 C58 . 1.515(8) ? C57 H57A . 0.9700 ? C57 H57B . 0.9700 ? C58 C59 . 1.493(9) ? C58 H58A . 0.9700 ? C58 H58B . 0.9700 ? C59 C60 . 1.546(7) ? C59 H59A . 0.9700 ? C59 H59B . 0.9700 ? C60 H60A . 0.9700 ? C60 H60B . 0.9700 ? C61 C62 . 1.517(8) ? C61 C66 . 1.539(7) ? C61 H61 . 0.9800 ? C62 C63 . 1.537(7) ? C62 H62A . 0.9700 ? C62 H62B . 0.9700 ? C63 C64 . 1.510(9) ? C63 H63A . 0.9700 ? C63 H63B . 0.9700 ? C64 C65 . 1.513(10) ? C64 H64A . 0.9700 ? C64 H64B . 0.9700 ? C65 C66 . 1.515(8) ? C65 H65A . 0.9700 ? C65 H65B . 0.9700 ? C66 H66A . 0.9700 ? C66 H66B . 0.9700 ? C67 C72 . 1.530(7) ? C67 C68 . 1.531(7) ? C67 H67 . 0.9800 ? C68 C69 . 1.511(7) ? C68 H68A . 0.9700 ? C68 H68B . 0.9700 ? C69 C70 . 1.516(8) ? C69 H69A . 0.9700 ? C69 H69B . 0.9700 ? C70 C71 . 1.522(8) ? C70 H70A . 0.9700 ? C70 H70B . 0.9700 ? C71 C72 . 1.521(8) ? C71 H71A . 0.9700 ? C71 H71B . 0.9700 ? C72 H72A . 0.9700 ? C72 H72B . 0.9700 ? C73 C74 . 1.538(7) ? C73 C78 . 1.541(7) ? C73 H73 . 0.9800 ? C74 C75 . 1.514(7) ? C74 H74A . 0.9700 ? C74 H74B . 0.9700 ? C75 C76 . 1.520(8) ? C75 H75A . 0.9700 ? C75 H75B . 0.9700 ? C76 C77 . 1.509(8) ? C76 H76A . 0.9700 ? C76 H76B . 0.9700 ? C77 C78 . 1.526(8) ? C77 H77A . 0.9700 ? C77 H77B . 0.9700 ? C78 H78A . 0.9700 ? C78 H78B . 0.9700 ? C79 C80 . 1.397(8) ? C79 C84 . 1.397(8) ? C80 C81 . 1.392(8) ? C80 H80 . 0.9300 ? C81 C82 . 1.366(9) ? C81 H81 . 0.9300 ? C82 C83 . 1.391(9) ? C82 H82 . 0.9300 ? C83 C84 . 1.364(8) ? C83 H83 . 0.9300 ? C85 C86 . 1.528(8) ? C85 C90 . 1.530(8) ? C85 H85 . 0.9800 ? C86 C87 . 1.541(8) ? C86 H86A . 0.9700 ? C86 H86B . 0.9700 ? C87 C88 . 1.532(9) ? C87 H87A . 0.9700 ? C87 H87B . 0.9700 ? C88 C89 . 1.499(9) ? C88 H88A . 0.9700 ? C88 H88B . 0.9700 ? C89 C90 . 1.530(8) ? C89 H89A . 0.9700 ? C89 H89B . 0.9700 ? C90 H90A . 0.9700 ? C90 H90B . 0.9700 ? C91 H91A . 0.9600 ? C91 H91B . 0.9600 ? C91 H91C . 0.9600 ? C92 H92A . 0.9600 ? C92 H92B . 0.9600 ? C92 H92C . 0.9600 ? C93 H93A . 0.9600 ? C93 H93B . 0.9600 ? C93 H93C . 0.9600 ? C94 H94A . 0.9600 ? C94 H94B . 0.9600 ? C94 H94C . 0.9600 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O1 H1 Cl2 . 0.82 2.47 3.243(6) 156.5 yes O2 H2 O1 . 0.82 2.29 2.731(10) 114.4 yes O3 H3 Cl1 . 0.82 2.44 3.259(7) 172.3 yes O4 H4 O2 . 0.82 2.42 2.735(12) 103.6 yes C6 H6B Cl2 . 0.97 2.70 3.453(6) 134.7 yes C11 H11 Cl5 2_556 0.93 2.73 3.474(6) 138.1 yes C20 H20B Cl1 . 0.97 2.67 3.511(6) 145.7 yes C24 H24A Br1 . 0.97 2.89 3.378(6) 112.1 ? C26 H26B Cl2 . 0.97 2.69 3.532(6) 146.1 ? C30 H30A Br2 . 0.97 2.82 3.359(5) 115.6 ? C36 H36B Cl1 . 0.97 2.65 3.406(6) 135.2 ? C42 H42B Cl4 . 0.97 2.66 3.388(6) 132.5 ? C56 H56B Cl3 . 0.97 2.64 3.495(6) 146.5 ? C60 H60B Br3 . 0.97 2.89 3.429(6) 116.2 ? C62 H62A Cl4 . 0.97 2.68 3.547(6) 149.7 ? C66 H66A Br4 . 0.97 2.86 3.446(6) 119.9 ? C68 H68B Cl3 . 0.97 2.70 3.414(6) 131.3 ? C78 H78A Cl5 . 0.97 2.67 3.531(6) 147.5 ? C90 H90A Cl5 2_556 0.97 2.65 3.395(7) 133.7 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C13 P1 C1 C6 . . . . 55.5(4) ? C19 P1 C1 C6 . . . . 162.0(4) ? Ru1 P1 C1 C6 . . . . -59.6(4) ? C13 P1 C1 C2 . . . . -69.5(5) ? C19 P1 C1 C2 . . . . 37.0(5) ? Ru1 P1 C1 C2 . . . . 175.4(3) ? C6 C1 C2 C3 . . . . 56.2(7) ? P1 C1 C2 C3 . . . . -177.5(4) ? C1 C2 C3 C4 . . . . -56.5(7) ? C2 C3 C4 C5 . . . . 54.8(8) ? C3 C4 C5 C6 . . . . -54.9(7) ? C4 C5 C6 C1 . . . . 56.7(7) ? C2 C1 C6 C5 . . . . -56.1(6) ? P1 C1 C6 C5 . . . . 175.7(4) ? C25 P2 C7 C12 . . . . 156.2(4) ? C31 P2 C7 C12 . . . . -96.5(5) ? Ru1 P2 C7 C12 . . . . 29.1(5) ? C25 P2 C7 C8 . . . . -32.7(5) ? C31 P2 C7 C8 . . . . 74.6(5) ? Ru1 P2 C7 C8 . . . . -159.7(4) ? C12 C7 C8 C9 . . . . -1.0(8) ? P2 C7 C8 C9 . . . . -172.5(4) ? C7 C8 C9 C10 . . . . 0.9(9) ? C8 C9 C10 C11 . . . . -0.5(9) ? C9 C10 C11 C12 . . . . 0.3(9) ? C10 C11 C12 C7 . . . . -0.5(9) ? C10 C11 C12 Br1 . . . . 179.6(4) ? C8 C7 C12 C11 . . . . 0.8(8) ? P2 C7 C12 C11 . . . . 172.7(4) ? C8 C7 C12 Br1 . . . . -179.2(4) ? P2 C7 C12 Br1 . . . . -7.4(6) ? C19 P1 C13 C18 . . . . 156.0(4) ? C1 P1 C13 C18 . . . . -96.6(4) ? Ru1 P1 C13 C18 . . . . 29.2(4) ? C19 P1 C13 C14 . . . . -23.3(5) ? C1 P1 C13 C14 . . . . 84.1(5) ? Ru1 P1 C13 C14 . . . . -150.1(4) ? C18 C13 C14 C15 . . . . 0.4(8) ? P1 C13 C14 C15 . . . . 179.7(4) ? C13 C14 C15 C16 . . . . 1.0(9) ? C14 C15 C16 C17 . . . . -1.7(10) ? C15 C16 C17 C18 . . . . 0.8(9) ? C16 C17 C18 C13 . . . . 0.8(9) ? C16 C17 C18 Br2 . . . . -176.8(5) ? C14 C13 C18 C17 . . . . -1.3(8) ? P1 C13 C18 C17 . . . . 179.3(4) ? C14 C13 C18 Br2 . . . . 176.2(4) ? P1 C13 C18 Br2 . . . . -3.2(6) ? C13 P1 C19 C24 . . . . -69.3(4) ? C1 P1 C19 C24 . . . . -175.0(4) ? Ru1 P1 C19 C24 . . . . 46.9(5) ? C13 P1 C19 C20 . . . . 166.2(4) ? C1 P1 C19 C20 . . . . 60.6(5) ? Ru1 P1 C19 C20 . . . . -77.6(4) ? C24 C19 C20 C21 . . . . 57.9(7) ? P1 C19 C20 C21 . . . . -176.8(5) ? C19 C20 C21 C22 . . . . -55.6(8) ? C20 C21 C22 C23 . . . . 54.6(9) ? C21 C22 C23 C24 . . . . -54.5(9) ? C22 C23 C24 C19 . . . . 56.6(8) ? C20 C19 C24 C23 . . . . -59.4(7) ? P1 C19 C24 C23 . . . . 175.5(5) ? C7 P2 C25 C30 . . . . -73.3(4) ? C31 P2 C25 C30 . . . . -178.5(4) ? Ru1 P2 C25 C30 . . . . 45.0(4) ? C7 P2 C25 C26 . . . . 161.8(4) ? C31 P2 C25 C26 . . . . 56.6(4) ? Ru1 P2 C25 C26 . . . . -79.9(4) ? C30 C25 C26 C27 . . . . 56.1(6) ? P2 C25 C26 C27 . . . . -178.5(4) ? C25 C26 C27 C28 . . . . -57.0(8) ? C26 C27 C28 C29 . . . . 57.5(8) ? C27 C28 C29 C30 . . . . -56.2(8) ? C28 C29 C30 C25 . . . . 55.0(7) ? C26 C25 C30 C29 . . . . -55.0(6) ? P2 C25 C30 C29 . . . . -179.9(4) ? C7 P2 C31 C36 . . . . 56.6(4) ? C25 P2 C31 C36 . . . . 165.3(4) ? Ru1 P2 C31 C36 . . . . -58.6(4) ? C7 P2 C31 C32 . . . . -68.4(4) ? C25 P2 C31 C32 . . . . 40.3(5) ? Ru1 P2 C31 C32 . . . . 176.4(3) ? C36 C31 C32 C33 . . . . 57.5(6) ? P2 C31 C32 C33 . . . . -175.3(4) ? C31 C32 C33 C34 . . . . -57.0(8) ? C32 C33 C34 C35 . . . . 55.6(8) ? C33 C34 C35 C36 . . . . -56.7(8) ? C34 C35 C36 C31 . . . . 58.7(7) ? C32 C31 C36 C35 . . . . -58.2(6) ? P2 C31 C36 C35 . . . . 172.2(4) ? C49 P3 C37 C38 . . . . -68.7(4) ? C55 P3 C37 C38 . . . . 39.4(4) ? Ru2 P3 C37 C38 . . . . 177.0(3) ? C49 P3 C37 C42 . . . . 55.9(4) ? C55 P3 C37 C42 . . . . 163.9(4) ? Ru2 P3 C37 C42 . . . . -58.4(4) ? C42 C37 C38 C39 . . . . 58.4(6) ? P3 C37 C38 C39 . . . . -174.6(4) ? C37 C38 C39 C40 . . . . -56.4(6) ? C38 C39 C40 C41 . . . . 53.0(7) ? C39 C40 C41 C42 . . . . -54.2(7) ? C40 C41 C42 C37 . . . . 58.2(6) ? C38 C37 C42 C41 . . . . -59.0(6) ? P3 C37 C42 C41 . . . . 173.0(4) ? C61 P4 C43 C48 . . . . 158.7(4) ? C67 P4 C43 C48 . . . . -93.6(5) ? Ru2 P4 C43 C48 . . . . 30.1(5) ? C61 P4 C43 C44 . . . . -29.0(5) ? C67 P4 C43 C44 . . . . 78.7(5) ? Ru2 P4 C43 C44 . . . . -157.6(4) ? C48 C43 C44 C45 . . . . 1.6(9) ? P4 C43 C44 C45 . . . . -170.9(5) ? C43 C44 C45 C46 . . . . 1.4(10) ? C44 C45 C46 C47 . . . . -3.4(11) ? C45 C46 C47 C48 . . . . 2.2(10) ? C46 C47 C48 C43 . . . . 0.9(9) ? C46 C47 C48 Br3 . . . . 179.2(5) ? C44 C43 C48 C47 . . . . -2.7(8) ? P4 C43 C48 C47 . . . . 170.1(5) ? C44 C43 C48 Br3 . . . . 179.0(4) ? P4 C43 C48 Br3 . . . . -8.1(6) ? C55 P3 C49 C54 . . . . 161.3(4) ? C37 P3 C49 C54 . . . . -92.3(4) ? Ru2 P3 C49 C54 . . . . 32.4(5) ? C55 P3 C49 C50 . . . . -24.0(5) ? C37 P3 C49 C50 . . . . 82.4(5) ? Ru2 P3 C49 C50 . . . . -152.8(4) ? C54 C49 C50 C51 . . . . 1.9(8) ? P3 C49 C50 C51 . . . . -173.0(4) ? C49 C50 C51 C52 . . . . 0.8(9) ? C50 C51 C52 C53 . . . . -2.0(9) ? C51 C52 C53 C54 . . . . 0.4(9) ? C52 C53 C54 C49 . . . . 2.5(9) ? C52 C53 C54 Br4 . . . . -176.8(4) ? C50 C49 C54 C53 . . . . -3.6(8) ? P3 C49 C54 C53 . . . . 171.5(4) ? C50 C49 C54 Br4 . . . . 175.7(4) ? P3 C49 C54 Br4 . . . . -9.1(6) ? C49 P3 C55 C60 . . . . -72.8(4) ? C37 P3 C55 C60 . . . . -177.1(4) ? Ru2 P3 C55 C60 . . . . 46.0(4) ? C49 P3 C55 C56 . . . . 163.9(4) ? C37 P3 C55 C56 . . . . 59.6(4) ? Ru2 P3 C55 C56 . . . . -77.4(4) ? C60 C55 C56 C57 . . . . 56.3(6) ? P3 C55 C56 C57 . . . . -179.4(4) ? C55 C56 C57 C58 . . . . -57.1(7) ? C56 C57 C58 C59 . . . . 56.7(7) ? C57 C58 C59 C60 . . . . -55.9(7) ? C56 C55 C60 C59 . . . . -54.7(6) ? P3 C55 C60 C59 . . . . -178.4(4) ? C58 C59 C60 C55 . . . . 55.6(7) ? C43 P4 C61 C62 . . . . 164.2(4) ? C67 P4 C61 C62 . . . . 59.7(4) ? Ru2 P4 C61 C62 . . . . -76.2(4) ? C43 P4 C61 C66 . . . . -71.9(5) ? C67 P4 C61 C66 . . . . -176.4(4) ? Ru2 P4 C61 C66 . . . . 47.7(5) ? C66 C61 C62 C63 . . . . 55.0(6) ? P4 C61 C62 C63 . . . . -179.9(4) ? C61 C62 C63 C64 . . . . -56.7(7) ? C62 C63 C64 C65 . . . . 56.9(7) ? C63 C64 C65 C66 . . . . -57.0(7) ? C64 C65 C66 C61 . . . . 55.4(7) ? C62 C61 C66 C65 . . . . -54.3(7) ? P4 C61 C66 C65 . . . . -178.2(5) ? C43 P4 C67 C72 . . . . -72.2(5) ? C61 P4 C67 C72 . . . . 36.4(5) ? Ru2 P4 C67 C72 . . . . 173.3(3) ? C43 P4 C67 C68 . . . . 54.3(4) ? C61 P4 C67 C68 . . . . 162.8(4) ? Ru2 P4 C67 C68 . . . . -60.2(4) ? C72 C67 C68 C69 . . . . -58.7(6) ? P4 C67 C68 C69 . . . . 171.0(4) ? C67 C68 C69 C70 . . . . 57.2(7) ? C68 C69 C70 C71 . . . . -54.3(8) ? C69 C70 C71 C72 . . . . 54.1(8) ? C70 C71 C72 C67 . . . . -56.4(7) ? C68 C67 C72 C71 . . . . 57.9(6) ? P4 C67 C72 C71 . . . . -173.4(4) ? C79 P5 C73 C74 . . . . 70.4(4) ? C85 P5 C73 C74 . . . . 176.7(4) ? Ru3 P5 C73 C74 . . . . -46.8(4) ? C79 P5 C73 C78 . . . . -166.9(4) ? C85 P5 C73 C78 . . . . -60.6(5) ? Ru3 P5 C73 C78 . . . . 75.9(4) ? C78 C73 C74 C75 . . . . 53.7(7) ? P5 C73 C74 C75 . . . . 175.3(4) ? C73 C74 C75 C76 . . . . -57.9(7) ? C74 C75 C76 C77 . . . . 59.1(7) ? C75 C76 C77 C78 . . . . -56.8(7) ? C76 C77 C78 C73 . . . . 53.5(7) ? C74 C73 C78 C77 . . . . -51.2(7) ? P5 C73 C78 C77 . . . . -173.8(4) ? C73 P5 C79 C80 . . . . 22.0(6) ? C85 P5 C79 C80 . . . . -85.6(5) ? Ru3 P5 C79 C80 . . . . 148.0(5) ? C73 P5 C79 C84 . . . . -155.7(5) ? C85 P5 C79 C84 . . . . 96.7(5) ? Ru3 P5 C79 C84 . . . . -29.7(5) ? C84 C79 C80 C81 . . . . 2.4(9) ? P5 C79 C80 C81 . . . . -175.4(5) ? C79 C80 C81 C82 . . . . -1.5(10) ? C80 C81 C82 C83 . . . . -0.1(10) ? C81 C82 C83 C84 . . . . 0.6(10) ? C82 C83 C84 C79 . . . . 0.4(10) ? C82 C83 C84 Br5 . . . . 177.7(5) ? C80 C79 C84 C83 . . . . -1.9(9) ? P5 C79 C84 C83 . . . . 176.1(5) ? C80 C79 C84 Br5 . . . . -179.2(4) ? P5 C79 C84 Br5 . . . . -1.3(6) ? C73 P5 C85 C86 . . . . -42.5(5) ? C79 P5 C85 C86 . . . . 66.1(5) ? Ru3 P5 C85 C86 . . . . -178.1(4) ? C73 P5 C85 C90 . . . . -169.1(4) ? C79 P5 C85 C90 . . . . -60.4(5) ? Ru3 P5 C85 C90 . . . . 55.4(5) ? C90 C85 C86 C87 . . . . -56.4(7) ? P5 C85 C86 C87 . . . . 175.7(5) ? C85 C86 C87 C88 . . . . 57.5(8) ? C86 C87 C88 C89 . . . . -56.7(9) ? C87 C88 C89 C90 . . . . 56.0(8) ? C88 C89 C90 C85 . . . . -56.7(8) ? C86 C85 C90 C89 . . . . 56.0(7) ? P5 C85 C90 C89 . . . . -175.2(4) ?