#------------------------------------------------------------------------------ #$Date: 2026-10-23 23:24:02 +0200 (Fri, 23 Oct 2026) $ #$Revision: 306995 $ #$URL: svn://www.crystallography.net/cod/cif/1/57/74/1577492.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1577492 loop_ _publ_author_name 'Westcott, Barry' 'Oliver, Allen G.' _publ_section_title ; trans-Diaquabis(pyridin-2-yl thiophen-2-yl ketone-\k2 N,O)zinc(II) bis(tetrafluoridoborate) ; _journal_coeditor_code WM4262 _journal_issue 10 _journal_name_full IUCrData _journal_paper_doi 10.1107/S2414314626010369 _journal_volume 11 _journal_year 2026 _chemical_formula_iupac '[Zn (C10 H7 B F4 N O S)2 (H2 O)2] (B F4)2' _chemical_formula_moiety 'C20 H18 B2 F8 N2 O4 S2 Zn 2+, 2(B F4 -)' _chemical_formula_sum 'C20 H18 B2 F8 N2 O4 S2 Zn' _chemical_formula_weight 653.47 _chemical_name_systematic ; trans-Diaquabis(pyridin-2-yl thiophen-2-yl ketone-\k^2^N,O)zinc(II) bis(tetrafluoridoborate) ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2019/3 _cell_angle_alpha 90 _cell_angle_beta 103.519(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 7.1601(3) _cell_length_b 11.9574(4) _cell_length_c 15.2293(5) _cell_measurement_reflns_used 9706 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 74.55 _cell_measurement_theta_min 4.75 _cell_volume 1267.75(8) _computing_cell_refinement ; SAINT (Bruker, 2023) ; _computing_data_collection ; APEX5 (Bruker, 2023) ; _computing_data_reduction ; SAINT (Bruker, 2023) ; _computing_molecular_graphics ; Mercury (Macrae et al., 2020) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) and ShelXle (H\"ubschle et al., 2011) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 120(2) _diffrn_detector 'CMOS Area Detector' _diffrn_detector_area_resol_mean 7.41 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Bruker Venture' _diffrn_measurement_method 'combination of \w and \f-scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_radiation_monochromator 'HELIOS Multi-layer' _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0400 _diffrn_reflns_av_unetI/netI 0.0121 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 50901 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 74.627 _diffrn_reflns_theta_min 4.753 _diffrn_source micro-focus _exptl_absorpt_coefficient_mu 3.734 _exptl_absorpt_correction_T_max 0.7917 _exptl_absorpt_correction_T_min 0.6322 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.712 _exptl_crystal_description block _exptl_crystal_F_000 656 _exptl_crystal_size_max 0.157 _exptl_crystal_size_mid 0.152 _exptl_crystal_size_min 0.057 _refine_diff_density_max 0.900 _refine_diff_density_min -0.436 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.052 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 182 _refine_ls_number_reflns 2591 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.052 _refine_ls_R_factor_all 0.0352 _refine_ls_R_factor_gt 0.0330 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0365P)^2^+1.6051P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0831 _refine_ls_wR_factor_ref 0.0846 _reflns_number_gt 2426 _reflns_number_total 2591 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file wm4262.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1577492 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.592 _shelx_estimated_absorpt_t_max 0.815 _shelx_hkl_file ; -2 0 0 2558.74 80.99 -2 0 0 2510.15 80.69 2 0 0 2521.45 80.69 2 0 0 2479.95 80.79 2 0 0 2481.45 80.69 2 0 0 2634.74 80.59 -3 0 0 0.00 1.20 -3 0 0 -0.30 1.70 -3 0 0 0.40 1.00 -3 0 0 0.00 0.80 3 0 0 0.10 0.60 3 0 0 0.30 1.20 3 0 0 -0.20 0.90 3 0 0 -0.70 0.60 3 0 0 0.50 0.70 4 0 0 97.79 4.80 4 0 0 104.19 4.50 4 0 0 103.69 4.40 4 0 0 103.69 4.70 4 0 0 103.29 4.00 4 0 0 102.69 4.60 -5 0 0 0.90 2.50 -5 0 0 2.10 1.20 -5 0 0 -1.70 1.40 -5 0 0 -0.90 1.20 -5 0 0 3.90 1.50 5 0 0 -3.20 2.10 5 0 0 -0.60 1.40 5 0 0 1.00 1.40 5 0 0 1.60 1.20 5 0 0 -3.60 2.60 5 0 0 1.00 2.10 5 0 0 -0.50 1.60 -6 0 0 261.57 10.00 -6 0 0 266.57 9.70 -6 0 0 265.87 10.00 -6 0 0 251.77 9.60 -6 0 0 262.47 11.80 -6 0 0 257.87 10.70 -6 0 0 248.48 9.80 -6 0 0 276.87 17.30 6 0 0 261.37 10.80 6 0 0 249.48 10.70 6 0 0 252.57 9.60 6 0 0 263.37 10.30 6 0 0 248.68 9.60 6 0 0 244.28 10.50 -7 0 0 -0.90 1.20 -7 0 0 0.20 2.00 -7 0 0 -3.60 1.60 -7 0 0 0.70 1.60 -7 0 0 1.50 1.10 -7 0 0 -0.40 1.10 -7 0 0 -0.20 1.40 -7 0 0 2.40 1.90 7 0 0 -0.30 1.00 7 0 0 -1.20 2.40 7 0 0 4.20 3.30 7 0 0 0.60 1.00 7 0 0 -0.80 1.10 -8 0 0 1.80 1.00 -8 0 0 5.10 1.50 -8 0 0 0.90 0.90 -8 0 0 2.80 1.50 8 0 0 3.90 1.00 8 0 0 3.90 1.00 8 0 0 1.80 1.00 8 -1 0 2.30 1.00 8 -1 0 1.30 0.90 8 -1 0 2.30 0.80 -8 1 0 0.00 0.90 -8 1 0 1.00 1.30 -8 1 0 3.40 0.90 7 -1 0 59.59 3.30 7 -1 0 56.29 3.00 7 -1 0 59.09 3.20 7 -1 0 52.89 4.60 7 -1 0 56.09 5.80 -7 1 0 53.89 4.00 -7 1 0 55.39 3.40 -7 1 0 54.69 3.40 -7 1 0 51.89 3.30 -7 1 0 52.39 4.20 -7 1 0 59.09 3.20 -7 1 0 62.59 3.90 -7 1 0 53.29 4.40 6 -1 0 3.60 3.70 6 -1 0 9.90 1.50 6 -1 0 10.50 2.30 6 -1 0 7.50 1.40 6 -1 0 10.80 4.60 -6 1 0 6.30 1.60 -6 1 0 5.40 2.00 -6 1 0 8.50 1.80 -6 1 0 14.20 1.90 -6 1 0 11.10 1.90 -6 1 0 7.80 2.50 -6 1 0 10.30 1.70 -6 1 0 9.50 2.00 5 -1 0 15.80 2.50 5 -1 0 18.30 1.90 5 -1 0 15.80 2.30 5 -1 0 16.30 2.50 5 -1 0 17.20 1.80 5 -1 0 13.80 2.80 5 -1 0 16.80 1.50 5 -1 0 16.90 2.30 -5 1 0 17.10 2.80 -5 1 0 15.70 1.90 -5 1 0 16.70 2.30 -5 1 0 16.50 3.40 -5 1 0 16.70 3.20 -5 1 0 18.20 1.60 -5 1 0 19.70 2.90 -5 1 0 19.70 2.30 4 -1 0 308.27 11.20 4 -1 0 297.77 11.10 4 -1 0 304.77 11.00 4 -1 0 269.17 10.80 4 -1 0 316.17 10.90 -4 1 0 269.37 11.50 -4 1 0 311.67 12.20 -4 1 0 313.37 12.00 -4 1 0 313.27 11.60 3 -1 0 2.80 1.00 3 -1 0 2.80 0.80 3 -1 0 1.60 0.80 3 -1 0 2.30 0.80 -3 1 0 2.40 1.30 -3 1 0 1.10 1.40 -3 1 0 2.00 1.00 -3 1 0 3.10 1.60 -3 1 0 2.60 1.20 2 -1 0 38.90 1.90 2 -1 0 37.00 1.80 2 -1 0 35.60 2.10 2 -1 0 39.00 1.90 -2 1 0 36.30 2.10 -2 1 0 39.20 2.20 -2 1 0 37.90 2.00 -2 1 0 37.70 2.30 1 -1 0 1138.29 37.80 1 -1 0 1166.68 37.60 1 -1 0 1215.98 37.60 1 -1 0 1172.88 37.60 -1 1 0 1185.38 37.50 -1 1 0 1208.18 37.80 -1 1 0 1140.99 37.60 -1 1 0 1162.98 37.50 0 -1 0 0.10 0.10 0 -1 0 0.20 0.10 0 -1 0 0.30 0.20 0 -1 0 0.20 0.20 0 -1 0 0.00 0.20 0 1 0 0.00 0.20 0 1 0 0.30 0.20 0 1 0 0.00 0.20 0 1 0 0.10 0.10 -1 -1 0 1167.58 36.40 -1 -1 0 1105.29 36.70 -1 -1 0 1093.99 36.60 -1 -1 0 1215.68 36.40 -1 -1 0 1178.88 36.70 1 1 0 1102.59 36.30 1 1 0 1147.59 36.40 1 1 0 1142.49 36.40 -2 -1 0 35.20 2.00 -2 -1 0 41.70 2.20 -2 -1 0 35.60 1.90 -2 -1 0 37.30 2.10 2 1 0 38.90 1.70 2 1 0 37.60 1.60 -3 -1 0 2.10 1.00 -3 -1 0 1.20 1.10 -3 -1 0 2.40 1.50 3 1 0 1.90 1.00 3 1 0 2.10 0.60 3 1 0 2.30 0.70 3 1 0 2.30 0.80 -4 -1 0 317.07 12.30 4 1 0 280.17 10.30 4 1 0 276.57 9.90 4 1 0 277.27 10.50 4 1 0 307.27 10.50 4 1 0 301.47 10.40 -5 -1 0 19.00 2.50 -5 -1 0 18.80 2.50 -5 -1 0 20.40 3.10 -5 -1 0 17.70 2.20 -5 -1 0 18.20 2.10 -5 -1 0 17.50 3.50 -5 -1 0 19.10 2.30 -5 -1 0 16.90 2.40 5 1 0 12.60 3.10 5 1 0 17.30 2.10 5 1 0 12.30 3.50 5 1 0 17.40 2.20 -6 -1 0 13.90 2.20 -6 -1 0 9.30 1.60 -6 -1 0 8.50 2.00 -6 -1 0 9.20 1.50 -6 -1 0 10.40 1.50 -6 -1 0 9.90 1.70 -6 -1 0 10.40 1.70 -6 -1 0 8.80 2.00 -6 -1 0 8.30 1.90 6 1 0 12.50 2.30 6 1 0 8.30 3.50 6 1 0 7.70 2.60 6 1 0 10.20 1.70 6 1 0 10.80 1.60 -7 -1 0 57.99 3.20 -7 -1 0 51.09 3.80 -7 -1 0 54.29 4.00 -7 -1 0 55.29 3.70 -7 -1 0 50.79 4.00 -7 -1 0 59.39 3.50 -7 -1 0 56.99 3.20 -7 -1 0 54.79 3.40 7 1 0 52.29 5.70 7 1 0 52.09 3.10 7 1 0 54.59 3.20 7 1 0 54.39 3.10 7 1 0 53.79 4.50 -8 -1 0 -0.20 2.00 -8 -1 0 0.70 1.70 -8 -1 0 0.10 1.00 -8 -1 0 0.50 1.00 8 1 0 0.20 1.10 8 1 0 2.10 0.90 8 1 0 0.10 0.90 8 -2 0 91.19 3.70 8 -2 0 95.69 3.80 8 -2 0 93.89 3.70 -8 2 0 88.19 3.80 -8 2 0 80.49 4.30 -8 2 0 95.79 4.00 7 -2 0 0.10 1.00 7 -2 0 0.90 0.90 7 -2 0 -0.90 1.10 7 -2 0 1.50 2.60 -7 2 0 0.00 1.00 -7 2 0 2.20 1.60 -7 2 0 0.10 1.00 -7 2 0 -0.70 1.40 -7 2 0 -1.60 1.40 6 -2 0 4.20 1.20 6 -2 0 4.40 1.00 6 -2 0 -0.10 3.10 6 -2 0 2.30 2.20 6 -2 0 4.00 1.20 6 -2 0 3.10 2.90 -6 2 0 3.50 1.50 -6 2 0 2.10 1.50 -6 2 0 3.50 1.30 -6 2 0 5.30 2.20 -6 2 0 -4.60 4.80 -6 2 0 3.70 1.50 -6 2 0 1.50 2.00 -6 2 0 4.00 1.40 -6 2 0 5.80 1.70 5 -2 0 58.89 4.80 5 -2 0 54.89 3.80 5 -2 0 55.29 4.20 5 -2 0 55.59 4.20 5 -2 0 58.09 3.80 5 -2 0 52.29 3.50 5 -2 0 52.09 2.70 -5 2 0 55.09 5.10 -5 2 0 51.89 3.10 -5 2 0 53.49 2.50 -5 2 0 49.90 3.20 -5 2 0 57.79 3.40 -5 2 0 56.29 3.70 4 -2 0 477.05 16.60 4 -2 0 476.95 16.90 4 -2 0 458.65 17.40 4 -2 0 470.15 17.00 4 -2 0 496.15 16.70 4 -2 0 484.45 16.00 -4 2 0 463.85 17.60 -4 2 0 505.15 17.80 3 -2 0 90.59 4.30 3 -2 0 92.39 4.00 3 -2 0 96.19 4.20 3 -2 0 94.69 4.20 3 -2 0 89.99 4.10 -3 2 0 93.99 4.30 -3 2 0 89.09 5.00 -3 2 0 91.89 4.60 -3 2 0 97.49 4.80 2 -2 0 311.37 10.70 2 -2 0 315.97 10.80 2 -2 0 318.87 10.80 2 -2 0 308.87 10.90 -2 2 0 295.07 10.70 -2 2 0 321.07 11.20 -2 2 0 300.17 11.00 -2 2 0 321.87 11.30 1 -2 0 818.02 26.30 1 -2 0 831.62 26.30 1 -2 0 810.02 26.30 1 -2 0 806.92 26.40 -1 2 0 796.42 26.20 -1 2 0 837.62 26.60 -1 2 0 822.62 26.20 -1 2 0 772.92 26.40 0 -2 0 967.80 31.80 0 -2 0 954.40 31.80 0 -2 0 1011.20 31.50 0 -2 0 1017.30 31.70 0 -2 0 1007.90 31.50 0 2 0 978.50 31.50 0 2 0 989.00 31.70 0 2 0 983.90 31.60 0 2 0 957.00 31.50 -1 -2 0 802.72 25.90 -1 -2 0 789.62 25.30 1 2 0 783.12 25.50 1 2 0 806.12 25.70 -2 -2 0 291.67 10.20 -2 -2 0 307.77 10.40 -2 -2 0 275.67 10.10 -2 -2 0 277.97 10.20 -2 -2 0 299.77 9.60 2 2 0 302.07 9.70 -3 -2 0 78.79 4.60 -3 -2 0 92.79 4.40 3 2 0 79.89 3.50 3 2 0 80.99 3.30 3 2 0 88.59 3.60 3 2 0 82.89 3.30 3 2 0 91.99 3.50 -4 -2 0 497.55 17.50 4 2 0 463.15 15.60 4 2 0 426.36 15.60 4 2 0 506.35 16.20 4 2 0 465.95 16.20 -5 -2 0 51.49 3.40 -5 -2 0 53.09 3.10 -5 -2 0 50.89 3.30 -5 -2 0 58.59 5.10 -5 -2 0 50.39 3.30 -5 -2 0 50.29 3.80 -5 -2 0 50.19 3.90 -5 -2 0 51.39 3.50 -5 -2 0 48.00 3.30 -5 -2 0 46.90 3.90 5 2 0 55.59 3.50 5 2 0 49.50 2.50 5 2 0 55.99 3.80 5 2 0 51.39 4.20 5 2 0 45.70 5.00 5 2 0 52.79 4.40 -6 -2 0 3.50 4.80 -6 -2 0 2.80 1.70 -6 -2 0 4.20 1.30 -6 -2 0 3.90 1.70 -6 -2 0 2.80 1.90 -6 -2 0 6.10 1.40 -6 -2 0 4.50 1.50 -6 -2 0 4.70 1.40 -6 -2 0 2.60 1.10 6 2 0 8.90 4.10 6 2 0 3.30 1.40 6 2 0 5.20 2.00 6 2 0 5.50 2.50 6 2 0 5.00 1.40 6 2 0 1.40 3.30 6 2 0 3.30 1.00 -7 -2 0 4.60 1.90 -7 -2 0 -0.20 2.20 -7 -2 0 -0.30 1.40 -7 -2 0 0.10 1.30 -7 -2 0 -5.90 2.60 -7 -2 0 1.00 1.10 -7 -2 0 1.00 1.10 -7 -2 0 -1.20 1.10 7 2 0 4.90 5.10 7 2 0 0.30 1.00 7 2 0 -0.40 2.50 7 2 0 0.20 1.10 7 2 0 0.70 3.00 7 2 0 0.70 1.30 -8 -2 0 90.99 3.90 -8 -2 0 98.89 4.20 -8 -2 0 93.19 4.00 8 2 0 92.29 3.70 8 -3 0 0.80 0.80 8 -3 0 1.40 1.10 8 -3 0 0.70 0.80 -8 3 0 0.50 0.80 -8 3 0 2.10 1.10 -8 3 0 1.40 0.90 7 -3 0 1.50 0.90 7 -3 0 0.50 4.10 7 -3 0 4.50 2.70 7 -3 0 -0.30 1.00 7 -3 0 1.00 0.90 -7 3 0 -0.10 1.30 -7 3 0 2.50 1.10 -7 3 0 0.90 1.40 -7 3 0 1.40 1.00 -7 3 0 -0.30 1.30 6 -3 0 28.50 3.90 6 -3 0 38.50 2.40 6 -3 0 38.60 5.10 6 -3 0 38.00 2.60 6 -3 0 44.80 5.20 6 -3 0 34.00 2.60 -6 3 0 40.90 5.90 -6 3 0 41.20 2.80 -6 3 0 39.90 3.00 -6 3 0 35.70 2.60 -6 3 0 41.20 6.60 -6 3 0 37.30 3.40 5 -3 0 886.31 31.70 5 -3 0 989.90 31.60 5 -3 0 900.31 30.50 5 -3 0 936.11 31.30 5 -3 0 925.91 30.30 5 -3 0 909.11 30.50 5 -3 0 951.60 31.80 -5 3 0 919.01 32.20 -5 3 0 889.01 31.20 -5 3 0 945.21 30.00 -5 3 0 921.81 32.60 -5 3 0 948.81 32.80 -5 3 0 956.10 30.90 -5 3 0 954.70 33.10 -5 3 0 878.81 30.40 -5 3 0 847.52 30.50 4 -3 0 136.49 5.90 4 -3 0 142.89 6.00 4 -3 0 125.09 6.20 4 -3 0 129.89 6.20 4 -3 0 133.99 5.10 4 -3 0 131.59 6.00 -4 3 0 127.29 6.70 -4 3 0 134.79 6.50 -4 3 0 127.29 6.80 -4 3 0 125.99 7.10 -4 3 0 129.19 6.50 -4 3 0 131.39 4.80 3 -3 0 133.49 5.60 3 -3 0 134.39 5.50 3 -3 0 128.69 5.40 3 -3 0 128.09 5.60 3 -3 0 140.89 5.60 -3 3 0 127.59 6.30 -3 3 0 126.29 5.80 -3 3 0 125.59 6.10 -3 3 0 131.99 5.70 -3 3 0 116.99 5.70 2 -3 0 230.58 8.30 2 -3 0 226.48 8.40 2 -3 0 239.98 8.30 2 -3 0 232.18 8.30 -2 3 0 230.78 8.80 -2 3 0 210.78 8.20 -2 3 0 228.38 8.50 -2 3 0 212.18 8.10 -2 3 0 241.88 10.20 1 -3 0 360.86 11.80 1 -3 0 350.96 11.70 1 -3 0 354.46 11.70 1 -3 0 339.47 11.80 -1 3 0 333.17 11.60 -1 3 0 343.47 11.60 -1 3 0 342.17 12.10 -1 3 0 338.47 11.90 0 -3 0 0.30 0.30 0 -3 0 0.60 0.40 0 -3 0 0.40 0.50 0 3 0 0.60 0.40 0 3 0 0.50 0.50 0 3 0 0.50 0.50 0 3 0 0.30 0.40 -1 -3 0 329.17 10.80 -1 -3 0 338.37 11.30 -1 -3 0 336.97 11.60 -1 -3 0 332.87 11.50 1 3 0 326.97 11.00 1 3 0 335.87 11.30 1 3 0 328.77 11.00 1 3 0 336.77 11.50 -2 -3 0 215.58 8.10 -2 -3 0 213.08 7.30 -2 -3 0 216.88 7.90 2 3 0 215.58 7.70 2 3 0 223.98 7.50 2 3 0 239.58 8.30 -3 -3 0 133.39 5.90 3 3 0 128.79 4.90 3 3 0 134.79 5.50 3 3 0 124.99 5.00 3 3 0 131.09 5.20 -4 -3 0 128.19 6.60 4 3 0 136.09 5.50 4 3 0 129.39 5.70 4 3 0 128.99 5.30 4 3 0 130.69 6.10 -5 -3 0 936.01 30.20 -5 -3 0 908.01 30.10 -5 -3 0 839.32 29.90 -5 -3 0 913.51 30.90 -5 -3 0 949.90 32.50 -5 -3 0 893.71 30.70 -5 -3 0 910.91 30.40 -5 -3 0 910.61 30.20 -5 -3 0 924.11 30.50 -5 -3 0 921.91 30.60 5 3 0 926.41 31.50 5 3 0 848.82 29.90 5 3 0 939.71 30.40 5 3 0 909.71 30.80 5 3 0 923.81 29.70 5 3 0 907.71 30.30 5 3 0 889.31 29.80 -6 -3 0 50.09 7.10 -6 -3 0 35.40 3.00 -6 -3 0 34.20 3.90 -6 -3 0 42.80 3.30 -6 -3 0 39.60 3.60 -6 -3 0 30.80 3.30 -6 -3 0 36.90 2.60 -6 -3 0 37.50 2.90 -6 -3 0 40.00 3.10 -6 -3 0 33.30 2.80 -6 -3 0 35.90 2.70 6 3 0 29.00 3.60 6 3 0 24.90 4.10 6 3 0 37.90 5.20 6 3 0 41.60 4.70 6 3 0 33.10 2.80 6 3 0 37.50 2.30 6 3 0 36.70 2.80 -7 -3 0 2.00 1.20 -7 -3 0 0.80 1.00 -7 -3 0 3.20 1.90 -7 -3 0 1.30 1.30 -7 -3 0 1.30 1.30 -7 -3 0 2.10 2.60 7 3 0 3.60 1.40 7 3 0 2.40 1.00 7 3 0 1.90 1.20 7 3 0 1.20 3.10 7 3 0 8.80 5.40 7 3 0 1.30 3.40 -8 -3 0 3.20 1.10 -8 -3 0 1.90 1.60 -8 -3 0 0.00 1.00 -8 -3 0 0.00 1.50 8 3 0 1.90 0.90 8 3 0 0.90 0.90 8 -4 0 2.00 0.90 8 -4 0 1.20 0.80 -8 4 0 1.60 1.10 -8 4 0 0.90 1.10 -8 4 0 1.40 1.00 7 -4 0 26.00 3.70 7 -4 0 26.60 2.20 7 -4 0 27.40 2.10 7 -4 0 28.50 2.00 -7 4 0 28.90 2.60 -7 4 0 24.80 2.90 -7 4 0 33.80 3.20 -7 4 0 26.80 2.10 -7 4 0 32.40 2.50 6 -4 0 17.00 1.80 6 -4 0 18.60 3.20 6 -4 0 8.30 5.30 6 -4 0 15.90 1.90 6 -4 0 13.10 1.60 -6 4 0 16.70 2.00 -6 4 0 12.90 1.60 -6 4 0 15.40 2.00 -6 4 0 18.70 2.60 5 -4 0 8.70 2.70 5 -4 0 6.30 1.30 5 -4 0 5.30 2.40 5 -4 0 7.50 2.10 5 -4 0 7.30 1.20 5 -4 0 6.70 1.40 5 -4 0 5.50 2.50 -5 4 0 6.00 2.90 -5 4 0 6.20 3.80 -5 4 0 6.80 1.30 -5 4 0 5.00 1.40 -5 4 0 5.50 0.80 -5 4 0 11.10 3.40 -5 4 0 5.40 1.40 4 -4 0 148.49 6.70 4 -4 0 135.09 6.40 4 -4 0 147.09 6.60 4 -4 0 146.09 6.90 4 -4 0 137.89 6.70 4 -4 0 143.19 5.50 -4 4 0 140.69 5.20 -4 4 0 145.89 6.40 -4 4 0 138.79 7.50 -4 4 0 137.79 7.60 -4 4 0 147.49 7.30 -4 4 0 144.69 8.00 3 -4 0 54.69 3.30 3 -4 0 59.59 3.40 3 -4 0 56.09 2.60 3 -4 0 59.29 3.40 3 -4 0 59.59 3.50 3 -4 0 60.29 3.40 -3 4 0 51.09 4.20 -3 4 0 61.79 4.50 -3 4 0 58.89 4.00 -3 4 0 59.19 3.70 -3 4 0 54.09 4.20 2 -4 0 209.38 7.80 2 -4 0 198.08 7.70 2 -4 0 213.58 7.80 2 -4 0 207.88 7.90 2 -4 0 206.98 7.70 -2 4 0 198.48 8.10 -2 4 0 197.68 7.70 -2 4 0 204.08 7.80 -2 4 0 210.28 8.40 -2 4 0 205.28 7.60 -2 4 0 209.08 8.60 1 -4 0 197.58 7.10 1 -4 0 191.98 7.30 1 -4 0 200.98 7.30 1 -4 0 198.18 7.20 -1 4 0 197.68 7.20 -1 4 0 202.48 7.30 -1 4 0 198.48 7.50 -1 4 0 201.08 7.70 0 -4 0 31.10 1.60 0 -4 0 31.10 1.50 0 -4 0 30.10 1.90 0 -4 0 28.30 1.80 0 4 0 36.10 1.90 0 4 0 30.20 1.60 0 4 0 32.50 2.10 0 4 0 32.20 1.70 -1 -4 0 201.78 7.50 -1 -4 0 195.98 6.60 -1 -4 0 205.68 7.60 -1 -4 0 195.28 7.20 1 4 0 198.68 7.20 1 4 0 194.88 6.90 1 4 0 199.78 7.50 1 4 0 193.98 7.00 -2 -4 0 182.38 7.20 -2 -4 0 187.18 6.50 -2 -4 0 199.88 7.70 -2 -4 0 194.38 7.50 2 4 0 204.68 6.90 2 4 0 189.28 7.40 2 4 0 203.28 7.30 2 4 0 185.98 6.90 2 4 0 200.28 7.00 -3 -4 0 60.49 3.80 3 4 0 48.70 2.90 3 4 0 55.59 2.70 3 4 0 57.89 3.30 3 4 0 51.69 2.80 -4 -4 0 145.19 7.40 4 4 0 141.49 6.60 4 4 0 136.49 5.70 4 4 0 133.59 5.20 4 4 0 139.29 5.70 4 4 0 144.99 6.10 -5 -4 0 5.90 1.70 -5 -4 0 6.70 1.30 -5 -4 0 7.80 1.60 -5 -4 0 7.50 4.00 -5 -4 0 5.90 1.30 -5 -4 0 7.10 1.60 -5 -4 0 7.30 2.10 -5 -4 0 4.90 1.70 -5 -4 0 6.70 1.50 -5 -4 0 6.30 1.40 -5 -4 0 4.90 1.70 -5 -4 0 5.60 1.70 5 4 0 6.90 2.30 5 4 0 6.80 1.90 5 4 0 12.50 3.20 5 4 0 7.40 1.90 5 4 0 6.30 1.10 5 4 0 6.80 2.20 -6 -4 0 16.70 2.10 -6 -4 0 14.80 2.20 -6 -4 0 14.60 2.10 -6 -4 0 15.20 2.00 -6 -4 0 15.80 2.00 -6 -4 0 14.10 1.70 -6 -4 0 11.90 1.60 -6 -4 0 17.30 1.90 6 4 0 15.50 1.80 6 4 0 13.10 3.30 6 4 0 17.20 2.70 6 4 0 18.30 1.70 6 4 0 16.80 1.90 -7 -4 0 32.90 2.70 -7 -4 0 25.80 2.70 -7 -4 0 28.00 2.60 -7 -4 0 31.30 2.40 -7 -4 0 30.00 3.20 -7 -4 0 27.60 2.40 7 4 0 33.50 4.40 7 4 0 31.40 2.10 7 4 0 37.00 4.10 7 4 0 30.20 2.30 7 4 0 31.20 2.70 -8 -4 0 5.00 1.60 -8 -4 0 3.50 2.10 -8 -4 0 0.70 1.10 -8 -4 0 0.60 1.30 8 4 0 3.40 1.00 8 4 0 1.60 0.90 8 -5 0 1.60 1.10 8 -5 0 3.00 0.70 -8 5 0 1.10 0.90 -8 5 0 1.30 0.70 -8 5 0 2.60 1.10 7 -5 0 6.20 1.10 7 -5 0 6.90 6.10 7 -5 0 8.00 1.30 7 -5 0 8.00 1.20 -7 5 0 6.70 1.70 -7 5 0 6.00 1.10 -7 5 0 4.90 1.30 -7 5 0 7.30 1.50 -7 5 0 4.40 1.20 6 -5 0 164.28 8.90 6 -5 0 172.98 6.70 6 -5 0 172.78 8.50 6 -5 0 171.98 6.80 6 -5 0 177.88 7.00 -6 5 0 167.98 6.80 -6 5 0 172.78 6.90 -6 5 0 176.48 7.40 -6 5 0 178.88 8.00 5 -5 0 3.70 2.30 5 -5 0 2.00 2.30 5 -5 0 2.80 1.10 5 -5 0 1.30 1.00 5 -5 0 3.20 2.60 5 -5 0 -0.40 2.70 5 -5 0 2.50 0.90 -5 5 0 3.10 1.30 -5 5 0 4.10 3.30 -5 5 0 -1.50 3.10 -5 5 0 1.50 0.70 -5 5 0 1.70 1.30 -5 5 0 4.00 1.20 -5 5 0 0.80 4.30 4 -5 0 108.49 6.10 4 -5 0 113.49 6.00 4 -5 0 107.99 4.90 4 -5 0 119.59 5.80 4 -5 0 118.79 5.90 4 -5 0 108.09 4.90 4 -5 0 113.09 5.60 -4 5 0 107.99 5.10 -4 5 0 110.99 6.50 -4 5 0 109.79 5.50 -4 5 0 113.39 4.30 -4 5 0 109.19 7.20 -4 5 0 119.59 7.80 -4 5 0 108.99 6.90 3 -5 0 907.21 29.60 3 -5 0 945.01 30.70 3 -5 0 908.11 30.70 3 -5 0 925.01 30.90 -3 5 0 901.81 29.30 -3 5 0 909.31 31.50 -3 5 0 893.41 31.70 -3 5 0 847.72 30.60 -3 5 0 933.91 30.90 2 -5 0 59.39 3.20 2 -5 0 52.59 3.10 2 -5 0 55.79 3.30 2 -5 0 50.29 3.10 2 -5 0 52.79 3.50 -2 5 0 52.29 3.30 -2 5 0 49.00 4.60 -2 5 0 50.79 3.20 -2 5 0 61.29 4.00 -2 5 0 55.09 3.10 -2 5 0 61.19 4.20 -2 5 0 49.99 3.60 1 -5 0 145.79 5.70 1 -5 0 141.09 5.80 1 -5 0 133.09 5.60 -1 5 0 145.89 5.80 -1 5 0 148.09 5.80 -1 5 0 146.59 6.20 -1 5 0 142.89 6.30 -1 5 0 146.49 6.60 -1 5 0 161.98 6.60 0 -5 0 0.10 0.60 0 -5 0 0.00 0.60 0 -5 0 -0.10 0.90 0 -5 0 0.70 0.90 0 5 0 1.10 0.90 0 5 0 0.00 1.40 0 5 0 0.20 0.70 0 5 0 2.00 1.20 0 5 0 0.20 0.90 0 5 0 0.10 0.90 -1 -5 0 135.99 5.70 -1 -5 0 144.89 6.20 -1 -5 0 143.09 5.00 1 5 0 140.69 5.30 1 5 0 140.89 5.50 1 5 0 143.39 5.70 1 5 0 144.79 5.40 1 5 0 140.59 6.10 -2 -5 0 53.89 3.50 -2 -5 0 48.10 3.40 2 5 0 54.59 2.70 2 5 0 42.10 3.30 2 5 0 51.79 3.00 2 5 0 51.19 2.70 2 5 0 52.59 3.50 2 5 0 52.09 2.70 -3 -5 0 947.51 31.20 3 5 0 888.31 29.50 3 5 0 939.81 29.80 3 5 0 926.31 30.40 3 5 0 821.62 29.10 3 5 0 889.61 29.80 -4 -5 0 108.19 6.70 -4 -5 0 97.59 4.80 -4 -5 0 106.79 4.50 -4 -5 0 110.39 5.10 -4 -5 0 104.19 5.10 -4 -5 0 107.69 5.50 -4 -5 0 100.59 4.40 -4 -5 0 107.19 5.10 -4 -5 0 108.39 4.70 4 5 0 101.79 5.80 4 5 0 109.09 4.20 4 5 0 109.39 5.00 4 5 0 113.29 5.10 4 5 0 106.49 5.20 4 5 0 108.99 5.80 -5 -5 0 0.80 1.00 -5 -5 0 2.80 1.50 -5 -5 0 4.70 1.50 -5 -5 0 1.40 1.10 -5 -5 0 1.90 1.60 -5 -5 0 2.60 1.40 -5 -5 0 0.40 1.70 -5 -5 0 3.10 1.50 -5 -5 0 1.00 1.20 -5 -5 0 0.60 1.10 -5 -5 0 2.30 4.50 -5 -5 0 5.50 2.60 5 5 0 0.50 2.30 5 5 0 0.30 2.50 5 5 0 8.50 3.00 5 5 0 0.40 1.70 5 5 0 1.10 1.80 5 5 0 3.50 1.00 5 5 0 5.40 2.20 5 5 0 0.70 3.30 -6 -5 0 165.68 6.70 -6 -5 0 178.08 7.10 -6 -5 0 174.88 7.70 -6 -5 0 174.38 7.00 -6 -5 0 172.78 7.00 -6 -5 0 170.88 7.30 -6 -5 0 175.08 7.80 -6 -5 0 177.58 7.40 6 5 0 170.28 6.50 6 5 0 165.68 8.40 6 5 0 170.48 7.60 6 5 0 160.08 6.70 6 5 0 169.18 8.80 -7 -5 0 5.40 1.20 -7 -5 0 8.70 1.40 -7 -5 0 6.50 1.40 -7 -5 0 5.50 1.50 -7 -5 0 4.40 1.30 7 5 0 6.20 1.20 7 5 0 6.50 2.00 7 5 0 12.40 3.90 7 5 0 13.50 3.00 -8 -5 0 2.60 0.90 -8 -5 0 4.30 1.50 -8 -5 0 3.20 1.10 8 5 0 2.60 0.90 7 -6 0 1.60 0.90 7 -6 0 1.30 1.40 7 -6 0 2.00 0.70 -7 6 0 1.20 1.00 -7 6 0 0.90 0.90 -7 6 0 1.10 1.30 -7 6 0 2.00 1.20 -7 6 0 1.60 1.00 6 -6 0 37.20 2.50 6 -6 0 26.10 4.40 6 -6 0 33.40 4.30 6 -6 0 38.70 2.50 6 -6 0 34.00 3.70 -6 6 0 37.00 2.80 -6 6 0 40.20 3.40 -6 6 0 39.40 2.60 -6 6 0 41.10 2.70 5 -6 0 15.80 2.00 5 -6 0 15.80 1.90 5 -6 0 14.60 3.20 5 -6 0 14.90 3.40 5 -6 0 15.10 1.80 5 -6 0 14.30 1.80 5 -6 0 16.00 3.20 5 -6 0 5.70 3.30 -5 6 0 19.10 2.20 -5 6 0 12.80 4.00 -5 6 0 14.30 2.00 -5 6 0 15.40 4.10 -5 6 0 12.20 1.30 -5 6 0 10.70 2.00 4 -6 0 119.79 6.50 4 -6 0 131.79 5.20 4 -6 0 135.99 6.90 4 -6 0 142.09 6.90 4 -6 0 125.69 7.20 4 -6 0 125.59 5.40 4 -6 0 131.89 5.60 4 -6 0 127.39 6.70 -4 6 0 135.89 8.20 -4 6 0 137.89 7.50 -4 6 0 127.69 6.20 -4 6 0 116.19 7.70 -4 6 0 128.29 5.70 -4 6 0 122.69 9.10 -4 6 0 132.99 5.00 -4 6 0 121.19 6.70 3 -6 0 37.10 3.60 3 -6 0 35.90 2.20 3 -6 0 35.30 3.40 3 -6 0 41.50 3.30 3 -6 0 35.60 3.30 3 -6 0 38.70 3.60 -3 6 0 35.90 1.80 -3 6 0 39.40 4.10 -3 6 0 38.40 5.00 -3 6 0 29.80 3.90 -3 6 0 35.70 2.50 -3 6 0 38.90 3.20 -3 6 0 42.40 4.60 -3 6 0 42.50 3.90 -3 6 0 34.20 4.20 2 -6 0 968.10 32.30 2 -6 0 947.81 32.20 2 -6 0 927.81 32.00 2 -6 0 989.00 32.40 2 -6 0 967.20 32.10 -2 6 0 946.01 33.20 -2 6 0 990.90 33.20 -2 6 0 961.20 33.00 -2 6 0 933.31 31.40 -2 6 0 972.40 32.10 -2 6 0 949.11 32.30 -2 6 0 995.70 32.80 -2 6 0 958.80 32.20 1 -6 0 362.66 12.40 1 -6 0 348.87 12.60 1 -6 0 353.16 12.80 1 -6 0 346.67 12.30 -1 6 0 345.27 12.60 -1 6 0 342.27 13.00 -1 6 0 350.36 13.00 -1 6 0 350.76 13.40 -1 6 0 356.76 13.50 -1 6 0 355.46 12.60 0 -6 0 89.89 4.00 0 -6 0 86.59 4.40 0 -6 0 91.39 3.70 0 -6 0 90.19 3.70 0 6 0 90.99 4.10 0 6 0 91.59 4.40 0 6 0 94.89 5.00 0 6 0 87.39 3.80 0 6 0 92.49 4.60 0 6 0 93.39 4.50 -1 -6 0 327.27 12.20 -1 -6 0 349.37 13.00 -1 -6 0 347.97 11.50 1 6 0 342.37 12.30 1 6 0 332.37 11.90 1 6 0 355.76 12.90 1 6 0 320.27 12.10 1 6 0 348.17 12.10 -2 -6 0 985.10 32.50 2 6 0 959.80 32.40 2 6 0 952.10 31.10 2 6 0 934.11 31.00 2 6 0 952.70 31.60 2 6 0 880.31 30.50 2 6 0 961.20 31.10 2 6 0 934.11 31.40 -3 -6 0 35.30 4.30 3 6 0 37.60 4.30 3 6 0 37.20 3.40 3 6 0 39.50 3.00 3 6 0 28.70 2.90 3 6 0 37.80 2.80 3 6 0 37.80 1.90 3 6 0 30.70 3.70 -4 -6 0 127.49 5.20 -4 -6 0 112.29 4.90 -4 -6 0 116.89 4.80 -4 -6 0 129.99 5.40 -4 -6 0 127.39 5.50 -4 -6 0 124.19 5.90 -4 -6 0 127.39 5.70 -4 -6 0 120.59 5.80 -4 -6 0 139.89 8.60 -4 -6 0 126.19 5.10 -4 -6 0 126.59 6.20 -4 -6 0 112.29 5.70 4 6 0 130.99 6.10 4 6 0 125.39 6.80 4 6 0 120.19 8.40 4 6 0 110.39 5.80 4 6 0 131.39 4.90 4 6 0 133.99 6.20 4 6 0 136.29 8.30 4 6 0 133.59 5.70 -5 -6 0 17.90 2.00 -5 -6 0 15.30 2.30 -5 -6 0 13.30 1.70 -5 -6 0 16.80 2.00 -5 -6 0 16.10 2.10 -5 -6 0 13.00 1.80 -5 -6 0 20.60 6.00 -5 -6 0 18.10 1.90 -5 -6 0 14.10 2.00 -5 -6 0 15.50 2.00 -5 -6 0 13.90 1.90 5 6 0 14.50 1.90 5 6 0 13.90 1.60 5 6 0 8.20 3.40 5 6 0 13.20 2.10 5 6 0 10.20 3.00 5 6 0 15.40 2.50 5 6 0 12.20 4.50 -6 -6 0 37.30 3.40 -6 -6 0 39.70 3.80 -6 -6 0 35.60 2.70 -6 -6 0 34.10 2.50 -6 -6 0 37.90 3.10 -6 -6 0 37.20 3.00 -6 -6 0 38.60 2.50 -6 -6 0 39.60 2.80 6 6 0 37.90 2.70 6 6 0 39.90 3.20 6 6 0 37.70 4.10 6 6 0 35.50 2.30 6 6 0 29.90 4.70 6 6 0 38.70 4.50 -7 -6 0 0.20 1.20 -7 -6 0 1.10 1.60 -7 -6 0 0.30 1.00 -7 -6 0 2.60 1.10 -7 -6 0 0.60 1.60 -7 -6 0 2.10 1.10 7 6 0 6.90 3.20 7 6 0 0.80 1.10 7 6 0 1.60 1.10 7 -7 0 97.19 3.80 -7 7 0 97.69 4.20 -7 7 0 94.79 3.80 -7 7 0 88.19 4.40 -7 7 0 88.29 3.80 -7 7 0 99.49 4.00 6 -7 0 42.00 2.50 6 -7 0 39.70 2.90 6 -7 0 40.10 4.60 6 -7 0 40.50 2.60 -6 7 0 39.70 2.90 -6 7 0 39.70 2.60 -6 7 0 43.10 2.60 -6 7 0 44.70 3.60 5 -7 0 79.29 3.80 5 -7 0 84.89 6.60 5 -7 0 61.79 7.20 5 -7 0 72.59 4.00 5 -7 0 79.29 3.90 5 -7 0 74.99 3.70 -5 7 0 85.19 8.80 -5 7 0 74.39 4.20 -5 7 0 74.19 4.60 -5 7 0 62.49 6.40 -5 7 0 81.69 7.30 4 -7 0 6.20 1.30 4 -7 0 8.70 2.60 4 -7 0 7.20 1.50 4 -7 0 9.80 1.40 4 -7 0 4.00 2.60 4 -7 0 9.20 1.40 4 -7 0 8.00 2.90 4 -7 0 9.90 3.20 -4 7 0 -0.40 4.90 -4 7 0 5.40 1.60 -4 7 0 2.00 3.30 -4 7 0 2.50 3.20 -4 7 0 9.50 2.50 -4 7 0 8.20 1.80 -4 7 0 8.30 1.00 -4 7 0 10.00 2.00 3 -7 0 2.00 1.90 3 -7 0 0.30 1.10 3 -7 0 0.50 1.50 3 -7 0 -1.00 1.90 3 -7 0 1.50 2.30 3 -7 0 1.90 2.80 3 -7 0 0.70 1.10 3 -7 0 2.00 1.80 3 -7 0 -0.30 1.20 -3 7 0 3.00 2.70 -3 7 0 1.10 2.00 -3 7 0 -1.00 2.40 -3 7 0 0.10 1.20 -3 7 0 0.20 1.70 -3 7 0 0.70 0.60 -3 7 0 -1.10 1.60 -3 7 0 -0.50 2.40 -3 7 0 0.50 0.90 -3 7 0 1.80 3.90 2 -7 0 -1.80 1.60 2 -7 0 0.70 1.50 2 -7 0 -1.10 1.60 2 -7 0 1.10 1.60 -2 7 0 -0.80 0.60 -2 7 0 0.60 1.70 -2 7 0 -0.20 1.70 -2 7 0 -0.40 2.70 -2 7 0 -3.20 2.40 -2 7 0 0.70 0.90 -2 7 0 -0.30 1.70 -2 7 0 -1.00 0.70 -2 7 0 -2.30 2.80 -2 7 0 -0.30 2.30 1 -7 0 107.39 5.00 1 -7 0 107.29 4.80 1 -7 0 102.39 4.80 1 -7 0 104.89 5.40 -1 7 0 102.19 5.10 -1 7 0 106.79 4.40 -1 7 0 107.39 6.20 -1 7 0 110.69 6.40 -1 7 0 103.19 5.20 -1 7 0 109.79 5.60 -1 7 0 106.69 5.60 0 -7 0 -0.10 1.60 0 -7 0 0.10 1.50 0 -7 0 0.00 1.00 0 -7 0 -0.10 1.30 0 7 0 -1.30 1.40 0 7 0 0.90 1.50 0 7 0 4.20 2.10 0 7 0 2.10 2.50 0 7 0 0.20 1.10 0 7 0 0.10 0.60 0 7 0 0.70 1.40 -1 -7 0 107.99 4.20 -1 -7 0 100.59 5.70 1 7 0 105.59 4.60 1 7 0 105.69 5.50 1 7 0 107.99 4.90 1 7 0 105.89 4.20 1 7 0 108.29 5.20 1 7 0 107.69 6.30 -2 -7 0 2.40 2.40 2 7 0 2.50 1.60 2 7 0 2.60 1.80 2 7 0 -1.10 1.40 2 7 0 5.60 2.80 2 7 0 1.30 1.40 -3 -7 0 -2.40 1.30 -3 -7 0 -1.40 1.50 -3 -7 0 0.90 0.90 -3 -7 0 1.10 3.10 -3 -7 0 -1.50 0.90 -3 -7 0 -0.40 1.20 -3 -7 0 1.80 1.60 -3 -7 0 1.70 0.90 -3 -7 0 3.90 1.60 3 7 0 -2.50 2.50 3 7 0 -0.80 1.90 3 7 0 0.20 1.60 3 7 0 0.00 2.30 3 7 0 -1.50 1.80 3 7 0 3.30 3.80 -4 -7 0 8.60 1.30 -4 -7 0 8.60 2.00 -4 -7 0 9.10 4.80 -4 -7 0 5.50 1.20 -4 -7 0 9.10 1.20 -4 -7 0 6.90 1.50 -4 -7 0 7.60 1.50 -4 -7 0 9.60 1.90 -4 -7 0 6.20 1.10 -4 -7 0 6.10 1.50 -4 -7 0 7.70 1.70 -4 -7 0 6.90 1.90 4 7 0 6.20 3.60 4 7 0 7.20 1.10 4 7 0 7.20 2.10 4 7 0 4.60 1.60 4 7 0 7.20 2.00 4 7 0 9.70 3.30 4 7 0 11.80 2.70 4 7 0 5.00 2.80 -5 -7 0 78.79 3.70 -5 -7 0 80.09 4.10 -5 -7 0 74.09 3.50 -5 -7 0 78.89 4.80 -5 -7 0 64.29 4.30 -5 -7 0 75.79 4.60 -5 -7 0 77.99 3.60 -5 -7 0 78.39 4.10 -5 -7 0 82.49 4.50 5 7 0 67.19 4.30 5 7 0 79.29 3.90 5 7 0 89.59 6.70 5 7 0 76.19 3.50 5 7 0 70.99 7.00 5 7 0 76.69 5.10 -6 -7 0 42.30 3.40 -6 -7 0 45.00 3.50 -6 -7 0 45.90 3.20 -6 -7 0 43.40 2.90 -6 -7 0 44.60 3.00 -6 -7 0 43.20 2.60 -6 -7 0 43.40 2.60 6 7 0 36.60 4.90 6 7 0 45.40 2.50 6 7 0 43.60 2.80 6 7 0 41.70 5.10 6 7 0 47.40 4.80 -7 -7 0 104.09 4.50 -7 -7 0 102.49 4.30 -7 -7 0 100.99 4.30 -7 -7 0 97.69 4.60 7 7 0 98.99 4.00 7 7 0 97.19 4.10 7 -8 0 0.20 0.60 -7 8 0 -1.20 0.90 -7 8 0 -0.70 1.00 -7 8 0 -0.20 0.70 6 -8 0 34.80 2.50 6 -8 0 39.70 2.30 6 -8 0 33.70 2.70 6 -8 0 30.60 2.60 -6 8 0 36.10 3.10 -6 8 0 44.10 2.80 5 -8 0 1.30 1.10 5 -8 0 -1.20 1.10 5 -8 0 3.90 3.10 -5 8 0 2.40 4.50 -5 8 0 0.50 1.80 -5 8 0 1.10 1.80 -5 8 0 3.20 4.90 -5 8 0 -2.90 3.10 4 -8 0 39.50 2.60 4 -8 0 42.30 4.70 4 -8 0 40.50 4.60 4 -8 0 38.70 2.70 4 -8 0 29.90 4.50 4 -8 0 35.30 2.60 -4 8 0 39.80 5.20 -4 8 0 33.70 2.00 -4 8 0 32.70 3.80 -4 8 0 43.10 9.00 -4 8 0 35.00 2.90 -4 8 0 35.60 3.10 -4 8 0 37.80 4.00 -4 8 0 26.30 4.80 3 -8 0 56.39 3.20 3 -8 0 52.99 3.40 3 -8 0 56.19 5.20 3 -8 0 62.29 4.90 3 -8 0 57.39 4.80 3 -8 0 54.09 3.30 -3 8 0 65.79 4.20 -3 8 0 57.29 2.60 -3 8 0 52.89 5.80 -3 8 0 52.99 3.70 -3 8 0 58.09 3.20 -3 8 0 63.09 3.60 -3 8 0 51.99 5.60 -3 8 0 51.09 4.20 -3 8 0 63.09 5.90 2 -8 0 70.69 4.60 2 -8 0 70.89 4.70 2 -8 0 64.69 3.60 2 -8 0 68.49 3.50 2 -8 0 64.69 4.80 2 -8 0 66.89 5.10 -2 8 0 63.39 3.90 -2 8 0 67.09 2.80 -2 8 0 64.49 4.10 -2 8 0 65.59 6.00 -2 8 0 67.29 5.70 -2 8 0 70.49 4.60 -2 8 0 63.59 4.80 -2 8 0 67.09 3.30 -2 8 0 68.99 6.50 -2 8 0 61.99 6.80 -2 8 0 69.79 5.30 -2 8 0 66.69 4.80 1 -8 0 6.90 2.00 1 -8 0 7.90 2.00 1 -8 0 6.10 1.20 1 -8 0 6.70 3.80 1 -8 0 5.70 1.10 -1 8 0 7.10 2.30 -1 8 0 5.90 1.90 -1 8 0 4.50 0.90 -1 8 0 4.00 2.20 -1 8 0 5.30 1.30 -1 8 0 4.80 1.00 -1 8 0 4.60 2.20 -1 8 0 -0.10 3.10 -1 8 0 5.30 1.50 -1 8 0 2.50 2.10 0 -8 0 488.55 16.90 0 -8 0 467.95 18.00 0 8 0 509.15 18.40 0 8 0 505.85 16.90 0 8 0 509.25 18.20 0 8 0 504.15 19.30 0 8 0 529.95 17.90 0 8 0 490.25 16.90 0 8 0 487.45 17.90 -1 -8 0 2.10 1.30 -1 -8 0 3.90 1.10 -1 -8 0 4.70 0.90 1 8 0 9.00 2.40 1 8 0 5.00 2.20 1 8 0 4.30 1.00 1 8 0 8.30 3.00 1 8 0 6.20 1.00 1 8 0 5.50 2.00 1 8 0 5.00 1.70 1 8 0 7.40 2.10 1 8 0 7.10 3.20 -2 -8 0 64.99 3.70 -2 -8 0 68.19 3.40 -2 -8 0 67.49 4.20 -2 -8 0 64.89 3.40 -2 -8 0 65.89 3.00 -2 -8 0 62.29 3.10 2 8 0 66.09 3.10 2 8 0 69.69 4.30 2 8 0 69.19 5.50 2 8 0 59.99 8.00 2 8 0 64.29 4.90 2 8 0 60.39 3.60 2 8 0 61.99 4.40 2 8 0 64.59 3.30 2 8 0 59.39 3.60 -3 -8 0 55.89 2.70 -3 -8 0 50.19 3.00 -3 -8 0 58.99 3.50 -3 -8 0 58.69 3.90 -3 -8 0 53.89 2.90 -3 -8 0 42.60 3.90 -3 -8 0 53.59 3.10 -3 -8 0 50.19 6.90 -3 -8 0 57.39 4.20 -3 -8 0 56.69 3.40 -3 -8 0 53.09 3.00 -3 -8 0 53.99 2.70 3 8 0 47.50 4.90 3 8 0 50.19 6.00 3 8 0 53.49 4.40 3 8 0 53.49 3.50 3 8 0 50.09 5.40 3 8 0 53.79 3.30 3 8 0 63.29 4.30 3 8 0 54.99 2.80 -4 -8 0 39.00 2.90 -4 -8 0 35.00 2.30 -4 -8 0 30.00 3.30 -4 -8 0 35.60 2.20 -4 -8 0 29.00 3.50 -4 -8 0 28.70 2.90 -4 -8 0 33.60 2.40 -4 -8 0 35.20 2.10 -4 -8 0 29.10 3.20 -4 -8 0 31.30 6.80 4 8 0 33.60 4.00 4 8 0 24.60 4.10 4 8 0 25.90 4.40 4 8 0 34.70 2.20 4 8 0 36.10 2.80 4 8 0 33.90 5.20 4 8 0 35.30 3.10 4 8 0 29.70 4.30 -5 -8 0 0.20 0.90 -5 -8 0 3.10 1.70 -5 -8 0 1.50 1.40 -5 -8 0 3.30 2.00 -5 -8 0 1.10 1.60 5 8 0 3.30 1.40 5 8 0 -2.80 5.10 5 8 0 6.30 2.80 5 8 0 4.00 1.10 5 8 0 2.30 1.80 5 8 0 0.50 4.60 -6 -8 0 35.00 2.40 -6 -8 0 36.80 2.60 -6 -8 0 37.40 2.70 -6 -8 0 38.30 2.30 6 8 0 36.70 2.20 6 8 0 34.90 2.50 6 8 0 41.60 5.90 6 8 0 28.50 3.70 -7 -8 0 0.60 0.90 -7 -8 0 3.60 1.40 -7 -8 0 0.70 0.80 -7 -8 0 1.20 1.00 7 8 0 0.20 0.90 6 -9 0 4.10 1.10 6 -9 0 5.20 0.90 -6 9 0 5.80 1.00 -6 9 0 4.30 0.90 -6 9 0 2.60 1.10 5 -9 0 11.90 1.50 5 -9 0 10.50 1.40 5 -9 0 9.30 1.50 5 -9 0 4.00 3.40 -5 9 0 4.10 4.90 -5 9 0 4.50 3.40 -5 9 0 9.30 1.50 -5 9 0 9.80 1.40 4 -9 0 4.20 1.20 4 -9 0 3.60 1.10 4 -9 0 0.70 3.00 4 -9 0 4.70 1.30 -4 9 0 3.00 4.40 -4 9 0 4.50 2.10 -4 9 0 5.80 1.60 -4 9 0 13.50 4.50 -4 9 0 4.70 1.50 3 -9 0 382.56 13.40 3 -9 0 382.06 13.50 3 -9 0 391.66 15.00 3 -9 0 346.57 15.20 3 -9 0 367.36 13.10 3 -9 0 351.46 15.50 -3 9 0 364.66 13.40 -3 9 0 388.96 16.10 -3 9 0 397.26 16.30 -3 9 0 368.16 13.80 -3 9 0 379.96 13.30 -3 9 0 381.76 14.20 2 -9 0 34.70 2.50 2 -9 0 22.80 4.90 2 -9 0 31.10 3.70 2 -9 0 31.80 2.40 2 -9 0 32.40 4.40 2 -9 0 38.30 2.70 2 -9 0 34.10 2.00 -2 9 0 32.20 4.10 -2 9 0 33.90 2.30 -2 9 0 38.20 3.30 -2 9 0 35.00 2.50 -2 9 0 33.40 3.20 -2 9 0 20.10 4.70 -2 9 0 28.60 2.70 -2 9 0 29.90 5.70 -2 9 0 33.90 4.40 -2 9 0 33.50 4.40 -2 9 0 38.80 5.00 1 -9 0 106.49 4.80 1 -9 0 109.09 5.80 1 -9 0 98.69 5.00 1 -9 0 104.29 4.60 1 -9 0 89.29 7.20 -1 9 0 112.79 4.80 -1 9 0 103.99 6.40 -1 9 0 109.89 7.20 -1 9 0 110.59 7.00 -1 9 0 106.29 5.20 -1 9 0 103.99 6.70 -1 9 0 101.59 4.60 -1 9 0 113.59 8.60 -1 9 0 109.49 5.00 -1 9 0 104.59 6.20 0 -9 0 0.20 1.50 0 -9 0 -1.00 0.70 0 -9 0 1.30 1.20 0 -9 0 1.00 1.00 0 -9 0 -0.60 1.00 0 9 0 -1.00 2.10 0 9 0 -3.60 2.40 0 9 0 -5.10 4.50 0 9 0 0.30 2.60 0 9 0 -0.70 1.10 0 9 0 0.10 1.20 0 9 0 1.20 2.50 0 9 0 0.10 0.80 0 9 0 -0.70 0.80 0 9 0 0.50 2.10 -1 -9 0 101.99 5.40 -1 -9 0 101.79 4.30 -1 -9 0 110.09 4.80 -1 -9 0 105.29 4.40 -1 -9 0 105.59 4.50 -1 -9 0 112.79 5.60 1 9 0 111.19 5.40 1 9 0 99.79 4.90 1 9 0 112.49 4.60 1 9 0 104.89 5.90 1 9 0 115.89 6.30 1 9 0 115.09 7.50 1 9 0 98.09 8.20 1 9 0 95.89 7.70 1 9 0 102.49 4.80 -2 -9 0 37.10 2.40 -2 -9 0 36.80 3.50 -2 -9 0 38.50 2.30 -2 -9 0 33.20 2.50 -2 -9 0 36.80 2.00 -2 -9 0 34.00 2.10 -2 -9 0 33.30 2.90 -2 -9 0 35.50 2.10 -2 -9 0 34.10 2.50 2 9 0 38.60 2.30 2 9 0 28.90 2.40 2 9 0 34.50 4.50 2 9 0 34.00 4.20 2 9 0 30.90 2.90 2 9 0 34.40 4.00 2 9 0 35.00 2.80 2 9 0 44.70 4.80 -3 -9 0 373.46 13.10 -3 -9 0 389.66 13.50 -3 -9 0 368.66 13.60 -3 -9 0 396.86 13.30 -3 -9 0 388.86 14.20 -3 -9 0 372.76 15.50 -3 -9 0 367.06 13.10 -3 -9 0 379.76 13.10 -3 -9 0 391.86 13.80 3 9 0 356.06 16.20 3 9 0 398.56 14.80 3 9 0 383.26 13.50 3 9 0 376.66 13.70 3 9 0 400.66 14.70 -4 -9 0 7.30 1.50 -4 -9 0 5.20 1.00 -4 -9 0 6.20 1.10 -4 -9 0 3.00 1.70 -4 -9 0 6.50 1.60 -4 -9 0 4.70 1.20 -4 -9 0 5.00 0.90 4 9 0 3.40 1.60 4 9 0 1.70 2.90 4 9 0 6.00 1.20 4 9 0 5.60 1.40 -5 -9 0 10.70 1.30 -5 -9 0 10.40 1.70 -5 -9 0 10.10 1.80 -5 -9 0 11.80 1.60 -5 -9 0 8.20 1.50 -5 -9 0 10.30 1.20 5 9 0 18.30 3.40 5 9 0 11.50 1.40 5 9 0 5.10 3.30 5 9 0 9.40 1.60 -6 -9 0 7.00 1.30 -6 -9 0 6.80 1.60 -6 -9 0 3.10 1.00 -6 -9 0 5.80 1.20 -6 -9 0 4.30 0.90 6 9 0 3.00 1.10 6 9 0 5.90 1.10 6 -10 0 15.10 1.30 6 -10 0 14.90 1.50 -6 10 0 13.70 2.10 -6 10 0 16.30 1.40 5 -10 0 -0.10 0.80 5 -10 0 2.10 0.90 5 -10 0 1.50 0.80 5 -10 0 1.20 1.70 -5 10 0 4.10 1.20 -5 10 0 -2.00 5.20 4 -10 0 2.00 4.40 4 -10 0 4.40 1.00 -4 10 0 1.70 4.80 -4 10 0 -9.60 8.60 -4 10 0 5.20 1.40 -4 10 0 6.90 2.10 3 -10 0 21.90 2.30 3 -10 0 24.50 2.30 3 -10 0 30.60 3.90 3 -10 0 25.80 2.20 -3 10 0 27.00 2.70 -3 10 0 26.80 2.30 -3 10 0 29.20 5.20 -3 10 0 20.30 4.80 -3 10 0 18.60 2.20 -3 10 0 22.90 2.90 2 -10 0 214.38 9.50 2 -10 0 213.68 8.10 2 -10 0 208.08 7.90 2 -10 0 205.38 7.90 2 -10 0 196.48 7.40 -2 10 0 205.58 8.50 -2 10 0 227.18 11.20 -2 10 0 209.88 10.70 -2 10 0 203.18 8.10 -2 10 0 213.28 8.10 -2 10 0 202.58 8.00 -2 10 0 186.28 10.50 -2 10 0 192.88 12.20 -2 10 0 208.08 8.70 1 -10 0 69.29 3.70 1 -10 0 81.59 4.00 1 -10 0 71.09 3.40 1 -10 0 70.79 4.70 -1 10 0 69.69 6.10 -1 10 0 69.89 3.70 -1 10 0 81.59 4.40 -1 10 0 80.09 4.10 -1 10 0 78.09 6.90 -1 10 0 84.49 6.90 -1 10 0 87.79 6.90 -1 10 0 78.19 3.80 -1 10 0 74.99 6.80 0 -10 0 1.50 0.80 0 -10 0 0.80 0.70 0 -10 0 1.50 1.10 0 -10 0 2.60 2.30 0 -10 0 0.60 0.70 0 -10 0 0.00 1.30 0 10 0 -2.30 2.90 0 10 0 1.50 0.90 0 10 0 5.30 3.30 0 10 0 1.90 0.90 0 10 0 2.40 3.70 0 10 0 0.50 2.70 0 10 0 1.10 2.80 0 10 0 1.40 1.60 -1 -10 0 81.99 6.00 -1 -10 0 80.89 3.70 -1 -10 0 78.99 3.50 -1 -10 0 86.49 4.70 -1 -10 0 70.39 5.10 -1 -10 0 69.69 3.90 1 10 0 72.79 5.90 1 10 0 72.99 3.80 1 10 0 77.79 6.60 1 10 0 62.79 6.60 1 10 0 76.39 5.90 1 10 0 78.59 3.80 1 10 0 76.69 4.30 -2 -10 0 203.58 8.40 -2 -10 0 211.28 9.00 -2 -10 0 217.78 8.10 -2 -10 0 226.98 7.90 -2 -10 0 213.18 7.70 -2 -10 0 212.88 7.90 -2 -10 0 208.68 8.00 -2 -10 0 220.88 7.90 -2 -10 0 220.78 8.10 2 10 0 219.58 8.40 2 10 0 215.48 8.60 2 10 0 230.38 10.10 2 10 0 199.48 9.90 2 10 0 203.88 8.10 2 10 0 225.68 8.20 2 10 0 226.68 10.80 -3 -10 0 24.30 3.20 -3 -10 0 30.90 2.70 -3 -10 0 22.00 1.70 -3 -10 0 22.70 1.80 -3 -10 0 26.20 1.80 -3 -10 0 22.10 3.80 -3 -10 0 21.70 2.10 -3 -10 0 23.40 2.00 -3 -10 0 27.90 2.10 3 10 0 24.70 2.50 3 10 0 23.80 2.40 3 10 0 27.20 4.50 3 10 0 25.80 2.10 3 10 0 27.70 3.90 -4 -10 0 5.80 0.90 -4 -10 0 2.40 1.80 -4 -10 0 6.90 1.70 -4 -10 0 6.30 1.10 -4 -10 0 6.30 1.40 -4 -10 0 3.60 0.90 -4 -10 0 4.10 1.10 4 10 0 3.70 3.20 4 10 0 10.50 4.50 4 10 0 5.10 1.30 4 10 0 3.50 1.40 4 10 0 3.20 1.70 -5 -10 0 2.40 1.40 -5 -10 0 4.60 1.70 -5 -10 0 2.00 0.90 -5 -10 0 0.20 0.80 -5 -10 0 2.40 0.90 5 10 0 3.80 3.50 5 10 0 1.30 1.10 5 10 0 0.80 1.00 5 10 0 7.50 2.10 -6 -10 0 16.00 1.90 -6 -10 0 17.60 1.40 -6 -10 0 16.20 3.00 6 10 0 18.80 1.70 6 10 0 16.10 1.80 5 -11 0 75.59 3.30 5 -11 0 74.89 3.00 -5 11 0 68.39 3.70 -5 11 0 74.59 3.70 -5 11 0 80.89 3.20 4 -11 0 6.80 1.10 4 -11 0 6.90 1.10 -4 11 0 8.20 2.10 -4 11 0 7.30 1.60 -4 11 0 14.60 5.50 3 -11 0 15.60 1.90 3 -11 0 15.50 1.70 -3 11 0 15.10 2.00 -3 11 0 13.70 1.90 -3 11 0 12.50 2.10 -3 11 0 -0.70 8.80 -3 11 0 4.50 4.90 2 -11 0 63.79 3.60 2 -11 0 76.09 3.60 -2 11 0 68.09 4.30 -2 11 0 69.79 8.30 -2 11 0 66.89 3.60 -2 11 0 56.79 7.10 -2 11 0 67.59 3.80 -2 11 0 71.29 3.80 -2 11 0 48.30 8.10 1 -11 0 70.19 3.40 1 -11 0 73.59 3.70 1 -11 0 70.99 3.20 1 -11 0 66.49 3.70 1 -11 0 66.59 3.20 1 -11 0 68.99 3.20 -1 11 0 78.29 3.70 -1 11 0 68.69 3.90 -1 11 0 76.09 4.30 -1 11 0 63.39 7.30 -1 11 0 75.59 7.20 -1 11 0 71.99 3.70 0 -11 0 -0.40 0.60 0 -11 0 -1.70 0.70 0 -11 0 -0.10 0.80 0 -11 0 -0.20 0.60 0 -11 0 1.60 1.60 0 11 0 0.70 0.90 0 11 0 -0.70 1.30 0 11 0 -0.20 1.10 0 11 0 -0.90 3.40 0 11 0 2.90 3.30 0 11 0 -0.50 1.00 -1 -11 0 72.59 3.30 -1 -11 0 67.69 3.30 -1 -11 0 69.39 3.40 -1 -11 0 75.29 3.30 -1 -11 0 72.09 3.10 -1 -11 0 67.19 3.40 1 11 0 56.29 6.90 1 11 0 67.69 3.60 1 11 0 78.99 6.50 1 11 0 66.89 4.10 1 11 0 73.59 3.90 1 11 0 74.59 3.70 1 11 0 73.79 7.00 -2 -11 0 67.19 3.40 -2 -11 0 68.89 3.20 -2 -11 0 67.19 3.50 -2 -11 0 70.39 3.20 -2 -11 0 66.79 3.30 2 11 0 62.69 3.60 2 11 0 74.09 3.60 2 11 0 73.69 3.70 2 11 0 73.89 6.30 2 11 0 69.49 7.40 2 11 0 71.39 4.10 -3 -11 0 15.50 1.80 -3 -11 0 14.00 1.70 -3 -11 0 14.80 1.50 -3 -11 0 12.30 2.10 -3 -11 0 18.60 1.90 -3 -11 0 16.50 1.90 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4 20.40 1.90 3 -11 4 22.00 1.90 -4 11 -4 6.70 1.00 -4 11 -4 6.40 1.20 4 -11 4 6.90 1.00 4 -11 4 7.30 1.10 4 -11 4 6.30 1.80 -5 11 -4 34.50 1.90 -5 11 -4 31.50 1.70 5 -11 4 34.80 2.20 6 10 -4 19.90 1.70 6 10 -4 23.20 2.10 6 10 -4 26.60 2.10 6 10 -4 17.70 1.90 -6 -10 4 25.20 1.60 -6 -10 4 22.30 1.90 -6 -10 4 23.20 1.50 5 10 -4 5.80 4.00 5 10 -4 5.80 1.20 5 10 -4 4.50 1.10 5 10 -4 15.60 5.30 -5 -10 4 4.00 1.40 -5 -10 4 5.30 1.00 -5 -10 4 4.20 0.90 -5 -10 4 4.30 0.90 4 10 -4 180.88 10.20 4 10 -4 143.49 9.30 4 10 -4 151.18 8.80 4 10 -4 176.58 6.70 4 10 -4 171.88 6.80 -4 -10 4 170.78 6.60 -4 -10 4 158.88 6.70 -4 -10 4 178.18 6.50 -4 -10 4 171.88 6.60 -4 -10 4 159.98 6.20 -4 -10 4 170.38 6.30 3 10 -4 103.79 8.40 3 10 -4 92.49 7.30 3 10 -4 100.19 4.70 3 10 -4 101.79 4.70 3 10 -4 101.09 4.60 3 10 -4 95.89 7.00 3 10 -4 100.39 4.90 3 10 -4 87.19 6.90 -3 -10 4 102.09 4.80 -3 -10 4 102.19 4.40 -3 -10 4 96.39 4.20 -3 -10 4 103.59 4.30 -3 -10 4 102.89 4.40 2 10 -4 6.60 1.50 2 10 -4 6.20 1.30 2 10 -4 2.90 5.70 2 10 -4 6.70 1.40 2 10 -4 5.50 3.40 2 10 -4 7.50 4.40 2 10 -4 5.90 1.50 -2 -10 4 7.50 1.30 -2 -10 4 7.70 1.50 -2 -10 4 8.20 1.10 -2 -10 4 8.00 1.30 -2 -10 4 3.80 1.30 1 10 -4 69.79 5.60 1 10 -4 75.49 7.60 1 10 -4 73.99 6.80 1 10 -4 83.99 4.20 1 10 -4 77.29 6.10 1 10 -4 76.89 3.90 1 10 -4 74.19 4.30 1 10 -4 81.69 4.00 1 10 -4 90.99 8.20 1 10 -4 79.09 3.90 1 10 -4 82.59 7.80 1 10 -4 79.59 7.30 -1 -10 4 82.99 4.30 -1 -10 4 76.99 3.70 -1 -10 4 75.19 3.90 0 10 -4 -3.00 5.40 0 10 -4 -5.10 3.70 0 10 -4 3.30 2.20 0 10 -4 2.10 1.00 0 10 -4 -5.10 5.10 0 10 -4 -8.70 4.90 0 10 -4 5.90 4.40 0 10 -4 2.60 1.50 0 10 -4 2.70 1.30 0 10 -4 2.50 1.40 0 -10 4 2.70 1.70 0 -10 4 2.00 1.20 0 -10 4 1.50 1.00 -1 10 -4 -0.50 1.30 -1 10 -4 7.50 5.70 -1 10 -4 1.70 6.70 -1 10 -4 1.70 5.90 -1 10 -4 7.70 7.30 -1 10 -4 3.00 1.60 -1 10 -4 -0.40 0.90 -1 10 -4 2.70 1.50 1 -10 4 -0.10 1.40 1 -10 4 1.40 1.10 1 -10 4 -2.30 5.60 1 -10 4 1.80 1.10 -2 10 -4 174.48 12.40 -2 10 -4 147.29 13.80 -2 10 -4 180.98 7.40 -2 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16.20 1.90 4 -6 7 17.30 4.10 4 -6 7 17.60 1.80 -5 6 -7 1.90 1.40 -5 6 -7 3.30 1.30 -5 6 -7 3.00 2.00 -5 6 -7 3.40 0.90 -5 6 -7 3.90 1.20 5 -6 7 0.00 2.90 5 -6 7 3.80 1.10 5 -6 7 4.90 1.10 5 -6 7 1.70 1.00 -6 6 -7 2.20 1.00 -6 6 -7 3.40 1.10 -6 6 -7 4.00 0.80 6 -6 7 2.70 0.80 6 -6 7 2.70 0.90 6 -6 7 2.20 1.20 8 5 -7 35.50 2.00 8 5 -7 37.40 2.00 -8 -5 7 39.10 2.10 -8 -5 7 39.10 2.00 7 5 -7 17.30 1.80 7 5 -7 21.40 2.70 7 5 -7 21.20 2.00 7 5 -7 16.30 1.70 7 5 -7 19.10 3.70 7 5 -7 4.20 6.20 -7 -5 7 20.50 2.40 -7 -5 7 16.10 1.90 -7 -5 7 21.20 1.90 -7 -5 7 18.20 1.90 -7 -5 7 18.70 2.00 6 5 -7 143.49 7.80 6 5 -7 142.69 6.50 6 5 -7 142.19 6.20 6 5 -7 132.49 6.00 6 5 -7 137.19 8.20 6 5 -7 129.89 7.30 6 5 -7 139.79 5.60 -6 -5 7 151.88 9.00 5 5 -7 80.49 6.10 5 5 -7 64.99 7.70 5 5 -7 82.59 3.80 5 5 -7 79.29 3.80 5 5 -7 79.19 4.70 5 5 -7 87.59 4.40 5 5 -7 88.29 5.80 5 5 -7 77.59 5.20 -5 -5 7 76.89 3.70 -5 -5 7 77.99 8.50 -5 -5 7 79.09 5.00 -5 -5 7 83.99 4.10 -5 -5 7 80.39 10.10 4 5 -7 4.10 2.30 4 5 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21.10 3.40 -6 -4 7 21.70 2.00 -6 -4 7 18.00 2.10 -6 -4 7 18.60 2.60 5 4 -7 275.67 10.90 5 4 -7 307.17 10.70 5 4 -7 310.37 12.20 5 4 -7 299.47 11.50 5 4 -7 319.37 12.60 5 4 -7 319.37 11.00 5 4 -7 324.37 12.10 5 4 -7 311.07 12.90 5 4 -7 312.47 12.40 5 4 -7 303.97 10.90 -5 -4 7 277.87 14.50 -5 -4 7 309.27 10.80 -5 -4 7 298.87 14.30 -5 -4 7 268.17 13.40 -5 -4 7 295.97 12.40 4 4 -7 32.80 3.60 4 4 -7 33.90 2.40 4 4 -7 33.90 4.40 4 4 -7 33.70 3.20 4 4 -7 30.60 2.60 4 4 -7 34.30 4.00 4 4 -7 29.60 3.90 4 4 -7 35.90 2.30 4 4 -7 31.50 2.70 -4 -4 7 27.80 4.70 -4 -4 7 30.60 4.10 -4 -4 7 35.60 3.70 -4 -4 7 34.00 4.90 -4 -4 7 33.40 2.00 -4 -4 7 31.10 6.30 3 4 -7 2.10 1.30 3 4 -7 -2.10 1.90 3 4 -7 0.50 1.60 3 4 -7 2.80 1.30 3 4 -7 -2.00 2.40 3 4 -7 -0.10 1.60 3 4 -7 1.90 1.70 3 4 -7 -1.90 0.90 -3 -4 7 -3.00 2.10 -3 -4 7 -4.10 3.70 -3 -4 7 2.60 2.90 -3 -4 7 0.10 0.70 -3 -4 7 1.20 2.80 -3 -4 7 -0.30 2.50 2 4 -7 19.60 2.40 2 4 -7 17.70 3.20 2 4 -7 23.30 2.70 2 4 -7 17.40 2.10 2 4 -7 17.50 2.10 2 4 -7 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206.68 7.80 -2 4 -8 206.78 7.70 2 -4 8 191.38 9.70 2 -4 8 207.38 10.30 2 -4 8 240.08 10.20 2 -4 8 219.28 10.10 2 -4 8 216.88 9.40 2 -4 8 211.68 8.10 -3 4 -8 23.90 2.50 -3 4 -8 22.90 2.30 -3 4 -8 22.70 2.50 -3 4 -8 21.30 2.70 -3 4 -8 27.30 3.80 -3 4 -8 23.50 2.30 -3 4 -8 28.10 2.70 -3 4 -8 24.70 2.30 -3 4 -8 26.10 3.50 3 -4 8 26.10 3.70 3 -4 8 26.00 2.00 3 -4 8 24.90 3.30 3 -4 8 22.60 2.90 3 -4 8 23.30 2.90 3 -4 8 27.90 4.10 3 -4 8 22.40 3.80 -4 4 -8 26.20 2.40 -4 4 -8 20.50 2.20 -4 4 -8 27.20 2.40 -4 4 -8 26.50 2.30 -4 4 -8 26.00 2.60 -4 4 -8 25.10 2.80 -4 4 -8 21.40 2.30 -4 4 -8 23.10 2.20 -4 4 -8 25.90 2.10 4 -4 8 27.20 2.60 4 -4 8 21.80 4.40 4 -4 8 22.00 2.50 -5 4 -8 3.20 1.70 -5 4 -8 8.90 1.40 -5 4 -8 6.90 1.20 -5 4 -8 7.00 1.40 -5 4 -8 6.50 1.40 -5 4 -8 7.90 3.10 -5 4 -8 4.50 1.60 5 -4 8 6.90 1.20 5 -4 8 7.20 1.20 5 -4 8 5.70 1.50 5 -4 8 1.90 2.90 -6 4 -8 30.20 2.20 -6 4 -8 30.40 2.80 -6 4 -8 37.50 2.10 -6 4 -8 36.60 2.30 -6 4 -8 33.20 2.20 6 -4 8 33.40 2.70 6 -4 8 38.40 2.20 6 -4 8 35.90 2.10 8 3 -8 16.70 1.30 -8 -3 8 15.80 1.40 -8 -3 8 16.30 1.60 -8 -3 8 14.30 2.20 -8 -3 8 11.10 1.50 7 3 -8 46.30 3.50 7 3 -8 52.39 2.70 7 3 -8 60.79 5.60 7 3 -8 49.80 3.00 7 3 -8 45.80 2.60 7 3 -8 37.60 10.10 -7 -3 8 54.09 3.80 -7 -3 8 52.49 2.90 -7 -3 8 47.50 3.10 6 3 -8 6.10 2.80 6 3 -8 8.00 1.40 6 3 -8 7.90 3.10 6 3 -8 6.50 1.50 6 3 -8 8.50 1.20 6 3 -8 9.40 1.60 6 3 -8 6.60 4.40 6 3 -8 8.70 1.30 -6 -3 8 5.00 1.90 5 3 -8 25.90 4.30 5 3 -8 21.20 1.90 5 3 -8 16.60 2.30 5 3 -8 21.70 2.10 5 3 -8 22.70 3.40 5 3 -8 22.00 3.90 5 3 -8 19.70 3.00 5 3 -8 14.70 2.70 5 3 -8 21.60 2.00 5 3 -8 22.00 2.00 -5 -3 8 14.00 5.20 -5 -3 8 17.80 5.70 -5 -3 8 34.60 9.50 -5 -3 8 13.50 3.80 -5 -3 8 19.00 1.70 4 3 -8 232.48 10.20 4 3 -8 245.28 9.90 4 3 -8 242.58 8.70 4 3 -8 233.48 8.80 4 3 -8 252.27 9.70 4 3 -8 227.88 8.80 4 3 -8 254.47 9.50 4 3 -8 250.07 10.50 -4 -3 8 252.57 13.20 -4 -3 8 244.58 11.90 -4 -3 8 252.57 13.40 -4 -3 8 246.88 8.80 -4 -3 8 255.77 13.10 3 3 -8 420.96 15.10 3 3 -8 451.95 15.80 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9 12.60 8.10 -5 -5 9 21.80 2.30 -5 -5 9 21.30 3.60 -5 -5 9 27.30 3.40 4 5 -9 431.26 15.60 4 5 -9 418.86 14.40 4 5 -9 419.16 14.50 4 5 -9 414.06 14.50 4 5 -9 435.86 16.40 4 5 -9 415.66 16.40 4 5 -9 435.36 15.30 4 5 -9 408.86 16.70 4 5 -9 410.06 14.80 -4 -5 9 388.56 17.60 -4 -5 9 420.66 14.50 -4 -5 9 423.16 21.10 -4 -5 9 424.06 18.60 -4 -5 9 432.56 18.20 3 5 -9 94.09 5.70 3 5 -9 89.89 4.20 3 5 -9 93.19 4.60 3 5 -9 97.09 5.70 3 5 -9 95.99 6.30 3 5 -9 88.19 4.00 3 5 -9 78.09 4.30 -3 -5 9 93.59 8.30 -3 -5 9 81.39 7.20 -3 -5 9 89.39 5.70 -3 -5 9 92.29 6.30 -3 -5 9 81.89 5.10 -3 -5 9 93.49 4.00 2 5 -9 9.10 3.10 2 5 -9 7.30 1.40 2 5 -9 7.70 2.40 2 5 -9 8.00 1.20 2 5 -9 6.50 1.30 2 5 -9 8.50 2.00 2 5 -9 2.90 3.10 2 5 -9 6.90 1.50 -2 -5 9 5.40 4.30 -2 -5 9 6.40 2.60 -2 -5 9 13.30 3.80 -2 -5 9 8.40 2.00 -2 -5 9 8.30 1.40 -2 -5 9 6.40 1.00 -2 -5 9 12.10 3.50 -2 -5 9 1.50 3.60 -2 -5 9 8.00 3.40 -2 -5 9 5.10 2.70 -2 -5 9 5.90 3.70 -2 -5 9 6.00 1.90 1 5 -9 326.47 11.70 1 5 -9 315.47 11.80 1 5 -9 306.47 12.80 1 5 -9 310.67 12.70 1 5 -9 344.97 12.20 1 5 -9 344.77 12.00 1 5 -9 316.97 12.00 -1 -5 9 334.47 11.80 -1 -5 9 304.17 13.50 -1 -5 9 301.67 14.70 -1 -5 9 317.37 11.40 -1 -5 9 333.37 13.10 -1 -5 9 333.37 13.50 -1 -5 9 336.37 13.70 -1 -5 9 342.17 13.90 -1 -5 9 329.67 15.00 -1 -5 9 311.67 13.20 0 5 -9 279.67 10.90 0 5 -9 254.47 9.20 0 5 -9 264.47 9.70 0 5 -9 274.07 10.20 0 5 -9 250.07 10.80 0 5 -9 275.67 10.00 0 5 -9 244.58 9.30 0 -5 9 255.37 10.50 0 -5 9 247.58 12.40 0 -5 9 258.37 11.00 0 -5 9 272.87 9.90 0 -5 9 251.67 11.10 0 -5 9 279.57 11.80 0 -5 9 240.88 11.70 0 -5 9 250.37 9.30 -1 5 -9 2.70 1.70 -1 5 -9 3.90 1.10 -1 5 -9 2.90 1.20 -1 5 -9 1.10 1.10 -1 5 -9 -1.70 3.60 -1 5 -9 1.80 1.00 -1 5 -9 3.70 1.10 -1 5 -9 3.00 1.00 -1 5 -9 3.50 1.60 1 -5 9 2.00 2.20 1 -5 9 4.20 4.50 1 -5 9 3.10 1.60 1 -5 9 4.70 2.90 1 -5 9 2.50 2.70 1 -5 9 2.20 1.10 1 -5 9 0.20 4.70 1 -5 9 3.60 1.90 -2 5 -9 172.28 7.20 -2 5 -9 190.08 8.10 -2 5 -9 192.48 7.20 -2 5 -9 184.68 7.30 -2 5 -9 177.68 7.20 -2 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51.99 4.00 6 4 -9 45.70 2.70 6 4 -9 46.40 2.70 6 4 -9 39.40 4.20 6 4 -9 39.60 3.10 -6 -4 9 46.70 3.80 -6 -4 9 46.40 2.80 5 4 -9 233.58 10.80 5 4 -9 243.18 9.40 5 4 -9 235.88 10.50 5 4 -9 228.18 8.70 5 4 -9 235.08 9.90 5 4 -9 223.58 13.20 5 4 -9 229.68 8.60 5 4 -9 235.38 8.60 5 4 -9 220.38 12.90 5 4 -9 237.88 8.70 -5 -4 9 242.88 8.80 -5 -4 9 234.48 13.30 -5 -4 9 234.28 13.00 -5 -4 9 239.28 10.30 -5 -4 9 251.77 11.00 4 4 -9 128.09 7.00 4 4 -9 132.79 5.40 4 4 -9 124.89 5.40 4 4 -9 125.09 5.40 4 4 -9 129.49 7.70 4 4 -9 124.99 5.40 4 4 -9 147.09 8.30 4 4 -9 134.99 7.20 4 4 -9 129.29 6.40 4 4 -9 141.49 6.00 -4 -4 9 131.39 12.10 -4 -4 9 136.69 7.10 -4 -4 9 129.49 5.30 -4 -4 9 132.49 7.80 -4 -4 9 132.39 9.90 -4 -4 9 132.29 9.00 3 4 -9 12.40 1.70 3 4 -9 15.50 2.00 3 4 -9 17.60 3.50 3 4 -9 15.60 3.00 3 4 -9 14.60 2.40 3 4 -9 16.10 2.10 3 4 -9 10.50 1.70 3 4 -9 13.20 1.80 -3 -4 9 14.00 3.70 -3 -4 9 13.20 2.00 -3 -4 9 17.20 3.30 -3 -4 9 15.10 5.10 -3 -4 9 1.50 4.90 -3 -4 9 11.00 3.80 -3 -4 9 13.20 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2.30 4 3 -9 34.20 4.00 4 3 -9 26.90 4.40 4 3 -9 27.50 3.10 4 3 -9 34.00 2.70 4 3 -9 36.20 4.50 4 3 -9 30.50 3.40 4 3 -9 36.00 3.20 4 3 -9 34.10 2.60 -4 -3 9 31.80 4.20 -4 -3 9 35.50 5.00 -4 -3 9 42.50 4.10 -4 -3 9 35.60 4.20 -4 -3 9 27.10 7.10 -4 -3 9 34.60 2.10 -4 -3 9 25.90 5.40 3 3 -9 2.10 1.20 3 3 -9 0.50 2.80 3 3 -9 2.00 0.90 3 3 -9 2.30 1.60 3 3 -9 1.80 2.30 3 3 -9 2.30 1.00 3 3 -9 0.40 1.00 3 3 -9 4.00 1.30 3 3 -9 1.20 2.00 -3 -3 9 -2.40 3.40 -3 -3 9 1.70 2.60 -3 -3 9 -1.00 3.10 -3 -3 9 2.50 0.70 -3 -3 9 -1.00 3.70 -3 -3 9 -0.50 1.40 -3 -3 9 2.00 4.20 -3 -3 9 1.00 1.90 2 3 -9 41.40 2.80 2 3 -9 46.20 2.90 2 3 -9 43.00 3.10 2 3 -9 46.30 2.90 2 3 -9 47.60 4.00 2 3 -9 46.70 4.00 2 3 -9 49.99 3.80 -2 -3 9 45.00 5.40 -2 -3 9 44.60 5.20 -2 -3 9 50.59 5.70 -2 -3 9 44.80 2.90 -2 -3 9 43.80 2.30 -2 -3 9 46.40 4.90 -2 -3 9 52.29 5.90 1 3 -9 31.50 3.40 1 3 -9 33.50 2.40 1 3 -9 30.90 3.10 1 3 -9 29.00 2.80 1 3 -9 35.10 2.40 1 3 -9 28.40 2.60 1 3 -9 31.20 3.20 -1 -3 9 23.70 4.30 -1 -3 9 32.70 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4.30 3.10 6 2 -9 0.50 1.80 6 2 -9 6.20 1.80 6 2 -9 1.40 3.10 6 2 -9 1.00 1.20 6 2 -9 3.20 1.00 6 2 -9 4.50 1.20 -6 -2 9 2.30 3.40 5 2 -9 75.49 3.60 5 2 -9 75.49 3.80 5 2 -9 74.09 3.80 5 2 -9 76.49 5.00 5 2 -9 78.19 4.20 5 2 -9 77.99 5.60 5 2 -9 81.39 6.10 -5 -2 9 68.39 6.80 -5 -2 9 79.79 3.60 -5 -2 9 74.49 10.00 -5 -2 9 72.09 9.30 4 2 -9 87.89 6.40 4 2 -9 89.29 4.00 4 2 -9 99.79 5.40 4 2 -9 90.29 4.60 4 2 -9 88.59 4.30 4 2 -9 95.89 4.10 4 2 -9 96.79 5.00 4 2 -9 94.79 5.60 -4 -2 9 98.89 6.80 -4 -2 9 89.89 4.00 -4 -2 9 98.69 9.00 -4 -2 9 89.59 5.00 -4 -2 9 92.29 10.90 -4 -2 9 85.89 8.10 -4 -2 9 101.29 9.30 -4 -2 9 88.99 5.50 -4 -2 9 88.59 5.60 3 2 -9 143.89 6.00 3 2 -9 142.09 6.10 3 2 -9 134.99 6.70 3 2 -9 139.19 6.60 3 2 -9 128.69 6.60 3 2 -9 137.59 5.80 3 2 -9 144.49 6.20 -3 -2 9 145.59 9.50 -3 -2 9 151.48 9.50 -3 -2 9 141.59 5.40 -3 -2 9 152.78 6.10 -3 -2 9 147.09 8.50 -3 -2 9 148.99 8.50 -3 -2 9 136.89 8.10 -3 -2 9 135.49 8.40 2 2 -9 45.40 2.90 2 2 -9 44.40 2.90 2 2 -9 42.10 2.90 2 2 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6.30 0 -5 10 85.09 4.30 0 -5 10 80.79 6.40 0 -5 10 81.99 6.50 0 -5 10 76.99 5.00 0 -5 10 91.09 5.60 -1 5 -10 89.19 4.30 -1 5 -10 69.19 3.90 -1 5 -10 81.39 4.30 -1 5 -10 76.09 3.80 -1 5 -10 85.99 4.10 -1 5 -10 79.39 4.20 -1 5 -10 82.49 3.90 -1 5 -10 82.69 3.70 1 -5 10 79.39 3.80 1 -5 10 80.79 4.10 1 -5 10 71.29 5.80 1 -5 10 76.09 5.00 1 -5 10 68.39 6.10 1 -5 10 82.39 4.80 1 -5 10 72.29 6.60 1 -5 10 84.69 9.60 1 -5 10 81.69 6.50 -2 5 -10 12.80 1.80 -2 5 -10 13.40 1.80 -2 5 -10 12.90 1.50 -2 5 -10 14.90 1.90 -2 5 -10 12.00 1.60 -2 5 -10 14.30 1.70 -2 5 -10 15.50 2.30 -2 5 -10 11.00 1.80 -2 5 -10 12.70 1.50 -2 5 -10 12.20 2.00 -2 5 -10 17.00 1.90 2 -5 10 16.30 3.80 2 -5 10 8.80 4.50 2 -5 10 15.70 1.80 2 -5 10 8.90 2.00 2 -5 10 12.10 4.30 2 -5 10 14.10 2.20 -3 5 -10 55.49 3.60 -3 5 -10 59.69 3.20 -3 5 -10 51.39 3.10 -3 5 -10 62.49 4.00 -3 5 -10 60.29 3.70 -3 5 -10 54.99 3.20 -3 5 -10 64.59 3.70 3 -5 10 57.89 4.50 3 -5 10 51.69 6.60 3 -5 10 56.19 5.00 3 -5 10 60.59 3.20 -4 5 -10 52.69 3.00 -4 5 -10 53.09 2.80 -4 5 -10 41.40 3.00 -4 5 -10 48.30 2.80 -4 5 -10 40.10 3.70 -4 5 -10 48.00 3.50 -4 5 -10 50.19 2.70 4 -5 10 47.00 3.30 4 -5 10 50.19 2.70 4 -5 10 48.20 2.80 4 -5 10 43.40 5.10 -5 5 -10 4.50 1.00 -5 5 -10 5.10 1.30 -5 5 -10 5.70 0.90 -5 5 -10 5.30 0.90 -5 5 -10 5.80 1.00 5 -5 10 7.00 1.20 5 -5 10 6.00 1.00 5 -5 10 5.40 1.00 5 -5 10 7.60 1.10 8 4 -10 7.60 0.90 -8 -4 10 7.90 1.10 -8 -4 10 6.80 0.90 7 4 -10 14.20 4.40 7 4 -10 11.80 2.60 7 4 -10 10.00 2.00 -7 -4 10 10.00 1.20 -7 -4 10 8.60 1.20 -7 -4 10 8.50 1.70 -7 -4 10 9.20 1.20 6 4 -10 277.47 9.90 6 4 -10 262.47 9.80 6 4 -10 280.17 14.80 6 4 -10 274.07 9.70 6 4 -10 276.77 10.50 6 4 -10 283.67 13.70 -6 -4 10 277.27 10.00 -6 -4 10 270.77 11.20 5 4 -10 34.20 2.40 5 4 -10 33.00 4.00 5 4 -10 28.00 2.80 5 4 -10 33.30 2.80 5 4 -10 34.80 2.40 -5 -4 10 40.10 4.90 -5 -4 10 34.20 8.40 -5 -4 10 32.80 3.90 -5 -4 10 35.80 2.30 4 4 -10 219.88 8.60 4 4 -10 213.28 9.00 4 4 -10 204.08 9.60 4 4 -10 220.38 10.10 4 4 -10 197.08 11.60 4 4 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-1 -4 10 72.49 5.50 -1 -4 10 64.39 4.60 -1 -4 10 76.59 7.50 -1 -4 10 77.09 5.60 -1 -4 10 67.29 7.30 -1 -4 10 75.59 5.90 -1 -4 10 65.69 6.70 0 4 -10 286.67 12.50 0 4 -10 317.17 11.10 0 4 -10 306.57 11.10 0 4 -10 336.17 12.40 0 4 -10 320.17 11.20 0 4 -10 323.47 12.20 0 4 -10 315.67 11.00 0 -4 10 313.57 15.20 0 -4 10 312.47 11.20 0 -4 10 334.57 13.60 0 -4 10 332.27 11.70 0 -4 10 307.47 13.00 0 -4 10 322.87 13.90 0 -4 10 325.67 13.50 0 -4 10 302.97 12.40 -1 4 -10 20.20 2.00 -1 4 -10 20.00 2.40 -1 4 -10 19.60 2.30 -1 4 -10 20.20 2.10 -1 4 -10 18.20 2.10 -1 4 -10 17.30 2.00 -1 4 -10 13.20 1.90 -1 4 -10 18.90 1.90 -1 4 -10 16.10 2.00 -1 4 -10 18.60 1.80 1 -4 10 17.70 3.60 1 -4 10 9.90 5.80 1 -4 10 18.90 2.80 1 -4 10 21.00 3.60 1 -4 10 21.40 3.40 1 -4 10 22.60 2.10 1 -4 10 18.50 2.60 -2 4 -10 1.90 1.10 -2 4 -10 0.70 1.00 -2 4 -10 1.00 1.10 -2 4 -10 2.10 1.00 -2 4 -10 -1.00 1.30 -2 4 -10 1.90 1.20 -2 4 -10 2.80 1.50 -2 4 -10 3.80 1.40 -2 4 -10 -0.10 1.10 -2 4 -10 4.20 1.70 2 -4 10 1.10 1.60 2 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-10 2.30 1.20 6 3 -10 -1.90 3.50 6 3 -10 1.40 0.90 6 3 -10 3.70 3.30 6 3 -10 -0.90 1.50 6 3 -10 0.10 1.00 -6 -3 10 -1.70 3.00 -6 -3 10 -0.50 1.60 5 3 -10 53.79 2.90 5 3 -10 55.79 2.90 5 3 -10 45.00 3.30 5 3 -10 52.09 3.50 5 3 -10 55.89 6.50 5 3 -10 52.79 4.80 -5 -3 10 51.59 5.50 -5 -3 10 49.99 2.80 -5 -3 10 70.29 12.10 -5 -3 10 43.30 7.50 -5 -3 10 56.89 8.10 -5 -3 10 58.59 4.50 4 3 -10 112.69 7.00 4 3 -10 108.49 5.20 4 3 -10 99.19 4.90 4 3 -10 120.39 6.50 4 3 -10 107.39 5.80 4 3 -10 103.29 4.50 4 3 -10 102.99 4.50 -4 -3 10 104.99 9.40 -4 -3 10 98.29 6.40 -4 -3 10 106.39 5.90 -4 -3 10 106.99 7.10 -4 -3 10 105.79 5.40 -4 -3 10 101.79 4.40 -4 -3 10 96.39 8.50 -4 -3 10 93.49 10.80 3 3 -10 49.40 6.10 3 3 -10 67.29 3.70 3 3 -10 63.09 4.30 3 3 -10 64.39 5.50 3 3 -10 56.99 3.50 3 3 -10 58.89 5.40 3 3 -10 61.19 4.20 3 3 -10 57.79 3.00 3 3 -10 64.09 3.50 -3 -3 10 56.59 7.40 -3 -3 10 59.49 3.70 -3 -3 10 62.09 7.90 -3 -3 10 62.19 4.50 -3 -3 10 61.69 5.70 2 3 -10 129.99 5.70 2 3 -10 132.19 6.00 2 3 -10 132.79 5.70 2 3 -10 128.39 5.50 2 3 -10 125.29 7.40 2 3 -10 118.19 7.20 2 3 -10 120.19 5.90 2 3 -10 125.89 6.40 -2 -3 10 132.59 8.40 -2 -3 10 119.49 8.20 -2 -3 10 141.29 9.50 -2 -3 10 124.39 8.00 -2 -3 10 136.79 7.60 -2 -3 10 134.39 9.10 -2 -3 10 133.59 5.80 -2 -3 10 112.59 8.00 -2 -3 10 129.79 5.00 1 3 -10 7.10 1.10 1 3 -10 7.00 1.20 1 3 -10 6.90 1.80 1 3 -10 7.60 1.80 1 3 -10 7.30 1.30 1 3 -10 5.80 2.20 -1 -3 10 5.10 2.20 -1 -3 10 6.40 2.80 -1 -3 10 2.90 3.90 -1 -3 10 5.30 3.10 -1 -3 10 7.60 3.20 -1 -3 10 9.30 4.10 0 3 -10 27.30 2.40 0 3 -10 26.10 2.20 0 3 -10 28.40 2.40 0 3 -10 29.40 3.70 0 3 -10 22.90 2.00 0 3 -10 30.60 2.10 0 3 -10 29.20 2.20 0 3 -10 23.40 2.10 0 -3 10 25.90 3.00 0 -3 10 32.20 4.60 0 -3 10 28.90 2.40 0 -3 10 21.60 5.10 0 -3 10 18.90 3.30 0 -3 10 28.30 3.70 0 -3 10 21.60 3.60 0 -3 10 25.90 3.50 -1 3 -10 162.68 6.30 -1 3 -10 156.08 6.20 -1 3 -10 152.38 6.20 -1 3 -10 169.48 6.90 -1 3 -10 151.28 5.90 -1 3 -10 165.98 6.20 -1 3 -10 158.78 6.20 -1 3 -10 160.88 6.40 -1 3 -10 144.29 6.50 -1 3 -10 159.28 6.60 -1 3 -10 162.48 6.10 -1 3 -10 152.68 6.40 1 -3 10 144.89 11.50 1 -3 10 148.69 7.60 1 -3 10 166.58 8.40 1 -3 10 162.48 6.60 1 -3 10 161.48 8.20 1 -3 10 156.48 9.20 1 -3 10 137.09 7.80 1 -3 10 164.68 8.10 -2 3 -10 3.00 1.20 -2 3 -10 1.70 1.10 -2 3 -10 1.30 1.10 -2 3 -10 0.40 1.00 -2 3 -10 4.10 1.60 -2 3 -10 -0.40 1.30 -2 3 -10 0.90 1.00 -2 3 -10 -1.20 1.30 -2 3 -10 1.90 1.10 -2 3 -10 3.40 1.30 -2 3 -10 0.40 1.20 -2 3 -10 -0.70 1.90 -2 3 -10 1.80 1.30 -2 3 -10 0.70 1.40 2 -3 10 -2.60 3.00 2 -3 10 2.10 1.90 2 -3 10 1.00 2.10 2 -3 10 3.70 3.30 2 -3 10 5.90 3.00 2 -3 10 2.50 2.20 2 -3 10 1.40 1.00 -3 3 -10 107.19 4.80 -3 3 -10 108.29 5.10 -3 3 -10 105.19 4.90 -3 3 -10 103.09 4.80 -3 3 -10 104.59 4.80 -3 3 -10 109.39 5.60 -3 3 -10 108.89 4.70 -3 3 -10 108.69 5.00 -3 3 -10 98.39 4.60 -3 3 -10 110.69 4.80 3 -3 10 105.49 4.70 3 -3 10 101.79 5.40 3 -3 10 95.69 5.40 3 -3 10 104.69 6.30 3 -3 10 112.39 8.30 -4 3 -10 77.79 4.30 -4 3 -10 75.49 4.00 -4 3 -10 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4 -1 -17 48.80 2.20 4 -1 -17 49.90 2.40 -4 1 17 46.90 3.80 -4 1 17 49.60 3.20 -4 1 17 45.90 3.00 3 -1 -17 14.40 1.30 3 -1 -17 13.70 1.60 3 -1 -17 15.50 1.30 3 -1 -17 15.20 1.30 -3 1 17 17.10 2.20 -3 1 17 11.30 1.90 -3 1 17 17.10 2.60 -3 1 17 13.60 5.70 2 -1 -17 28.40 1.90 2 -1 -17 23.60 2.50 2 -1 -17 29.60 1.70 2 -1 -17 29.90 1.80 2 -1 -17 26.30 2.60 2 -1 -17 30.20 1.80 -2 1 17 16.30 6.40 -2 1 17 26.80 3.10 -2 1 17 39.90 4.10 -2 1 17 32.50 2.50 1 -1 -17 40.50 2.10 1 -1 -17 44.40 2.30 1 -1 -17 43.10 2.20 1 -1 -17 42.40 2.20 1 -1 -17 41.10 2.30 1 -1 -17 44.80 2.40 1 -1 -17 38.10 2.40 -1 1 17 41.50 3.40 -1 1 17 39.00 2.80 -1 1 17 35.70 5.00 0 -1 -17 22.10 1.80 0 -1 -17 22.20 1.60 0 -1 -17 22.20 1.50 0 -1 -17 25.60 1.50 0 -1 -17 22.10 1.70 0 -1 -17 24.40 1.80 0 1 17 21.00 2.90 0 1 17 21.30 2.10 -1 -1 -17 19.00 1.70 -1 -1 -17 15.90 1.60 -1 -1 -17 14.90 1.50 -1 -1 -17 19.60 1.70 -1 -1 -17 18.70 1.60 -1 -1 -17 18.30 2.00 1 1 17 12.50 2.20 -2 -1 -17 5.90 0.90 -2 -1 -17 3.60 0.80 -2 -1 -17 5.30 0.80 -2 -1 -17 6.00 1.20 5 -2 -17 0.30 0.50 5 -2 -17 1.10 0.50 -5 2 17 1.30 1.50 4 -2 -17 25.10 1.50 4 -2 -17 24.20 2.10 4 -2 -17 21.50 1.50 4 -2 -17 25.60 1.40 -4 2 17 21.30 2.70 -4 2 17 27.00 2.50 -4 2 17 27.30 2.60 3 -2 -17 157.78 5.80 3 -2 -17 162.78 5.80 3 -2 -17 158.48 5.80 3 -2 -17 160.28 5.80 -3 2 17 157.18 6.40 -3 2 17 161.08 6.80 -3 2 17 149.59 7.40 2 -2 -17 0.50 0.90 2 -2 -17 0.20 0.60 2 -2 -17 1.30 0.70 2 -2 -17 1.00 0.70 2 -2 -17 0.40 0.80 -2 2 17 -2.10 4.60 -2 2 17 -0.30 1.40 -2 2 17 -0.30 1.50 -2 2 17 1.70 2.60 1 -2 -17 38.20 2.10 1 -2 -17 38.80 2.00 1 -2 -17 37.30 2.10 1 -2 -17 38.10 2.20 1 -2 -17 38.90 2.00 1 -2 -17 37.10 2.10 -1 2 17 41.20 3.40 -1 2 17 43.50 2.80 -1 2 17 34.10 5.40 0 -2 -17 0.00 0.60 0 -2 -17 1.80 0.90 0 -2 -17 0.00 0.80 0 -2 -17 1.00 0.70 0 -2 -17 1.70 0.80 0 2 17 -0.90 1.20 0 2 17 4.40 1.80 -1 -2 -17 2.00 0.90 -1 -2 -17 0.80 0.70 -1 -2 -17 -0.20 0.80 -1 -2 -17 0.90 0.80 -1 -2 -17 0.00 0.80 5 -3 -17 0.90 0.50 -5 3 17 -0.60 1.60 4 -3 -17 77.19 3.10 4 -3 -17 79.59 3.40 4 -3 -17 82.99 3.10 4 -3 -17 72.99 3.10 -4 3 17 81.09 4.00 -4 3 17 67.99 4.20 3 -3 -17 38.70 1.90 3 -3 -17 34.60 1.90 3 -3 -17 36.50 2.80 3 -3 -17 36.40 1.80 3 -3 -17 37.30 2.10 -3 3 17 33.40 2.70 -3 3 17 30.80 3.80 -3 3 17 43.10 3.10 2 -3 -17 0.70 0.70 2 -3 -17 1.30 0.80 2 -3 -17 0.10 0.70 2 -3 -17 -0.20 1.00 2 -3 -17 1.20 0.80 2 -3 -17 0.10 0.60 -2 3 17 1.10 3.10 -2 3 17 0.70 1.30 -2 3 17 -1.40 1.50 1 -3 -17 58.09 2.50 1 -3 -17 51.19 2.60 1 -3 -17 62.49 2.60 1 -3 -17 52.79 2.50 1 -3 -17 58.69 2.70 1 -3 -17 56.99 2.60 -1 3 17 47.00 3.70 -1 3 17 55.99 3.20 0 -3 -17 83.79 3.40 0 -3 -17 71.39 3.60 0 -3 -17 87.29 3.40 0 -3 -17 85.89 3.30 0 -3 -17 82.69 3.40 0 -3 -17 72.19 3.30 0 -3 -17 87.59 3.30 0 3 17 81.09 3.70 0 3 17 70.69 4.60 -1 -3 -17 -0.10 0.60 -1 -3 -17 0.00 0.70 -1 -3 -17 1.40 0.70 -1 -3 -17 0.90 0.60 -1 -3 -17 -0.80 0.90 -1 -3 -17 1.50 0.70 -1 -3 -17 1.60 1.20 -5 4 17 41.10 3.50 4 -4 -17 0.40 0.60 4 -4 -17 0.70 0.60 4 -4 -17 0.20 1.10 -4 4 17 0.10 0.40 -4 4 17 1.00 1.20 -4 4 17 2.60 1.90 3 -4 -17 16.30 1.30 3 -4 -17 11.30 1.30 3 -4 -17 13.60 1.10 -3 4 17 13.20 1.80 -3 4 17 15.30 2.10 -3 4 17 10.40 2.60 2 -4 -17 3.60 0.70 2 -4 -17 6.00 0.90 2 -4 -17 7.10 1.20 2 -4 -17 4.30 0.70 2 -4 -17 5.00 0.90 2 -4 -17 4.20 0.80 -2 4 17 3.80 1.60 -2 4 17 2.60 1.40 1 -4 -17 14.40 1.30 1 -4 -17 13.90 1.20 1 -4 -17 10.50 1.10 1 -4 -17 11.70 1.20 1 -4 -17 12.90 1.50 1 -4 -17 10.50 1.30 -1 4 17 10.20 1.60 -1 4 17 10.40 2.00 0 -4 -17 2.80 1.30 0 -4 -17 2.40 1.10 0 -4 -17 2.10 1.10 0 -4 -17 1.10 0.80 0 -4 -17 1.80 1.00 -1 -4 -17 75.39 2.80 -1 -4 -17 71.79 2.90 -1 -4 -17 73.19 2.90 -1 -4 -17 73.29 2.90 -1 -4 -17 71.39 2.80 4 -5 -17 0.00 0.40 4 -5 -17 0.50 0.50 -4 5 17 -0.80 0.60 -4 5 17 -1.80 1.10 -4 5 17 2.60 2.00 3 -5 -17 1.30 0.70 3 -5 -17 0.40 0.80 3 -5 -17 1.60 0.60 3 -5 -17 1.10 0.60 -3 5 17 0.50 0.40 -3 5 17 2.40 1.40 -3 5 17 -2.10 1.20 2 -5 -17 102.19 4.10 2 -5 -17 117.69 4.50 2 -5 -17 109.69 4.30 2 -5 -17 98.59 3.90 2 -5 -17 111.49 4.10 -2 5 17 106.09 5.00 -2 5 17 103.69 5.50 1 -5 -17 6.80 1.10 1 -5 -17 6.30 0.80 1 -5 -17 7.80 1.00 1 -5 -17 5.20 1.20 -1 5 17 5.20 1.80 0 -5 -17 -1.20 0.80 0 -5 -17 0.70 0.60 0 -5 -17 0.50 0.60 0 -5 -17 1.00 0.50 0 -5 -17 0.10 0.60 3 -6 -17 11.90 0.90 3 -6 -17 11.50 1.00 -3 6 17 7.80 1.40 2 -6 -17 2.90 0.70 2 -6 -17 2.20 0.60 2 -6 -17 2.60 0.60 -2 6 17 5.30 1.50 1 -6 -17 76.99 3.20 1 -6 -17 69.79 2.90 1 -6 -17 74.79 2.90 1 -6 -17 74.69 3.00 3 4 -18 0.70 0.70 -3 -4 18 1.60 1.00 2 4 -18 14.60 1.60 2 4 -18 14.60 1.20 2 4 -18 16.00 1.60 -2 -4 18 10.80 1.30 -2 -4 18 17.30 1.90 1 4 -18 32.20 1.60 1 4 -18 29.20 1.70 -1 -4 18 34.80 2.40 -1 -4 18 29.70 1.80 4 3 -18 20.40 1.40 -4 -3 18 17.60 2.00 3 3 -18 71.89 3.50 3 3 -18 78.49 3.00 3 3 -18 78.89 3.10 -3 -3 18 78.69 3.80 -3 -3 18 87.29 4.20 2 3 -18 17.10 1.30 2 3 -18 18.60 1.60 2 3 -18 18.20 1.40 -2 -3 18 14.20 1.80 -2 -3 18 20.60 2.10 1 3 -18 9.90 1.20 1 3 -18 13.10 1.30 -1 -3 18 10.70 2.40 -1 -3 18 11.60 1.60 0 3 -18 10.10 1.10 0 3 -18 12.00 1.30 0 -3 18 11.90 1.40 4 2 -18 1.80 0.50 4 2 -18 3.00 0.60 -4 -2 18 2.40 1.20 3 2 -18 26.50 1.40 3 2 -18 22.00 2.00 3 2 -18 30.00 2.10 -3 -2 18 28.70 2.10 -3 -2 18 28.40 2.50 2 2 -18 34.80 2.00 2 2 -18 35.90 1.80 2 2 -18 35.90 1.90 -2 -2 18 40.70 2.30 -2 -2 18 38.50 2.50 -2 -2 18 34.20 2.80 1 2 -18 6.00 0.90 1 2 -18 5.40 0.80 1 2 -18 7.10 1.10 -1 -2 18 5.90 1.30 -1 -2 18 7.60 1.10 0 2 -18 82.09 3.20 0 2 -18 80.09 3.20 0 -2 18 83.19 3.50 4 1 -18 19.00 1.10 4 1 -18 17.50 1.20 -4 -1 18 21.50 2.30 -4 -1 18 16.20 2.00 3 1 -18 3.50 0.90 3 1 -18 3.70 0.80 -3 -1 18 2.90 1.50 -3 -1 18 3.60 2.20 -3 -1 18 4.00 1.90 2 1 -18 7.00 0.80 2 1 -18 6.80 1.10 2 1 -18 6.80 0.90 -2 -1 18 5.30 1.40 -2 -1 18 6.30 1.30 1 1 -18 39.10 2.00 1 1 -18 41.70 2.00 1 1 -18 37.60 2.00 1 1 -18 37.70 2.00 -1 -1 18 46.70 4.30 0 1 -18 1.30 0.70 0 1 -18 1.20 0.90 0 1 -18 0.30 0.70 0 1 -18 1.20 0.70 0 -1 18 0.00 0.90 4 0 -18 139.99 5.00 4 0 -18 139.39 4.90 -4 0 18 140.69 5.90 -4 0 18 140.79 5.40 3 0 -18 0.20 0.50 3 0 -18 -0.20 0.70 3 0 -18 0.30 0.60 -3 0 18 0.40 1.20 -3 0 18 0.10 1.20 -3 0 18 3.20 1.70 2 0 -18 8.00 1.00 2 0 -18 6.60 0.80 2 0 -18 9.20 1.10 -2 0 18 8.90 1.90 -2 0 18 6.70 1.30 -2 0 18 5.20 1.40 1 0 -18 1.70 0.80 1 0 -18 -0.30 0.60 1 0 -18 0.30 0.90 1 0 -18 0.90 0.70 -1 0 18 0.60 1.40 0 0 -18 0.40 0.70 0 0 -18 0.80 0.70 0 0 -18 -0.50 0.70 0 0 18 -0.20 1.00 4 -1 -18 19.30 1.30 4 -1 -18 21.50 1.20 4 -1 -18 22.10 1.80 -4 1 18 20.50 2.20 -4 1 18 26.40 2.70 3 -1 -18 3.80 0.70 3 -1 -18 4.80 0.80 3 -1 -18 2.90 0.80 -3 1 18 0.50 1.20 -3 1 18 3.60 1.30 -3 1 18 0.20 1.80 2 -1 -18 6.60 0.80 2 -1 -18 6.40 0.90 -2 1 18 4.10 1.20 -2 1 18 6.60 1.50 -2 1 18 2.40 2.80 1 -1 -18 42.80 1.90 1 -1 -18 40.30 2.10 -1 1 18 42.70 2.90 -1 1 18 34.50 2.40 0 -1 -18 0.20 0.80 0 -1 -18 0.20 0.70 0 -1 -18 -1.10 1.40 0 -1 -18 -1.10 0.60 4 -2 -18 0.70 0.50 4 -2 -18 2.50 0.70 -4 2 18 1.10 1.20 -4 2 18 -0.10 1.60 3 -2 -18 21.80 1.90 3 -2 -18 23.30 1.40 3 -2 -18 24.90 1.40 3 -2 -18 25.70 1.50 -3 2 18 24.60 2.10 -3 2 18 32.60 4.30 -3 2 18 18.10 2.40 2 -2 -18 34.60 1.80 2 -2 -18 30.80 1.80 2 -2 -18 39.30 1.90 1 -2 -18 7.10 0.90 1 -2 -18 5.30 1.30 1 -2 -18 4.90 1.00 1 -2 -18 6.80 0.90 -1 2 18 6.40 1.30 -1 2 18 7.40 1.60 0 -2 -18 77.49 3.20 0 -2 -18 84.49 3.10 0 -2 -18 80.69 3.10 -4 3 18 17.80 2.50 3 -3 -18 78.59 3.00 3 -3 -18 82.79 3.10 -3 3 18 82.89 3.90 2 -3 -18 15.80 1.10 2 -3 -18 15.40 1.30 2 -3 -18 13.60 1.10 -2 3 18 19.70 2.10 -2 3 18 12.60 1.70 1 -3 -18 13.20 1.40 1 -3 -18 10.30 1.20 1 -3 -18 9.80 1.20 1 -3 -18 9.00 1.40 1 -3 -18 9.90 1.10 1 -3 -18 12.60 1.10 0 -3 -18 13.30 1.00 0 -3 -18 12.30 1.10 0 -3 -18 10.60 1.30 3 -4 -18 1.10 0.50 3 -4 -18 0.20 0.70 -3 4 18 -0.70 1.10 2 -4 -18 16.20 1.70 2 -4 -18 14.90 1.20 2 -4 -18 14.70 1.10 -2 4 18 11.40 1.60 1 -4 -18 31.00 1.80 1 -4 -18 33.70 1.60 -2 0 19 1.60 1.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 66316 _shelx_res_file ; TITL bw2601_a.res in P2(1)/n bw2601_a.res created by SHELXL-2019/3 at 11:32:47 on 21-Sep-2026 REM Old TITL bw2601 in P21/n #14 REM SHELXT solution in P2(1)/n REM R1 0.127, Rweak 0.005, Alpha 0.021, Orientation as input REM Formula found by SHELXT: C20 B2 N2 O4 F8 S2 Zn CELL 1.54178 7.1601 11.9574 15.2293 90.000 103.519 90.000 ZERR 2.000 0.0003 0.0004 0.0005 0.000 0.002 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H B N O F S ZN UNIT 40 36 4 4 8 16 4 2 TEMP -154.15 SIZE 0.057 0.152 0.157 L.S. 10 BOND $H LIST 4 FMAP 2 PLAN 20 HTAB O2 F1 HTAB O2 F2_$2 MPLA 5 ZN1 O1 N1 N1_$1 O1_$1 MPLA 9 N1 C1 C2 C3 C4 C5 C6 O1 ZN1 MPLA 6 C6 C7 C8 C9 C10 S1 EQIV $1 1-x, 1-y, 1-z EQIV $2 3/2-x, 1/2+y, 3/2-z ACTA WGHT 0.036500 1.605100 FVAR 0.40778 ZN1 8 0.500000 0.500000 0.500000 10.50000 0.03343 0.02063 = 0.02105 -0.00211 0.01042 0.00279 S1 7 0.187593 0.723747 0.699585 11.00000 0.03700 0.03222 = 0.02409 0.00448 0.01309 0.01063 F1 6 0.802154 0.247746 0.679034 11.00000 0.06485 0.02526 = 0.08700 -0.00290 -0.00287 -0.00738 F2 6 0.808887 0.077506 0.738991 11.00000 0.07152 0.08049 = 0.05749 0.04475 0.00545 0.01019 F3 6 0.526410 0.150395 0.661754 11.00000 0.03034 0.10356 = 0.05070 -0.00344 0.01385 0.00040 F4 6 0.747952 0.098581 0.588749 11.00000 0.06304 0.06827 = 0.04793 -0.02155 0.02421 -0.00266 C1 1 0.789023 0.665226 0.458210 11.00000 0.02954 0.05021 = 0.02567 0.00861 0.01102 0.00371 AFIX 43 H1 2 0.826771 0.605726 0.424795 11.00000 -1.20000 AFIX 0 O1 5 0.369089 0.603218 0.580059 11.00000 0.03038 0.01944 = 0.02654 -0.00298 0.01306 -0.00236 O2 5 0.727414 0.456950 0.615343 11.00000 0.05712 0.02680 = 0.02732 -0.00336 -0.00094 0.00762 AFIX 148 H2A 2 0.725141 0.394592 0.624017 11.00000 0.05198 AFIX 148 H2B 2 0.724115 0.493151 0.651629 11.00000 0.06806 AFIX 0 N1 4 0.642087 0.649482 0.497017 11.00000 0.02623 0.03014 = 0.02053 0.00419 0.00834 0.00126 C2 1 0.888054 0.765355 0.465082 11.00000 0.02506 0.06164 = 0.03257 0.01842 0.00708 -0.00378 AFIX 43 H2 2 0.989151 0.775495 0.435059 11.00000 -1.20000 AFIX 0 C3 1 0.837788 0.849605 0.515929 11.00000 0.02726 0.04563 = 0.04084 0.01667 -0.00175 -0.01249 AFIX 43 H3 2 0.904055 0.919023 0.521513 11.00000 -1.20000 AFIX 0 C4 1 0.689204 0.833193 0.559428 11.00000 0.02771 0.03021 = 0.03174 0.00567 0.00039 -0.00547 AFIX 43 H4 2 0.656277 0.889617 0.597064 11.00000 -1.20000 AFIX 0 C5 1 0.590734 0.732820 0.546538 11.00000 0.02370 0.02446 = 0.01987 0.00473 0.00174 -0.00030 C6 1 0.425009 0.701979 0.587040 11.00000 0.02377 0.02027 = 0.01625 0.00031 0.00124 0.00079 C7 1 0.330029 0.780738 0.633800 11.00000 0.02802 0.02150 = 0.01799 -0.00011 0.00258 0.00187 C8 1 0.322431 0.897303 0.634500 11.00000 0.03762 0.02332 = 0.03041 -0.00126 0.00187 0.00489 AFIX 43 H8 2 0.390280 0.944439 0.602466 11.00000 -1.20000 AFIX 0 C9 1 0.201797 0.936142 0.688551 11.00000 0.05251 0.02992 = 0.03827 -0.01250 0.00134 0.01316 AFIX 43 H9 2 0.178309 1.013201 0.696706 11.00000 -1.20000 AFIX 0 C10 1 0.122109 0.852763 0.727972 11.00000 0.04935 0.04655 = 0.02439 -0.00584 0.00919 0.02096 AFIX 43 H10 2 0.038714 0.865221 0.767203 11.00000 -1.20000 AFIX 0 B1 3 0.719113 0.142870 0.667901 11.00000 0.02638 0.02213 = 0.02491 0.00308 0.00586 0.00034 REM REM bw2601_a.hkl REM HKLF 4 REM bw2601_a.res in P2(1)/n REM wR2 = 0.0846, GooF = S = 1.052, Restrained GooF = 1.052 for all data REM R1 = 0.0330 for 2426 Fo > 4sig(Fo) and 0.0352 for all 2591 data REM 182 parameters refined using 0 restraints END WGHT 0.0365 1.6058 REM Highest difference peak 0.900, deepest hole -0.436, 1-sigma level 0.060 Q1 1 0.7502 0.1349 0.7649 11.00000 0.05 0.90 Q2 1 0.8129 0.0660 0.6412 11.00000 0.05 0.64 Q3 1 0.7110 0.2459 0.6322 11.00000 0.05 0.39 Q4 1 0.5062 0.7238 0.5632 11.00000 0.05 0.30 Q5 1 0.5845 0.0900 0.7055 11.00000 0.05 0.30 Q6 1 0.7434 0.1586 0.5963 11.00000 0.05 0.30 Q7 1 0.3506 0.8423 0.6360 11.00000 0.05 0.28 Q8 1 0.2740 0.7568 0.6628 11.00000 0.05 0.28 Q9 1 0.6968 0.2590 0.6932 11.00000 0.05 0.28 Q10 1 0.7836 0.0567 0.7174 11.00000 0.05 0.25 Q11 1 0.8457 0.2573 0.6790 11.00000 0.05 0.24 Q12 1 0.5845 0.2094 0.6788 11.00000 0.05 0.24 Q13 1 0.8984 0.1373 0.7198 11.00000 0.05 0.24 Q14 1 0.3652 0.7472 0.6051 11.00000 0.05 0.23 Q15 1 0.1457 0.7929 0.7273 11.00000 0.05 0.23 Q16 1 0.7167 0.6582 0.4804 11.00000 0.05 0.22 Q17 1 0.7691 0.8380 0.5411 11.00000 0.05 0.22 Q18 1 0.6476 0.6809 0.5387 11.00000 0.05 0.21 Q19 1 0.3920 0.9182 0.6497 11.00000 0.05 0.21 Q20 1 0.6412 0.7772 0.5684 11.00000 0.05 0.21 ; _shelx_res_checksum 32189 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn Zn1 0.500000 0.500000 0.500000 0.02437(12) Uani d 1 . . S S1 0.18759(8) 0.72375(5) 0.69959(3) 0.03012(14) Uani d 1 . . F F1 0.8022(3) 0.24775(13) 0.67903(14) 0.0624(5) Uani d 1 . . F F2 0.8089(3) 0.07751(18) 0.73899(13) 0.0714(6) Uani d 1 . . F F3 0.5264(2) 0.15039(18) 0.66175(11) 0.0608(5) Uani d 1 . . F F4 0.7480(3) 0.09858(16) 0.58875(11) 0.0579(5) Uani d 1 . . C C1 0.7890(3) 0.6652(2) 0.45821(15) 0.0344(5) Uani d 1 . . H H1 0.826771 0.605726 0.424795 0.041 Uiso calc 1 . . O O1 0.3691(2) 0.60322(11) 0.58006(9) 0.0244(3) Uani d 1 . . O O2 0.7274(3) 0.45695(15) 0.61534(11) 0.0389(4) Uani d 1 . . H H2A 0.725(2) 0.395(2) 0.6240(11) 0.052(10) Uiso calc 1 . . H H2B 0.724(2) 0.4932(17) 0.6516(13) 0.068(13) Uiso calc 1 . . N N1 0.6421(2) 0.64948(15) 0.49702(11) 0.0252(4) Uani d 1 . . C C2 0.8881(3) 0.7654(2) 0.46508(16) 0.0397(6) Uani d 1 . . H H2 0.989151 0.775495 0.435059 0.048 Uiso calc 1 . . C C3 0.8378(3) 0.8496(2) 0.51593(17) 0.0395(6) Uani d 1 . . H H3 0.904055 0.919023 0.521513 0.047 Uiso calc 1 . . C C4 0.6892(3) 0.83319(19) 0.55943(15) 0.0310(5) Uani d 1 . . H H4 0.656277 0.889617 0.597064 0.037 Uiso calc 1 . . C C5 0.5907(3) 0.73282(17) 0.54654(13) 0.0232(4) Uani d 1 . . C C6 0.4250(3) 0.70198(16) 0.58704(12) 0.0207(4) Uani d 1 . . C C7 0.3300(3) 0.78074(16) 0.63380(13) 0.0230(4) Uani d 1 . . C C8 0.3224(3) 0.89730(18) 0.63450(15) 0.0315(5) Uani d 1 . . H H8 0.390280 0.944439 0.602466 0.038 Uiso calc 1 . . C C9 0.2018(4) 0.9361(2) 0.68855(17) 0.0418(6) Uani d 1 . . H H9 0.178309 1.013201 0.696706 0.050 Uiso calc 1 . . C C10 0.1221(4) 0.8528(2) 0.72797(15) 0.0400(6) Uani d 1 . . H H10 0.038714 0.865221 0.767203 0.048 Uiso calc 1 . . B B1 0.7191(3) 0.14287(19) 0.66790(16) 0.0245(5) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Zn1 0.0334(2) 0.0206(2) 0.0211(2) 0.00279(15) 0.01042(15) -0.00211(14) S1 0.0370(3) 0.0322(3) 0.0241(3) 0.0106(2) 0.0131(2) 0.00448(19) F1 0.0648(11) 0.0253(7) 0.0870(13) -0.0074(7) -0.0029(9) -0.0029(8) F2 0.0715(12) 0.0805(14) 0.0575(11) 0.0102(10) 0.0054(9) 0.0448(10) F3 0.0303(8) 0.1036(15) 0.0507(9) 0.0004(8) 0.0138(7) -0.0034(9) F4 0.0630(10) 0.0683(11) 0.0479(9) -0.0027(9) 0.0242(8) -0.0216(8) C1 0.0295(11) 0.0502(14) 0.0257(10) 0.0037(10) 0.0110(9) 0.0086(10) O1 0.0304(7) 0.0194(7) 0.0265(7) -0.0024(5) 0.0131(6) -0.0030(5) O2 0.0571(11) 0.0268(9) 0.0273(8) 0.0076(8) -0.0009(7) -0.0034(7) N1 0.0262(8) 0.0301(9) 0.0205(8) 0.0013(7) 0.0083(7) 0.0042(7) C2 0.0251(11) 0.0616(16) 0.0326(12) -0.0038(11) 0.0071(9) 0.0184(11) C3 0.0273(11) 0.0456(14) 0.0408(13) -0.0125(10) -0.0018(10) 0.0167(11) C4 0.0277(11) 0.0302(11) 0.0317(11) -0.0055(9) 0.0004(8) 0.0057(9) C5 0.0237(9) 0.0245(10) 0.0199(9) -0.0003(8) 0.0017(7) 0.0047(7) C6 0.0238(9) 0.0203(9) 0.0162(8) 0.0008(7) 0.0012(7) 0.0003(7) C7 0.0280(10) 0.0215(10) 0.0180(9) 0.0019(7) 0.0026(7) -0.0001(7) C8 0.0376(12) 0.0233(10) 0.0304(11) 0.0049(9) 0.0019(9) -0.0013(8) C9 0.0525(15) 0.0299(12) 0.0383(13) 0.0132(11) 0.0013(11) -0.0125(10) C10 0.0493(14) 0.0466(14) 0.0244(11) 0.0210(11) 0.0092(10) -0.0058(10) B1 0.0264(11) 0.0221(11) 0.0249(11) 0.0003(9) 0.0059(9) 0.0031(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn -1.5491 0.6778 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N1 Zn1 N1 3_666 . 180.0 ? N1 Zn1 O1 3_666 3_666 78.06(6) ? N1 Zn1 O1 . 3_666 101.94(6) ? N1 Zn1 O1 3_666 . 101.94(6) ? N1 Zn1 O1 . . 78.06(6) ? O1 Zn1 O1 3_666 . 180.00(6) ? N1 Zn1 O2 3_666 . 93.30(7) ? N1 Zn1 O2 . . 86.70(7) ? O1 Zn1 O2 3_666 . 88.75(6) ? O1 Zn1 O2 . . 91.25(6) ? N1 Zn1 O2 3_666 3_666 86.70(7) ? N1 Zn1 O2 . 3_666 93.30(7) ? O1 Zn1 O2 3_666 3_666 91.25(6) ? O1 Zn1 O2 . 3_666 88.75(6) ? O2 Zn1 O2 . 3_666 180.0 ? C10 S1 C7 . . 91.42(12) ? N1 C1 C2 . . 122.1(2) ? N1 C1 H1 . . 118.9 ? C2 C1 H1 . . 118.9 ? C6 O1 Zn1 . . 115.38(12) ? Zn1 O2 H2A . . 109.5 ? Zn1 O2 H2B . . 109.5 ? H2A O2 H2B . . 117.4 ? C1 N1 C5 . . 119.2(2) ? C1 N1 Zn1 . . 125.16(16) ? C5 N1 Zn1 . . 115.26(13) ? C3 C2 C1 . . 118.8(2) ? C3 C2 H2 . . 120.6 ? C1 C2 H2 . . 120.6 ? C2 C3 C4 . . 119.8(2) ? C2 C3 H3 . . 120.1 ? C4 C3 H3 . . 120.1 ? C5 C4 C3 . . 118.4(2) ? C5 C4 H4 . . 120.8 ? C3 C4 H4 . . 120.8 ? N1 C5 C4 . . 121.54(19) ? N1 C5 C6 . . 113.04(17) ? C4 C5 C6 . . 125.39(19) ? O1 C6 C7 . . 118.84(18) ? O1 C6 C5 . . 117.80(17) ? C7 C6 C5 . . 123.35(17) ? C8 C7 C6 . . 132.8(2) ? C8 C7 S1 . . 111.11(16) ? C6 C7 S1 . . 116.03(15) ? C7 C8 C9 . . 111.4(2) ? C7 C8 H8 . . 124.3 ? C9 C8 H8 . . 124.3 ? C10 C9 C8 . . 113.4(2) ? C10 C9 H9 . . 123.3 ? C8 C9 H9 . . 123.3 ? C9 C10 S1 . . 112.67(18) ? C9 C10 H10 . . 123.7 ? S1 C10 H10 . . 123.7 ? F3 B1 F2 . . 111.9(2) ? F3 B1 F4 . . 108.78(19) ? F2 B1 F4 . . 109.5(2) ? F3 B1 F1 . . 110.4(2) ? F2 B1 F1 . . 108.2(2) ? F4 B1 F1 . . 108.0(2) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Zn1 N1 3_666 2.0624(18) ? Zn1 N1 . 2.0624(18) ? Zn1 O1 3_666 2.1030(13) ? Zn1 O1 . 2.1030(13) ? Zn1 O2 . 2.1598(16) ? Zn1 O2 3_666 2.1598(16) ? S1 C10 . 1.697(2) ? S1 C7 . 1.728(2) ? F1 B1 . 1.381(3) ? F2 B1 . 1.368(3) ? F3 B1 . 1.364(3) ? F4 B1 . 1.376(3) ? C1 N1 . 1.335(3) ? C1 C2 . 1.383(4) ? C1 H1 . 0.9500 ? O1 C6 . 1.243(2) ? O2 H2A . 0.76(2) ? O2 H2B . 0.71(2) ? N1 C5 . 1.352(3) ? C2 C3 . 1.369(4) ? C2 H2 . 0.9500 ? C3 C4 . 1.392(3) ? C3 H3 . 0.9500 ? C4 C5 . 1.383(3) ? C4 H4 . 0.9500 ? C5 C6 . 1.506(3) ? C6 C7 . 1.443(3) ? C7 C8 . 1.395(3) ? C8 C9 . 1.404(3) ? C8 H8 . 0.9500 ? C9 C10 . 1.357(4) ? C9 H9 . 0.9500 ? C10 H10 . 0.9500 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O2 H2A F1 . 0.76 1.97 2.691(2) 160 yes O2 H2B F2 2_656 0.71 2.01 2.709(2) 171 yes